Low Temperature Densification of ZnO-Based Ceramic Using Phenolic Resin as Binder

2014 ◽  
Vol 668-669 ◽  
pp. 35-38
Author(s):  
Hui Zeng ◽  
Jing Jing Xie ◽  
Hai Tao Liu ◽  
Zheng Yi Fu
Keyword(s):  
Mechanical Properties ◽  
Boundary Layer ◽  
Low Temperature ◽  
Grain Boundary ◽  
Phenolic Resin ◽  
Bending Strength ◽  
Effect Of Temperature ◽  
Microstructure And Mechanical Properties

ZnO-based ceramic was densified at low temperature by using PSP as binder. The results showed that phenolic resin filled in the ZnO grain boundary layer. The sample has a well hardness of 0.8 GPa and bending strength of 78 MPa. The effect of temperature on the microstructure and mechanical properties was also investigated. It was found that the samples sintered at 300 °C showed higher density and better mechanical properties.

Microstructure and Mechanical Properties of SiC-Al2O3 Nanocomposite Prepared by Surface Modified SiC Nanopowders

2007 ◽  
Vol 336-338 ◽  
pp. 2251-2253
Author(s):  
Lu Ting Yan ◽  
Wen Jie Si ◽  
Lian Yun Liu ◽  
Yan Peng Zheng ◽  
Chun Ai Dai
Keyword(s):  
Mechanical Properties ◽  
Low Temperature ◽  
Plasma Polymerization ◽  
Bending Strength ◽  
Low Temperature Plasma ◽  
Temperature Plasma ◽  
Microstructure And Mechanical Properties ◽  
The Matrix ◽  
Ultimate Bending Strength ◽  
Surface Modified

SiC nanopowders were surface modified by low temperature plasma polymerization. 5vol% SiC-Al2O3 nanocomposite was prepared by adding the surface modified SiC nanopowders into the matrix of Al2O3.The influence of surface modified SiC nanopowders on the properties and structure of SiCAl2O3 nanocomposite was studied. The surface modified SiC-Al2O3 nanocomposite had higher density and nicer mechanical properties than untreated SiC- Al2O3 nanocomposite because of the improvement of dispersion. The hardness and toughness of the SiC- Al2O3 nanocomposite were higher than monolithic Al2O3 but the ultimate bending strength was not perfect because of retardation of the densification and formation of unsintered pores caused by the induced oxygen during the process of powder treatment.

Effects of TiO2 on the microstructure and mechanical properties of Al2O3/ZrO2 composites

1996 ◽  
Vol 11 (6) ◽  
pp. 1545-1551 ◽  
Author(s):  
Chii-Shyang Hwang ◽  
Yu-Jing Chang
Keyword(s):  
Mechanical Properties ◽  
Electron Microscope ◽  
Grain Boundary ◽  
Room Temperature ◽  
Bending Strength ◽  
Microstructure And Mechanical Properties ◽  
Analytical Electron ◽  
Analytical Electron Microscope ◽  
Ar Gas ◽  
Zirconia Toughened Alumina

The microstructure and mechanical properties of hot-pressed zirconia-toughened alumina (ZTA), fabricated from the ZTA powders containing (Zr, Ti)O2 in Ar gas were investigated. In hot-pressed ZTA, the presence of Ti concentration in the grains of Al2O3 or (Zr, Ti)O2 was analyzed by the energy dispersive spectroscopy (EDS) attached to the analytical electron microscope (AEM) apparatus. Experimental results showed that some Ti ions diffused to the grain boundary and into the Al2O3 grains, thereby enhancing the densification of hot-pressed ZTA. It was possible to retain tetragonal ZrO2 at room temperature in the ZTA specimens containing ≥5.5 mol% TiO2 and hot pressed at 1350 °C for 1 h. The bending strength and toughness of hot-pressed ZTA were enhanced by the addition of TiO2.

Structure and properties of compact articles from high-alloyed iron powder with adding of boron nitride

2020 ◽  
pp. 39-48
Author(s):  
B. O. Bolshakov ◽  
◽  
R. F. Galiakbarov ◽  
A. M. Smyslov ◽  
◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Boron Nitride ◽  
Grain Boundary ◽  
Bending Strength ◽  
Physical And Mechanical Properties ◽  
Operating Conditions ◽  
Structure And Properties ◽  
Steam Turbines ◽  
Friction Forces ◽  
Wide Range

The results of the research of structure and properties of a composite compact from 13 Cr – 2 Мо and BN powders depending on the concentration of boron nitride are provided. It is shown that adding boron nitride in an amount of more than 2% by weight of the charge mixture leads to the formation of extended grain boundary porosity and finely dispersed BN layers in the structure, which provides a high level of wearing properties of the material. The effect of boron nitride concentration on physical and mechanical properties is determined. It was found that the introduction of a small amount of BN (up to 2 % by weight) into the compacts leads to an increase in plasticity, bending strength, and toughness by reducing the friction forces between the metal powder particles during pressing and a more complete grain boundary diffusion process during sintering. The formation of a regulated structure-phase composition of powder compacts of 13 Cr – 2 Mо – BN when the content of boron nitride changes in them allows us to provide the specified physical and mechanical properties in a wide range. The obtained results of studies of the physical and mechanical characteristics of the developed material allow us to reasonably choose the necessary composition of the powder compact for sealing structures of the flow part of steam turbines, depending on their operating conditions.

scholarly journals Effect of Sintering Temperature on Microstructure and Mechanical Properties of Hot-Pressed Fe/FeAl2O4 Composite

Crystals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 422
Author(s):  
Kuai Zhang ◽  
Yungang Li ◽  
Hongyan Yan ◽  
Chuang Wang ◽  
Hui Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Bending Strength ◽  
Sintering Temperature ◽  
Raw Materials ◽  
Hot Press ◽  
Microstructure And Mechanical Properties ◽  
Powder Particles ◽  
Hot Press Sintering ◽  
Sintering Method

An Fe/FeAl2O4 composite was prepared with Fe-Fe2O3-Al2O3 powder by a hot press sintering method. The mass ratio was 6:1:2, sintering pressure was 30 MPa, and holding time was 120 min. The raw materials for the powder particles were respectively 1 µm (Fe), 0.5 µm (Fe2O3), and 1 µm (Al2O3) in diameter. The effect of sintering temperature on the microstructure and mechanical properties of Fe/FeAl2O4 composite was studied. The results showed that Fe/FeAl2O4 composite was formed by in situ reaction at 1300 °C–1500 °C. With the increased sintering temperature, the microstructure and mechanical properties of the Fe/FeAl2O4 composite showed a change law that initially became better and then became worse. The best microstructure and optimal mechanical properties were obtained at 1400 °C. At this temperature, the grain size of Fe and FeAl2O4 phases in Fe/FeAl2O4 composite was uniform, the relative density was 96.7%, and the Vickers hardness and bending strength were 1.88 GPa and 280.0 MPa, respectively. The wettability between Fe and FeAl2O4 was enhanced with increased sintering temperature. And then the densification process was accelerated. Finally, the microstructure and mechanical properties of the Fe/FeAl2O4 composite were improved.

Preparation and Properties of SiC/Phenolic Resin for the Heat of LED

2016 ◽  
Vol 848 ◽  
pp. 454-459
Author(s):  
Cong Wu ◽  
Kang Zhao ◽  
Yu Fei Tang ◽  
Ji Yuan Ma
Keyword(s):  
Mechanical Properties ◽  
Thermal Conductivity ◽  
Powder Metallurgy ◽  
Phenolic Resin ◽  
Bending Strength ◽  
Experimental Results ◽  
Low Thermal Conductivity ◽  
Industry Standard ◽  
Insulation Performance

In order to solve the problem that low thermal conductivity of the plastics for the heat of LED, SiC/Phenolic resin for the heat of LED were fabricated combining powder metallurgy. The effects of particles diameters, content and adding nanoparticles on thermal conductivity of the fabricated composites were investigated, the mechanical properties were also characterized. The experimental results showed that the materials were obtained, and the insulation performance of the fabricated SiC/Phenolic resin was higher than the industry standard one, the thermal conductivity reached 4.1W/(m·k)-1. And the bending strength of the fabricated composites was up to 68.11MPa. The problem of low thermal conductivity of the material is expected to be solved. In addition, it is meaningful for improving LED life.

Effect of temperature on microstructure and mechanical properties of ECAPed (TiB + La2O3)/Ti-6Al-4V composites

2018 ◽  
Vol 146 ◽  
pp. 149-158 ◽  
Author(s):  
Juan Xiang ◽  
Yuanfei Han ◽  
Jianwen Le ◽  
Guangfa Huang ◽  
Lv Xiao ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Effect Of Temperature ◽  
Microstructure And Mechanical Properties

Influence of Stirring Time and Holding Time on Microstructure and Properties of the A356 Alloy Modified by Sc

2013 ◽  
Vol 750-752 ◽  
pp. 687-690 ◽  
Author(s):  
Su Zhang ◽  
Gang Yang ◽  
Jian Hong Yi ◽  
Hong Yan
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Grain Boundary ◽  
Eutectic Silicon ◽  
A356 Alloy ◽  
Holding Time ◽  
Test Results ◽  
Modification Effect ◽  
Microstructure And Mechanical Properties ◽  
Stirring Time

Effects of the holding time and the stirring time on the microstructure and mechanical properties of A356 alloy modified by Sc are researched. According to the test results, most of the eutectic silicon phases have changed to the shape of creeping point, dispersed in the grain boundary of α (Al) phase while stirring 1 minute, in which case both the tensile strength and elongation reach the highest, resulting in the best modification effect. The results also indicate that microstructure and mechanical properties of the alloy reach are the best modification effect when the melt is held 15 minute. It can be known that the optimal stirring time is 1 minute and the optimal holding time is 15 minute in the experiment condition of the work.

scholarly journals Effects of Mechanical Ball Milling Time on the Microstructure and Mechanical Properties of Mo2NiB2-Ni Cermets

Materials ◽  
2019 ◽  
Vol 12 (12) ◽  
pp. 1926 ◽  
Author(s):  
Lei Zhang ◽  
Zhifu Huang ◽  
Yangzhen Liu ◽  
Yupeng Shen ◽  
Kemin Li ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Ball Milling ◽  
Milling Time ◽  
Bending Strength ◽  
Volume Fraction ◽  
Milling Process ◽  
Microstructure And Mechanical Properties ◽  
Mechanical Ball Milling ◽  
Ball Milling Time ◽  
Milled Powders

Mo2NiB2-Ni cermets have been extensively investigated due to their outstanding properties. However, studies have not systematically examined the effect of the powder milling process on the cermets. In this study, Mo, Ni, and B raw powders were subjected to mechanical ball milling from 1 h to 15 h. XRD patterns of the milled powders confirmed that a new phase was not observed at milling times of 1 h to 15 h. With the increase in the mechanical ball milling time from 1 h to 11 h, raw powders were crushed to small fragments, in addition to a more uniform distribution, and with the increase in the mechanical ball milling time to greater than 11 h, milled powders changed slightly. Mo2NiB2-Ni cermets were fabricated by reaction boronizing sintering using the milled powders at different ball milling times. The milling time significantly affected the microstructure and mechanical properties of Mo2NiB2-Ni cermets. Moreover, the Mo2NiB2 cermet powder subjected to a milling time of 11 h exhibited the finest crystal size and the maximum volume fraction of the Mo2NiB2 hard phase. Furthermore, the cermets with a milling time of 11 h exhibited a maximum hardness and bending strength of 87.6 HRA and 1367.3 MPa, respectively.

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