Synthesis of Papercut-Like Carbon Sheets by a Simple Pyrolysis Method

2011 ◽  
Vol 239-242 ◽  
pp. 544-547
Author(s):  
Ling Ling Zhu ◽  
Pei Pei Xiao ◽  
Yi Tai Qian
Keyword(s):  
Thermal Stability ◽  
Powder Diffraction ◽  
Amorphous Carbon ◽  
Calcium Carbide ◽  
X Ray ◽  
Prepared Sample ◽  
Pyrolysis Method ◽  
Average Size ◽  
20 Nm ◽  
Thermal Stability Of

In this study, papercut-like carbon sheets with an average size of about 20 nm in thickness have been successfully synthesized by the pyrolysis of tetrachloromethane and calcium carbide in an autoclave in 600 °C in the existence of alloy (Fe-Co-Ni). The X-ray powder diffraction (XRD) reveals amorphous carbon nature of the as-prepared sample. The thermal stability of the as-prepared sample was also studied.

scholarly journals Effects of Current on Arc Fabrication of Cu Nanoparticles

2010 ◽  
Vol 2010 ◽  
pp. 1-5 ◽  
Author(s):  
M. Z. Kassaee ◽  
F. Buazar ◽  
E. Motamedi
Keyword(s):  
Thermal Stability ◽  
Distilled Water ◽  
Face Centered Cubic ◽  
Cu Nanoparticles ◽  
Dta Analysis ◽  
Face Centered ◽  
Average Size ◽  
20 Nm ◽  
Thermal Stability Of ◽  
Sem Analyses

Arc-fabricated copper nanoparticles (Cu Nps) size, morphology and the crystalline structure, as well as the yields of Nps appear sensitive to the applied currents (50–160 A) in distilled water. The results indicate that the sizes of Cu Nps are directly proportional to the currents employed. At 50 A, TEM, XRD, and SEM analyses show fabrication of relatively purest, the most dispersed, face-centered cubic (fcc) brown Cu Nps with rather smallest average size of 20 nm. At the same current, the TGA-DTA analysis reveals neither weight loss nor gain, indicating thermal stability of the fabricated Cu Nps.

Synthesis and Thermal Stability of Nontransformable Tetragonal (ZrO2)0.96(REO1.5)0.04 (Re=Sc3+, Y3+) Nanocrystals

2013 ◽  
Vol 334-335 ◽  
pp. 60-64 ◽  
Author(s):  
Mohammad Reza Loghman-Estark ◽  
Reza Shoja Razavi ◽  
Hossein Edris
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
Scanning Electron Microscopy ◽  
Sol Gel ◽  
Average Diameter ◽  
X Ray ◽  
Transmission Electron ◽  
20 Nm ◽  
Thermal Stability Of ◽  
Scanning Electron

Scandia, yttria doped zirconia ((ZrO2)0.96(REO1.5)0.04(RE=Sc3+, Y3+)) nanoparticles were prepared by the modified sol-gel method. The microstructure of the products was characterized by X-ray diffractometry (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM) and Raman spectroscopy. Thermal stabillity of SYSZ nanocrystals were also investigated. The SYSZ nanocrystals synthesized with EGM:Zr+4mole ratio 4:1, calcined at 700°C, have average diameter of ~20 nm.

Synthesis and structural study from X-ray powder diffraction of Pb0.5Th2(PO4)3

1997 ◽  
Vol 12 (2) ◽  
pp. 76-80 ◽  
Author(s):  
A. El-Yacoubi ◽  
R. Brochu ◽  
A. Serghini ◽  
M. Louër ◽  
M. Alami Talbi ◽  
...  
Keyword(s):  
Crystal Structure ◽  
Thermal Stability ◽  
Structural Study ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Structure Type ◽  
Powder Diffraction Data ◽  
Monoclinic Symmetry ◽  
X Ray ◽  
Thermal Stability Of

A new mixed lead thorium phosphate, Pb0.5Th2(PO4)3, has been isolated in the system PbO–ThO2–P2O5. Its crystal structure (monoclinic symmetry, a=17.459(1) Å, b=6.8451(4) Å, c=8.1438(5) Å, β=101.247(5)°, space group C2/c) has been determined from conventional monochromatic X-ray powder diffraction data. The structure is related to the MITh2(PO4)3 structure type. Lead atoms are located in the channels parallel to the c axis, out of the twofold axis for 0.97 Å, and are statistically distributed on a quarter of crystallographic positions. The thermal stability of this material is greater than that of the monazite-type compound PbTh(PO4)2.

Particularities of Structure and Stability of Cationic-Ordered Layered Titanates

2011 ◽  
Vol 170 ◽  
pp. 190-193 ◽  
Author(s):  
Irina Zvereva ◽  
Anna Sankovich ◽  
Alexander Missyul
Keyword(s):  
Electron Microscopy ◽  
Thermal Stability ◽  
Thermal Analysis ◽  
Scanning Electron Microscopy ◽  
Thermal Annealing ◽  
Powder Diffraction ◽  
X Ray ◽  
Stable Temperature ◽  
Thermal Stability Of ◽  
Scanning Electron

Thermal stability of the layered titanates NdMTiO4 and Nd2M2Ti3O10 (M=Na, K) featured with 1 or 3 perovskite layers has been investigated in thermal annealing at 780 – 1400°С. Their structure variations are monitored using thermal analysis (TGA, DTA), X-ray powder diffraction, and scanning electron microscopy. Judging from the decomposition sequence and the stable temperature range for individual phase, the structure of Nd2M2Ti3O10 with three perovskite layers is identified most stable among these layer titanates. As a whole, the K-containing phases are less stable than the Na-containing ones.

Strontium Hydroxyapatite Synthesis, Characterization and Cell Cytotoxicity

2010 ◽  
Vol 160-162 ◽  
pp. 117-122 ◽  
Author(s):  
Zhi Hong Li ◽  
Ji Min Wu ◽  
Shu Jie Huang ◽  
J. Guan ◽  
Xi Zheng Zhang
Keyword(s):  
Thermal Stability ◽  
Hydrothermal Method ◽  
Bone Repair ◽  
X Ray Diffraction ◽  
X Ray ◽  
Strontium Hydroxyapatite ◽  
Transmission Electron ◽  
20 Nm ◽  
Thermal Stability Of ◽  
Phase Chemical

Strontium hydroxyapatite powders was prepared by the hydrothermal method using Sr(NO3)2 and (NH4)2HPO4 as reagents. Fourier transform infrared spectroscopy, X-ray diffraction, Transmission electron microscope, Energy dispersive X-ray, and Thermogravimetric-differential thermal analysis were employed to investigate the crystalline phase, chemical composition, morphology, and thermal stability of the Strontium hydroxyapatite. And the cytotoxicity of Strontium hydroxyapatite was analyzed through MTT assay. Results showed that Strontium hydroxyapatite prepared by hydrothermal Method has excellent crystal structure, good dispersion, high purity, and rod-like morphology with dimensions 200-500 nm in length and 20 nm in diameter. Meanwhile, the apatite has poor thermal stability. However, the apatite is cytocompatible and may have better biocompatibility, which can serve as strontium source incorporation into calcium phosphate cement and for bone repair.

scholarly journals Effect of Annealing, Stoichiometry, and Surface on Magnetism of (Pr,Dy)FeCoB Microparticles Ensemble

2017 ◽  
Vol 62 (3) ◽  
pp. 1923-1930 ◽  
Author(s):  
E.N. Kablov ◽  
O.G. Ospennikova ◽  
E.I. Kunitsyna ◽  
V.P. Piskorskii ◽  
D.V. Korolev ◽  
...  
Keyword(s):  
Thermal Stability ◽  
Magnetic Properties ◽  
Phase Composition ◽  
Photoelectron Spectroscopy ◽  
Surface States ◽  
Anisotropy Field ◽  
X Ray ◽  
Average Size ◽  
Thermal Stability Of ◽  
Effect Of Surface

AbstractMagnetic properties of powder (Pr,Dy)FeCoB ferrimagnetic alloys and effects of annealing, surface states were analyzed. X-ray photoelectron spectroscopy and Mössbauer spectra of powders indicate the effect of surface states on phase composition and magnetic properties of the studied powder, if particles average size is smaller than 10 μm. Effect of stoichiometry on magnetic anisotropy was found. Thermal stability of anisotropy field was proved by replacement of Fe atoms with Co atoms.

ChemInform Abstract: X-Ray Powder Diffraction, Moessbauer Spectroscopy, and Thermal Stability of Fe7(PO4)6.

ChemInform ◽  
2010 ◽  
Vol 30 (51) ◽  
pp. no-no
Author(s):  
A. A. Belik ◽  
A. P. Malakho ◽  
K. V. Pokholok ◽  
B. I. Lazoryak
Keyword(s):  
Thermal Stability ◽  
Powder Diffraction ◽  
Moessbauer Spectroscopy ◽  
X Ray ◽  
Thermal Stability Of

Preparation and Characterization of Polyacrylonitrile-Metal-O-MMT Nanocomposites

2011 ◽  
Vol 221 ◽  
pp. 316-320
Author(s):  
Hui Xia Feng ◽  
Gong Wei Fu ◽  
Yi Wang ◽  
Na Li Chen ◽  
Rui Chen Yang
Keyword(s):  
Thermal Stability ◽  
Powder Diffraction ◽  
Interlayer Space ◽  
In Situ Polymerization ◽  
X Ray ◽  
Thermal Stability Of ◽  
Better Than ◽  
Montmorillonite Nanocomposites

Polyacrylonitrile-metal-O-montmorillonite nanocomposites were prepared by means of in situ polymerization. The Na-montmorillonite was modified by quaternary ammonium salt after the exchange of its interlayer cations with Ni2+. Infrared spectra and X-ray powder diffraction were employed to characterize the obtained polyacrylonitrile-metal-O-montmorillonite. The results of FTIR show that metal-O-montmorillonite has been concerned with the polymerization of PAN. The result of X-ray powder diffraction shows that the inserting of the acrylonitrile monomer can enlarge the interlayer space of montmorillonite. It is also shown that the polyacrylonitrile-metal-O- montmorillonite nanocomposites have been synthesized. The thermal stability of PAN /MMT is better than that of pure PAN.

Intercalation of non-aromatic heterocyclic amines into layered zirconium glycine-N,N-dimethylphosphonate

2010 ◽  
Vol 64 (1) ◽  
Author(s):  
Xin Yang ◽  
Xiang-Kai Fu ◽  
Ren-Quan Zeng
Keyword(s):  
Thermal Stability ◽  
Powder Diffraction ◽  
Heterocyclic Amines ◽  
New Materials ◽  
Acid Base ◽  
Guest Molecules ◽  
X Ray ◽  
Diffraction Patterns ◽  
Aromatic Heterocyclic ◽  
Thermal Stability Of

AbstractNew materials were prepared by intercalation reactions between layered zirconium glycine-N,N-dimethylphosphonate (ZGDMP) and non-aromatic heterocyclic amines: piperazine, piperidine, and morpholine. X-ray powder diffraction patterns showed that the entrance of piperazine, piperidine, and morpholine caused an interlayer expansion of 0.40 nm, 0.66 nm, and 0.67 nm, respectively. The infrared spectra were in agreement with an acid-base reaction, involving layered acid host COOH of ZGDMP and basic center atoms of guest molecules. Thermogravimetric curves revealed thermal stability of the intercalation compounds and content of the inserted amine molecules. These results indicate that non-aromatic heterocyclic amines were intercalated into the galleries of host ZGDMP.

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