Investigation on High-Phosphorus Electroless Ni–P Plating Technology of Stainless Steel

2011 ◽  
Vol 291-294 ◽  
pp. 129-132
Author(s):  
Xiao Juan Wu ◽  
Zheng Jun Liu ◽  
Guo De Li

The high-phosphorus electroless Ni–P plating was coated on the surface of stainless steel. Five parameters, which have much effect on coating quality, were chosen to optimize the high-phosphorus electroless Ni–P plating technology in L16(45) orthogonal test. By means of x-ray diffraction and scanning electron microscopy, the morphologies and phase structures of coating were analyzed. Furthermore, the mechanical properties of coating were studied by micro-hardness tester and universal friction-wear testing machine. The results reveal that the optimal technical parameters are as follows: 20 g•L-1 for NiSO4, 23 g•L-1 for NaH2PO2, 15 g•L-1 for C6H5O7Na3•2H2O, 8 g•L-1 for H2N-CH2-COOH, 10g•L-1 for CH3COONa, 7 g•L-1 for C4H6O4, with PH value of 4.6, which leads to perfect coating quality. Besides, the P content is 11.64 wt.%, i.e. a high-P coating. The micro-hardness of the coating is 550.67 HV and the wear loss, 4.7×10-3 g. The thermal shock test suggests that between coating and matrix exist a perfect cohesion, which is due to the homogenous and compact coating, with an amorphous structure, under the condition of the optimal technical parameters.

2011 ◽  
Vol 337 ◽  
pp. 87-90 ◽  
Author(s):  
Xiao Juan Wu ◽  
Zheng Jun Liu ◽  
Guo De Li

The high-phosphorus electroless Ni–P plating coating with 11.64 at.% was prepared by electroless technology. By means of x-ray diffraction and scanning electron microscopy, the morphologies and phase structures of coating were analyzed. Furthermore, the mechanical properties of coating were studied by micro-hardness tester and universal friction-wear testing machine. The results reveal that, with increasing heat-treatment temperatures, the hardness and the wear resistance of the coating are enhanced increasingly. Treated by 1 hour at 500 oC, the hardness and the wear resistance both display a optimum value, i.e. 1004 HV and 1.5×10-3g, respectively. The thermal shock test suggests that between coating and matrix exist a perfect cohesion.


2020 ◽  
Vol 184 ◽  
pp. 01003
Author(s):  
K. Ramya Sree ◽  
G. Keerthi Reddy ◽  
K. Aishwarya ◽  
E. Nirmala Devi ◽  
Ram. Subbiah

AISI 253MA Stainless steel samples were treat with the gas nitrating process at low heat around 450°C. It was seen that all-inclusive austenite stage exist when it is nitrade to 8 hours and post addition at time of nitrading to 16 hours the mix of ferrites and progressively substance of nitrogen was gathered in the following layers. Farther nitrading to 24 hour it has seen at Cr-N stage was discovered and turns the steel progressively firmer superficially. Erode tests were led by tribological wear testing machine to examine the tribological wear loss. Volume wear was found to be least in 18 hours test which demonstrated better improvement of wear improvement. High hardness were found in 24 hrs showing a hardness of 1080Hv. The sample nitrided to 24 hours exhibited better wear resistance, high hardness and low wear loss as well as low volume wear loss. Assessment examinations of nitrided test samples were investigated under scanning electron magnifying analysis.


2013 ◽  
Vol 300-301 ◽  
pp. 833-836
Author(s):  
Shi Jie Wang ◽  
Hao Lin ◽  
Xiao Ren Lv

The progressing cavity pump (PCP) always works in the waxy oil well. Therefore the research on the influence of various liquid paraffin contents in crude oil on the friction and wear behaviors of the progressing cavity pump`s stator is very important for choosing the best stator rubber and developing the service life of PCP. Wear behavior of nitrile butadiene rubber (NBR) and fluororubber (FKM) was investigated at room temperature using a reciprocating friction and wear testing machine under the various paraffin contents in crude oil (0%、10%、30%、50%、100%). The wear morphology of blend was analyzed through the stereomicroscope and the wear behavior of two blends was also discussed and compared. The results show that the wear resistance of FKM is better than that of NBR under the same paraffin content in crude oil; With the increase of the paraffin content, the wear and coefficient of friction also increase. When the paraffin content in crude oil is less than 30%, the wear loss of NBR and FKM are basically the same; When the paraffin content in crude oil is more than 30%, the wear loss of NBR is far more than that of FKM.


Coatings ◽  
2018 ◽  
Vol 8 (12) ◽  
pp. 451 ◽  
Author(s):  
Hongmei Zhu ◽  
Yongzuo Li ◽  
Baichun Li ◽  
Zhenyuan Zhang ◽  
Changjun Qiu

Post-treatment is crucial to improve the comprehensive performance of laser-cladded martensitic stainless steel coatings. In this work, a low-temperature tempering treatment (210 °C), for the first time, was performed on the laser-cladded AISI 420 martensitic stainless steel coating. The microstructure and properties of the pre- and post-tempering specimens were carefully investigated by XRD, SEM, TEM, a micro-hardness tester, a universal material testing machine and an electrochemical workstation. The results show that the as-cladded AISI 420 stainless steel coating mainly consisted of martensite, austenite, Fe3C and M23C6 carbides. The phase constituent of the coating remained the same, however, the martensite decomposed into finer tempered martensite with the precipitation of numerous nano-sized Fe3C carbides and reverted austenite in the as-tempered specimen. Moreover, a slight reduction was found in the micro-hardness and tensile strength, while a significant increase in elongation was achieved after tempering. The fractography showed a transition from brittle fracture to ductile fracture accordingly. The as-tempered coating exhibited a striking combination of mechanical properties and corrosion resistance. This work can provide a potential strategy to enhance the overall properties of the laser-deposited Fe-based coating for industrial applications.


2015 ◽  
Vol 1119 ◽  
pp. 628-632
Author(s):  
Alain Kusmoko ◽  
Druce Dunne ◽  
Hui Jun Li

Stellite 6 was deposited by laser cladding on a martensitic stainless steel substrate with energy inputs of 1 kW (MSS-1) and 1.8 kW (MSS-1.8). The chemical compositions and microstructures of these coatings were characterized by atomic absorption spectroscopy, optical microscopy and scanning electron microscopy. The microhardness of the coatings was measured and the wear mechanism of the coatings was assessed using a pin-on-plate (reciprocating) wear testing machine. The results showed less cracking and pore development for Stellite 6 coatings applied to the MSS steel substrate with the lower heat input (MSS-1). Further, the Stellite coating for MSS-1 was significantly harder than that obtained for MSS-1.8. The wear test results indicated that the weight loss for MSS-1 was much lower than for MSS-1.8. It is concluded that the lower hardness of the coating for MSS-1.8, markedly reduced the wear resistance of the Stellite 6 coating.


Author(s):  
A. Karthikeyan ◽  
S. Nallusamy

One of the most common problems encountered in many industrial products and its applications is wear. The purpose of this experimental research article is to analyze the wear behaviour of Al-6063 based SiC composites using pin on disc testing machine. In this present investigation there are nine different samples of Al/SiC composites with 5%, 7% and 9% volume of SiC were prepared through stir casting process. The sliding distance of 500 meter and the load 10 N were applied for wear testing of these prepared samples. From the experimental results, it was observed that the sliding velocity is greatly affects the wear rate and on increasing the sliding velocity the wear loss increases. It was also found that the wear loss decreases by increasing the amount of reinforcement element. Scanning electron microscope was used to examine the wear surfaces and found that the micro and transverse cracks, mild and severe wear occurred in the composite worn surfaces and wear structure of the composites.


SPE Journal ◽  
2021 ◽  
pp. 1-16
Author(s):  
Y. Zhou ◽  
J. H. Hu ◽  
B. Tan ◽  
Y. Jiang ◽  
Y. F. Tang

Summary Sealing is a technical bottleneck that affects drilling efficiency and cost in deep, difficult-to-drill formations. The spiral combination seal with active sand removal performance is a new type of seal, and the wear mechanism is not clear, resulting in no effective design. In this study, the wear properties of materials were measured by a friction-and-wear testing machine, and the measurement methods and criteria of wear loss and friction coefficient were established. The fitting function of working condition and friction coefficient was studied by fitting regression method. The law of influence of working conditions on friction coefficient and wear amount was determined. The actual wear model and evaluation criteria of wear condition were established by using wear test data and geometric relationship. The relationship among working conditions, contact stress, and wear depth is determined by numerical simulation method, and the wear mechanism of the new seal is revealed, which provides a theoretical basis for its application.


2011 ◽  
Vol 130-134 ◽  
pp. 984-988
Author(s):  
Xiao Peng Huang ◽  
Jian Long Huang ◽  
Jing Feng Wu ◽  
Ke Ping Zhang

Metal materials wear loss against plant abrasive of different wear process was obtained by simulation test on the abrasive wear testing machine. On the basis of it, the GM (1, 1) model is established by using grey theory. Then the state of experiment data is divided using markov chain, the state transition matrix is constructed, finally the grey markovian model is established and wear prediction of metal materials against plant abrasive is gained. The results indicate that wear prediction based on the grey markovian model is more precise than the GM (1, 1), model, relative error being only 1.13%


2013 ◽  
Vol 420 ◽  
pp. 234-239
Author(s):  
Feng Yan Yang ◽  
Shi Jie Wang ◽  
Xiao Ren Lv

The wear mechanisms of different graphite contents of NBR by 45# steel under dry sliding and water lubrication were investigated. On MPV-600 computer-controlled abrasive wear testing machine, the coefficients of friction were measured continuously. Results showed that under dry sliding condition, the rubber wear loss is big, the coefficient of friction is higher, the temperature of the friction surface is rise obviously. Wear loss and friction coefficient of NBR decrease with the increase of graphite contents; With the increase of graphite contents wear loss and the friction coefficient decreases, and is mainly due to the graphite lubrication performance and increase the stiffness of the rubber contact area. At low content of graphite, adhesive wear of NBR is showed, in the high content of graphite, abrasive wear is showed. Water lubrication condition, wear surface level off, the wear loss is very small, and the lubrication and cooling effect of water makes the friction coefficient decrease. Graphite content is higher, the wear loss and coefficient of friction is smaller.


2014 ◽  
Vol 619 ◽  
pp. 13-17 ◽  
Author(s):  
Alain Kusmoko ◽  
Druce P. Dunne ◽  
Hui Jun Li

Stellite 6 was deposited by laser cladding on an austenitic stainless steel substrate (ASS) with energy inputs of 1 kW (ASS 1) and 1.8 kW (ASS 1.8). The chemical compositions and microstructures of these coatings were characterized by atomic absorption spectroscopy, optical microscopy and scanning electron microscopy. The microhardness of the coatings was measured and the wear mechanism of the coatings was assessed using a pin-on-plate (reciprocating) wear testing machine. The results showed less cracking and pore development for Stellite 6 coatings applied to the austenitic stainless steel substrate with the lower heat input (ASS 1). Further, the Stellite coating for ASS 1 was significantly harder than that obtained for ASS 1.8. The wear test results showed that the weight loss for ASS 1 was much lower than for ASS 1.8. It is concluded that the lower hardness of the coating for ASS 1.8, together with the softer underlying substrate structure, markedly reduced the wear resistance of the Stellite 6 coating.


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