Study on Water-Based Paint Stripper for Tinplate

2013 ◽  
Vol 690-693 ◽  
pp. 2071-2075
Author(s):  
Ning Duan ◽  
Yao Wen Gao ◽  
Teng Zhang ◽  
Ke Ming Wu ◽  
Yin Feng Zhang
Keyword(s):  
Electron Microscopy ◽  
Mass Fraction ◽  
Steel Surface ◽  
Ammonium Bromide ◽  
Distilled Water ◽  
Water Based ◽  
Corrosive Effect ◽  
Stripping Efficiency ◽  
Sem Test ◽  
Scanning Electron

A novel water-based paint stripper was prepared for white, metallic ink and varnish coated on the tinplate steel surface. The effect of accelerator and surfactant on stripping efficiency was investigated with the types and dosage of the accelerator and surfactant, the stripping temperature and stirring up condition. The highest stripping efficiency was achieved with the stripper composited by (mass fraction) 35% benzyl alcohol, 6% propanediol carbonate, 10% formic acid, 2% cetyl tri-methyl ammonium bromide (CTMAB) and 47% distilled water, respectively. This paint stripper had low volatility, and was not easy to burn. Scanning electron microscopy (SEM) test indicated that the paint stripper had little corrosive effect on tinplates.

Scanning Electron Microscopy-cuticular Lesions on the Roundworm Ascaris Suum

1970 ◽  
Vol 28 ◽  
pp. 114-115
Author(s):  
P. A. Madden ◽  
W. R. Anderson
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Freeze Drying ◽  
Room Temperature ◽  
Secondary Electron ◽  
Distilled Water ◽  
Freeze Dried ◽  
Silver Paint ◽  
To Come ◽  
Scanning Electron

The intestinal roundworm of swine is pinkish in color and about the diameter of a lead pencil. Adult worms, taken from parasitized swine, frequently were observed with macroscopic lesions on their cuticule. Those possessing such lesions were rinsed in distilled water, and cylindrical segments of the affected areas were removed. Some of the segments were fixed in buffered formalin before freeze-drying; others were freeze-dried immediately. Initially, specimens were quenched in liquid freon followed by immersion in liquid nitrogen. They were then placed in ampuoles in a freezer at −45C and sublimated by vacuum until dry. After the specimens appeared dry, the freezer was allowed to come to room temperature slowly while the vacuum was maintained. The dried specimens were attached to metal pegs with conductive silver paint and placed in a vacuum evaporator on a rotating tilting stage. They were then coated by evaporating an alloy of 20% palladium and 80% gold to a thickness of approximately 300 A°. The specimens were examined by secondary electron emmission in a scanning electron microscope.

scholarly journals SEM, EDS and Electrical Capacitance Study on Electrodeposited Ni-Cu Layers

2019 ◽  
Vol 70 (9) ◽  
pp. 3210-3212
Author(s):  
Oana Claudia Ciobotea Barbu ◽  
Ioana Alina Ciobotaru ◽  
Anca Cojocaru ◽  
Florin Mihai Benga ◽  
Danut Ionel Vaireanu
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Chemical Composition ◽  
Electrochemical Method ◽  
Steel Substrate ◽  
Distilled Water ◽  
Electrical Capacitance ◽  
Nickel Copper ◽  
Scanning Electron

Nickel-Copper metallic layers were deposited onto a steel substrate by using the electrochemical method. The morphology and the chemical composition of the deposited layers were studied by scanning electron microscopy. The electrical capacitance was measured on a functional supercapacitor made of two Ni-Cu deposited layers and a Nafion 117� membrane hydrated with distilled water, which served as a dielectric separator.

Ultrastructure of the Tertiary Envelope of the Cyst of the Tadpole Shrimp Triops longicaudatus (Branchiopoda; Notostraca)

2000 ◽  
Vol 6 (S2) ◽  
pp. 872-873
Author(s):  
James R. Rosowski ◽  
Terry L. Bartels ◽  
James F. Colburn ◽  
Jannell L. Colton ◽  
Denton Belk ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Fairy Shrimp ◽  
Distilled Water ◽  
Thin Sections ◽  
Rainfall Events ◽  
Transmission Electron ◽  
Tadpole Shrimp ◽  
Species Specific ◽  
Scanning Electron

Tadpole shrimp inhabit temporary freshwater pools and ponds where their occurrence is largely regulated by rainfall events and water temperature. When dry basins are flooded, cysts of Triops imbibe water and hatch to produce rapidly growing, carapaced larvae. While previous studies show anostracan (fairy shrimp) cyst-surface morphology often species specific, few studies illustrate shell ultrastructure of Triops and none has considered T. longicaudatus. Here we examine the shell of T. longicaudatus (Notostraca) and compare its fine structure to other species of Triops and to that of Artemiafranciscana(Anostraca), which we previously studied.Cysts, produced in culture from Utah broodstock, were purchased from Triops, Inc., 1924 Creighton Rd., Pensacola, FL 32504. Thin sections of cysts were prepared for transmission electron microscopy (TEM) as previously described (Fig. 1). Cysts were also examined with scanning electron microscopy (SEM), dry, whole or fractured (Figs. 2,3), or after imbibition and/or hatching in oxygen saturated, double-distilled water, at 25 ° C.

scholarly journals Effect of Intermediate Flush Using Different Devices to Prevent Chemical Smear Layer Formation

2017 ◽  
Vol 28 (4) ◽  
pp. 447-452
Author(s):  
Camilla Corrêa Silva ◽  
Vivian Maria Durange Ferreira ◽  
Gustavo De-Deus ◽  
Daniel Rodrigo Herrera ◽  
Maíra do Prado ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Root Canal ◽  
Smear Layer ◽  
Distilled Water ◽  
Layer Formation ◽  
Rank Tests ◽  
Signed Rank ◽  
Chlorhexidine Solution ◽  
Conventional Irrigation ◽  
Scanning Electron

Abstract This study compared the effect of intermediate flush with distilled water delivered by conventional irrigation, EndoVac microcannula or Self-Adjusting File (SAF) system in the prevention of chemical smear layer (CSL) formation. Thirty human premolars were used. Canals were prepared with Reciproc system and 5.25% NaOCl. After chemomechanical preparation, samples were divided in 3 groups (n=10) according to the intermediate irrigation protocol with distilled water using: conventional irrigation, EndoVac microcannula or SAF. A final flush with 2% chlorhexidine solution was used and scanning electron microscopy was performed to assess protocol effectiveness. Two calibrated evaluators attributed scores according the presence or absence of CSL on the surface of the root canal walls at the coronal, middle and apical thirds, as follows: (1) no CSL; (2) small amounts of CSL; (3) moderate CSL; and (4) heavy CSL. Differences between protocols were analyzed with Kruskal-Wallis and Mann-Whitney U tests. Friedman and Wilcoxon signed rank tests were used for comparison between each root canal third. SAF resulted in less formation of CSL when compared with the conventional irrigation and EndoVac microcannula (p<0.05). When root canal thirds were analyzed, conventional irrigation and EndoVac groups showed less CSL formation at coronal and middle thirds in comparison to the apical third (p<0.05). In SAF group, there was no difference among the thirds (p>0.05). It may be concluded that an intermediate flush of distilled water, delivered by the SAF system resulted in a better reduction of CSL formation during chemomechanical preparation.

The Effect of Different Silica Compositions to the Properties of Silica Foam Fabricated Using Slurry Method

2017 ◽  
Vol 888 ◽  
pp. 121-125 ◽  
Author(s):  
Syazwani Baharom ◽  
Sufizar Ahmad ◽  
Muhamad Izranuddin Mohd Ramli
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Compressive Strength ◽  
Polyethylene Glycol ◽  
Morphological Analysis ◽  
Strength Test ◽  
Distilled Water ◽  
Compressive Strength Test ◽  
Slurry Method ◽  
Scanning Electron

Silica foams with 50% – 70% porosity have been developed by mixing silica powder, polyethylene glycol (PEG) and carboxymethyl cellulose (CMC) into distilled water to make slurry. Polyurethane foam (PU) as the template is immersed into the slurry with 45 wt.%, 50 wt.% and 55 wt.%. of silica composition and finally sintered at 1100°C, 1200°C, 1300°C and 1400°C. Several tests which are morphological analysis, porosity and density test, and compressive strength test are compulsory to determine the physical and mechanical of the silica foam. The morphology of the foam has been observed using Scanning Electron Microscopy (SEM) and the result of pore size distribution is in the range of 255.91 μm to 489.14 μm. The porosity and density obtained from the porosity and density test was 50%-73.66% and 0.5499 g/cm³ up to 0.9757 g/cm³, respectively. Meanwhile, the compressive strength of sintered silica foam obtained is 0.01471 N/mm² up to 0.1467 N/mm².

scholarly journals Synthesis and thermal conductivity of functionalized biocarbon-Fe3O4 nanocomposite-based green nanofluid for heat transfer applications

2021 ◽  
Vol 321 ◽  
pp. 01003
Author(s):  
Divya Barai ◽  
Sohan Parbat ◽  
Bharat Bhanvase
Keyword(s):  
Heat Transfer ◽  
Electron Microscopy ◽  
Thermal Conductivity ◽  
Nanocomposite Particles ◽  
X Ray ◽  
Conductivity Enhancement ◽  
Water Based ◽  
One Step ◽  
Ultrasound Assisted ◽  
Scanning Electron

Bio-based graphitic carbon was synthesized in this work by one-step carbonization of bamboo waste at low temperature. This bio-based carbon was then functionalized in order to decorated it with Fe3O4 nanoparticles. The functionalized biocarbon-Fe3O4 (f-biocarbon-Fe3O4) nanocomposite was synthesized using ultrasound-assisted coprecipitation method which was then confirmed by scanning electron microscopy, Fourier transform infrared spectroscopy, and X-ray diffractometry. Water-based nanofluid was prepared using the synthesized f-biocarbon-Fe3O4 nanocomposite particles. Thermal conductivity of this nanofluid was analyzed at different concentrations and temperatures. A thermal conductivity enhancement of almost 80% was recorded at 35°C for nanofluid containing 0.1 vol.% of f-biocarbon-Fe3O4 nanocomposite particles compared to water. Also, empirical model is developed for prediction of thermal conductivity as a function of concentration and temperature of bamboo waste-derived f-biocarbon-Fe3O4 nanocomposite-based green nanofluid.

scholarly journals Improvement of Mechanical and Rheological Properties of Natural Rubber for Anti-Vibration Applications

2017 ◽  
Vol 13 (2) ◽  
Author(s):  
Nabel K. Abd Ali ◽  
Malia. M. Farhan ◽  
Abbas S . Moosa
Keyword(s):  
Electron Microscopy ◽  
Natural Rubber ◽  
Mechanical Tests ◽  
Friction Resistance ◽  
Synthetic Rubber ◽  
Structure Morphology ◽  
Rheological Test ◽  
Sem Test ◽  
Master Batch ◽  
Scanning Electron

Abstract   This research aims to study and improve the passivating specifications of rubber resistant to  vibration. In this paper, seven different rubber recipes were prepared based on mixtures of natural rubber(NR)  as an essential part in addition to the synthetic rubber (IIR, BRcis, SBR, CR)with different rates. Mechanical tests such as tensile strength, hardness, friction, resistance to compression, fatigue and creep testing in addition to the rheological test were performed. Furthermore, scanning electron microscopy (SEM)test was used to examine the structure morphology of rubber. After studying and analyzing the results, we found that, recipe containing (BRcis) of 40% from the natural rubber has the best mechanical and physical specifications to be used in applications that require the presence of rubber, resistant to vibration. Keywords: Ant vibration behavior , Natural rubber, Synthetic rubber, master batch.

scholarly journals Study of Corrosion Behavior of N’-(2-(2-oxomethylpyrrol-1-yl)ethyl)piperidine for Mild Steel in the Acid Environment

2021 ◽  
Vol 12 (3) ◽  
pp. 3638-3646
Keyword(s):  
Electron Microscopy ◽  
Mild Steel ◽  
Steel Surface ◽  
Inhibition Efficiency ◽  
Protective Layer ◽  
Solution Temperature ◽  
Inhibitor Concentration ◽  
Acid Environment ◽  
Experimental Findings ◽  
Scanning Electron

The corrosion inhibition of mild steel in 1 M hydrochloric acid solution by N'-(2-(2-oxomethylpyrrol-1-yl)ethyl)piperidine (N-OPEP) was studied employing weight loss techniques. The experimental findings revealed that N-OPEP is the most excellent corrosion inhibitor, and the inhibitory performance increases with an increase in the inhibitor concentration. Furthermore, the inhibition efficiency decreases with an increase in the solution Temperature. The adsorption of inhibitor molecules on a mild steel surface followed Langmuir’s isotherm model and was found to be spontaneous. Scanning electron microscopy (SEM) photographs approved the formation of a protective layer of the inhibitor molecules on the surface of mild steel.

Fluid Performance Study for Groove Grinding a Nickel-Based Superalloy Using Electroplated Cubic Boron Nitride (CBN) Grinding Wheels

2004 ◽  
Vol 126 (3) ◽  
pp. 451-458 ◽  
Author(s):  
Frank C. Gift, ◽  
Wojciech Z. Misiolek
Keyword(s):  
Electron Microscopy ◽  
Cubic Boron Nitride ◽  
Metal Deposition ◽  
Process Conditions ◽  
Performance Study ◽  
Grinding Wheels ◽  
Nickel Based Superalloy ◽  
Satisfactory Performance ◽  
Water Based ◽  
Scanning Electron

The performance of three water-based grinding fluids was analyzed and compared to a neat oil tested under the same process conditions. Light optical and scanning electron microscopy observations show the mechanism of metal deposition that leads to CBN wheel failure for water-based fluids. To improve the performance of the water-based fluids, a new nozzle layout is proposed that would prevent metal deposition on the CBN wheels. The proposed solution is not chemical, but mechanical in nature and the presented setting should be optimized in the future to assure satisfactory performance of the CBN wheels with water-based fluids.

Phosphoric Acid Rate Addition Effect in the Hydroxyapatite Synthesis by Neutralization Method

2006 ◽  
Vol 530-531 ◽  
pp. 593-598 ◽  
Author(s):  
D.S. Gouveia ◽  
Ana Helena A. Bressiani ◽  
José Carlos Bressiani
Keyword(s):  
Electron Microscopy ◽  
Heating Rate ◽  
Calcium Phosphates ◽  
Molar Ratio ◽  
Infrared Spectrometry ◽  
Distilled Water ◽  
X Ray Diffraction ◽  
Vacuum Filtration ◽  
X Ray ◽  
Scanning Electron

Calcium phosphates with different Ca/P molar ratio can be obtained depending the precipitation conditions such as pH and temperature. In this work the effect of the pH’s variation during the H3PO4 addition in the synthesis of hydroxyapatite-HA, (Ca/P molar ratio 1.67) by neutralization method, was studied. The H3PO4 addition’s rate was 1.0, 1.5, 8.0 mL.min-1 and in other experiment the H3PO4 was added at a time. After the addition was completed the pH ranged from 7-12. The suspensions were kept during 24 hours for ripening. The precipitate was separated from the suspension by vacuum filtration, washed with distilled water and dried at 70°C/24h. Afterwards the materials were analyzed by thermogravimetric analysis (TGA) with heating rate of 10°C/min in air. The calcination of the powders was accomplished at 800°C/3h with heating rate of 10°C.min-1. The powders were characterized by X-ray diffraction (XRD), infrared spectrometry (FTIR), specific surface area (BET), and scanning electron microscopy (SEM). The results indicated that the ratio of addition of the acid can influence both the morphology and the formation of the phases (HA and TCP) in the obtained powders.

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