Microstructural Study of Copper and Copper/Alumina Composite Coatings Produced by Cold Spray Process

2010 ◽  
Vol 89-91 ◽  
pp. 556-561 ◽  
Author(s):  
Dimitris Pantelis ◽  
Kostoula Triantou ◽  
Charikleia Sarafoglou ◽  
Dimitris Christoulis ◽  
Francois Borit ◽  
...  
Keyword(s):  
Cross Sections ◽  
Composite Coatings ◽  
Cold Spraying ◽  
Xrd Analysis ◽  
Al2o3 Particle ◽  
Copper Particles ◽  
Spray Process ◽  
Coating Method ◽  
Alumina Composite ◽  
The Cross

Cold spraying is a novel coating method, by which many composites have been successfully sprayed. The objective of this study was to thoroughly characterize the microstructure of copper as well as copper/alumina composite coatings obtained using this technique. Composite coatings which differed to the percentage of Al2O3 in the initial powder blend as well as the Al2O3 particle size were studied. Coatings presented Ra of the order of 6-8 μm, with the copper coating having the highest value. Using optical microscopy the deformation of the copper particles of the cross sections was evident. Thickness ranged from 170 to 450 μm for the different coatings. The surfaces and the cross sections of the coatings were studied by means of scanning electron microscopy. Craters and Al2O3 particles that were embedded in the copper particles were observed. The XRD analysis of the powders and the respective coatings presented no differences.

scholarly journals Microstructure, Microhardness, Fracture Toughness, and Abrasive Wear of In-Situ Synthesized TiC/Ti-Al Composite Coatings by Cold Spraying Combined with Heat Treatment

Coatings ◽  
2021 ◽  
Vol 11 (9) ◽  
pp. 1034 ◽  
Author(s):  
Xiao Chen ◽  
Chengdi Li ◽  
Xiaobo Bai ◽  
Hao Liu ◽  
Shunjian Xu ◽  
...  
Keyword(s):  
Fracture Toughness ◽  
Intermetallic Compounds ◽  
Composite Coatings ◽  
Cold Spraying ◽  
Xrd Analysis ◽  
Gas Temperature ◽  
Al Composite ◽  
Average Porosity ◽  
Annealed Coating

TiAl intermetallic compounds, as a new kind of high-performance light-weight structural material, are widely applied in many fields. Titanium carbide (TiC) as the reinforcing phase could improve the mechanical properties, wear resistance, and heat-resistance stability of TiAl intermetallic compounds. Ti(Al, C) mixture powders were deposited by cold spraying at gas temperature of 250 °C, 450 °C, and 550 °C. Then, Ti(Al, C) coatings were annealed at temperatures of 650 °C for different times and following holding at 1100 °C for 3 h. The microstructure, microhardness, fracture toughness, and abrasive wear of Ti-Al composite coatings were investigated. The research results were that the particle size of mixture powders decreased as the ball milling time prolonging. Ti(Al) solid solution appeared in the mixture powders as the milling time increased to 30 h. The average porosity of the coating sprayed at 550 °C was the lowest (0.85%). The as-sprayed coatings exhibited the same phase compositions with the mixture powders. The coating sprayed at gas temperature of 550 °C has the highest microhardness and the lowest weight loss. Ti-Al intermetallic was in-situ synthesized after annealing at 650 °C. The average porosity of the annealed coating (sprayed at 450 °C) was the lowest. The content of Ti-Al intermetallic compounds of the annealed coating sprayed at 450 °C is the highest. The X-ray diffraction (XRD) analysis results are consistent with the EDS analysis of the annealed coatings after annealing at 650 °C. Ti-Al intermetallic compounds were almost completely formed in the three kinds of the coatings after annealing at 650 °C for 20 h and following holding at 1100 °C for 3 h. TiAl and TiAl3 intermetallic phases were in-situ synthesized in the coatings based on the energy dispersive spectroscopy (EDS) and XRD analysis. TiC was also in situ synthesized in the coatings as the annealing temperature increased to 1100 °C. The annealed coating (sprayed at 450 °C) has the highest microhardness, fracture toughness, and wear resistance properties after annealing at 1100 °C for 3 h.

Mechanical Properties of Alumina Composite Hardened by Ultra Dispersed Diamonds

2002 ◽  
Author(s):  
Maksim Kireitseu ◽  
L. Yerakhavets ◽  
Ion Nemerenco
Keyword(s):  
Mechanical Properties ◽  
Spectral Analysis ◽  
Composite Coatings ◽  
Xrd Analysis ◽  
Hertzian Contact ◽  
Load Rating ◽  
X Ray ◽  
Variable Porosity ◽  
Alumina Composite

Structure and mechanical properties of composite coatings that contain of 5 to 25% (vol.) of ultra-dispersed diamonds, different alumina phases, and components of SiC, AlN have been investigated. Structure, grains morphology, presence of pores and their distribution, interaction zones were investigated with SEM, X-ray-phase analysis and micro-X-ray-spectral analysis. Material was formed by impulse pressing. It is revealed that the material has variable-porosity, high density, microhardness up to 25 GPa and load rating. XRD analysis shows that the structure includes the diamond phase. To investigate load rating of the material Hertzian contact was used. Ultra-dispersed diamonds strength the structure in general as well as mechanical properties and quality of composite coatings.

scholarly journals Optimization of ceramic content in nickel–alumina composite coatings obtained by low pressure cold spraying

2021 ◽  
Vol 405 ◽  
pp. 126732
Author(s):  
M. Winnicki ◽  
S. Kozerski ◽  
A. Małachowska ◽  
L. Pawłowski ◽  
M. Rutkowska-Gorczyca
Keyword(s):  
Composite Coatings ◽  
Cold Spraying ◽  
Low Pressure ◽  
Alumina Composite

The cross sections for different channels in heavy ion nuclear reactions

1971 ◽  
Vol 32 (1) ◽  
pp. 7-9 ◽  
Author(s):  
J. Galin ◽  
D. Guerreau ◽  
M. Lefort ◽  
X. Tarrago
Keyword(s):  
Cross Sections ◽  
Nuclear Reactions ◽  
Heavy Ion ◽  
The Cross

Experimental Studies Of Multilayer Glass Structures On Compression, Compression With Bending And Simple Bending

2019 ◽  
pp. 22-30
Keyword(s):  
Cross Section ◽  
Cross Sections ◽  
Applied Load ◽  
Experimental Studies ◽  
Strength Properties ◽  
Research Topic ◽  
Normative Values ◽  
Laminated Glass ◽  
The Cross ◽  
Experimental Values

The work of multilayer glass structures for central and eccentric compression and bending are considered. The substantiation of the chosen research topic is made. The description and features of laminated glass for the structures investigated, their characteristics are presented. The analysis of the results obtained when testing for compression, compression with bending, simple bending of models of columns, beams, samples of laminated glass was made. Overview of the types and nature of destruction of the models are presented, diagrams of material operation are constructed, average values of the resistance of the cross-sections of samples are obtained, the table of destructive loads is generated. The need for development of a set of rules and guidelines for the design of glass structures, including laminated glass, for bearing elements, as well as standards for testing, rules for assessing the strength, stiffness, crack resistance and methods for determining the strength of control samples is emphasized. It is established that the strength properties of glass depend on the type of applied load and vary widely, and significantly lower than the corresponding normative values of the strength of heat-strengthened glass. The effect of the connecting polymeric material and manufacturing technology of laminated glass on the strength of the structure is also shown. The experimental values of the elastic modulus are different in different directions of the cross section and in the direction perpendicular to the glass layers are two times less than along the glass layers.

scholarly journals The Influence of Aluminum Content on Oxidation Resistance of New-Generation ODS Alloy at 1200 °C

Metals ◽  
2020 ◽  
Vol 10 (11) ◽  
pp. 1478 ◽  
Author(s):  
Luděk Stratil ◽  
Vít Horník ◽  
Petr Dymáček ◽  
Pavla Roupcová ◽  
Jiří Svoboda
Keyword(s):  
Oxidation Resistance ◽  
Cross Sections ◽  
Aluminum Content ◽  
Energy Dispersive Spectrometer ◽  
Oxide Dispersion Strengthened ◽  
Xrd Analysis ◽  
Al Content ◽  
Α Al2o3 ◽  
New Generation ◽  
Ods Alloy

The aim of the paper is to evaluate the effect of aluminum content on the oxidation resistance of new-generation of oxide dispersion strengthened (ODS) alloy at 1200 °C. Three grades of the alloy of chemical composition Fe-15Cr-xAl-4Y2O3 with different Al contents x = 0.3 wt.%, 2.0 wt.% and 5.5 wt.% are prepared by mechanical alloying. The alloys are consolidated by high temperature rolling followed by heat treatment. To study the oxidation resistance the samples are isothermally aged in the air for 1 h, 4 h, 16 h and 64 h at 1200 °C. The oxidation kinetics, composition and formation mechanism of the oxide layers are analyzed. The weight gain of prepared steels is estimated. The kinetics of oxidation is studied on metallographic cross-sections of the exposed samples by scanning electron microscopy (SEM) and energy dispersive spectrometer (EDS) analysis. The oxides on the surfaces are identified by X‑ray diffraction (XRD) analysis. The Al content significantly enhances the oxidation resistance of the alloy. For a sufficiently high Al content in the alloy a compact oxide layer of α‑Al2O3 on the surface is formed, which significantly suppresses further oxidation process.

scholarly journals Total cross sections of eγ → $$ eX\overline{X} $$ processes with X = μ, γ, e via multiloop methods

2021 ◽  
Vol 2021 (1) ◽  
Author(s):  
Roman N. Lee ◽  
Alexey A. Lyubyakin ◽  
Vyacheslav A. Stotsky
Keyword(s):  
Cross Section ◽  
Cross Sections ◽  
Elliptic Integral ◽  
High Energy ◽  
Calculation Methods ◽  
Complete Elliptic Integral ◽  
Total Cross Sections ◽  
Multiloop Calculation ◽  
The Cross ◽  
Analytical Expressions

Abstract Using modern multiloop calculation methods, we derive the analytical expressions for the total cross sections of the processes e−γ →$$ {e}^{-}X\overline{X} $$ e − X X ¯ with X = μ, γ or e at arbitrary energies. For the first two processes our results are expressed via classical polylogarithms. The cross section of e−γ → e−e−e+ is represented as a one-fold integral of complete elliptic integral K and logarithms. Using our results, we calculate the threshold and high-energy asymptotics and compare them with available results.

scholarly journals Asymptotic Behavior of Stable Structures Made of Beams

2021 ◽  
Author(s):  
Georges Griso ◽  
Larysa Khilkova ◽  
Julia Orlik ◽  
Olena Sivak
Keyword(s):  
Asymptotic Behavior ◽  
Cross Section ◽  
Cross Sections ◽  
Linear Elasticity ◽  
Circular Cross Section ◽  
Linear Elasticity Theory ◽  
Linear Elastic ◽  
The Cross ◽  
Small Rotation ◽  
Stable Structures

AbstractIn this paper, we study the asymptotic behavior of an $\varepsilon $ ε -periodic 3D stable structure made of beams of circular cross-section of radius $r$ r when the periodicity parameter $\varepsilon $ ε and the ratio ${r/\varepsilon }$ r / ε simultaneously tend to 0. The analysis is performed within the frame of linear elasticity theory and it is based on the known decomposition of the beam displacements into a beam centerline displacement, a small rotation of the cross-sections and a warping (the deformation of the cross-sections). This decomposition allows to obtain Korn type inequalities. We introduce two unfolding operators, one for the homogenization of the set of beam centerlines and another for the dimension reduction of the beams. The limit homogenized problem is still a linear elastic, second order PDE.

Preparation and properties of polyurethane coatings modified by polysilazane

2019 ◽  
Vol 32 (6) ◽  
pp. 611-619 ◽  
Author(s):  
Xiaoli Liu ◽  
Zhen Ge ◽  
Wenguo Zhang ◽  
Yunjun Luo
Keyword(s):  
Mechanical Property ◽  
Photoelectron Spectroscopy ◽  
Composite Coatings ◽  
Composite Films ◽  
Dip Coating ◽  
Water Contact ◽  
Research Attention ◽  
Elongation At Break ◽  
Coating Method ◽  
Dip Coating Method

Due to their unique physicochemical properties, polysilazanes exhibit excellent performance when combined with some resin matrixes, which had drawn great research attention. In this article, polyurethane (PU) was firstly prepared by polytetrahydrofuran glycol, isophorone diisocyanate, and 1,4-butanediol as main materials. Then, the prepared PU was blended with polysilazane by mixing the two solutions together, which was cured to films via dip-coating method at room temperature. The structure, thermal stability, and surface properties of the composite coatings were investigated by Fourier-transform infrared spectroscopy, thermogravimetric analysis, scanning electron microscopy, and X-ray photoelectron spectroscopy. The results demonstrated that after modification with polysilazane, the heat resistance, hydrophobicity, and mechanical property of the PU coatings were improved. When the content of polysilazane was 6 wt%, the mechanical property of the composite films was optimized, with a maximum tensile strength of 25.7 MPa and elongation at break of 797%. Meanwhile, the water contact angle of the composite film was 107° and the water absorption reached a minimum of 2.1%, which showed improved hydrophobicity and water resistance.

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