New Photothermal Deflection Method to Determine Thermal Properties of Bulk Semiconductors

2010 ◽  
Vol 297-301 ◽  
pp. 525-530
Author(s):  
Imen Gaied ◽  
Salima Lassoued ◽  
Fredéric Genty ◽  
Noureddine Yacoubi
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Thermal Diffusivity ◽  
Modulation Frequency ◽  
Phase Variation ◽  
Sample Surface ◽  
Halogen Lamp ◽  
Bulk Semiconductors ◽  
Photothermal Deflection ◽  
Modulated Light

In this paper, we present a new Photothermal Deflection Technique (PTD) to determine thermal properties of bulk doped or undoped semiconductor such as GaAs, GaSb, InAs, etc. The method proposed here consists in covering the sample with a thin graphite layer in order to increase the photothermal signal and to ovoid any reflection on the sample surface. This method deals with the analysis of the logarithm of amplitude and phase variation of the photothermal signal versus square root modulation frequency where the sample placed in air is heated by a modulated light beam coming from a halogen lamp. So the best coincidence between experimental curves and corresponding theoretical ones gives simultaneously the best values of thermal conductivity and thermal diffusivity of the sample. These obtained values are in good agreement with those found in literature. The advantage of applying this method in this way lies in its simplicity and its sensibility to both thermal conductivity and thermal diffusivity.

Investigation of Thermal Properties of Thin Semiconductor Layers Deposited on a Glass Substrate by the Photothermal Deflection Technique

2010 ◽  
Vol 297-301 ◽  
pp. 537-542
Author(s):  
Imen Gaied ◽  
Mohamed Ben Rabeh ◽  
Adel Rabhi ◽  
Mounir Kanzari ◽  
Noureddine Yacoubi
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Glass Substrate ◽  
Modulation Frequency ◽  
Halogen Lamp ◽  
Square Root ◽  
Thin Semiconductor ◽  
Phase Variations ◽  
Photothermal Deflection

In this work we describe a method based on the Photothermal Deflection Technique adapted for the determination of thermal properties of thin semiconductor layers deposited on a glass substrate. The sample placed in air is heated thanks a modulated pump uniform beam coming from a halogen lamp. The thermal conductivity and the thermal diffusivity are obtained by comparing the amplitude and phase variations versus square root modulation frequency between the experimental curves and the corresponding theoretical ones. The best coincidence permits to deduce the thermal properties of the sample.

scholarly journals Improvement of the Thermal Properties of Sorel Cements

2020 ◽  
Author(s):  
Rim Zgueb ◽  
Amal Brichni ◽  
Noureddine Yacoubi
Keyword(s):  
Thermal Conductivity ◽  
Compressive Strength ◽  
Thermal Properties ◽  
Thermal Diffusivity ◽  
Thermal Insulation ◽  
Building Material ◽  
Polyvinyl Acetate ◽  
Cement Matrix ◽  
Photothermal Deflection

Sorel cements is a promising building material for insulation applications. Indeed, the effect of polyvinyl acetate polymer on cements has been investigated. The polyvinyl acetate polymer was added to the cement matrix with a percentage of 0, 5, 10, 15 and 20% by weight of Sorel cement. The thermal properties of Sorel cement were determined by photothermal deflection technique. Thermal properties such as thermal conductivity and thermal diffusivity are measured by coincidentally the experimental curves of the photothermal signal with the best corresponding theoretical curves. The results revealed that the incorporation of polyvinyl acetate polymer enhance the thermal insulation and reduce the compressive strength of Sorel cement.

Thermal Characterization of Carbon-Carbon Composites

2011 ◽  
Author(s):  
Messiha Saad ◽  
Darryl Baker ◽  
Rhys Reaves
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Thermal Diffusivity ◽  
Specific Heat ◽  
Critical Role ◽  
Carbon Composite ◽  
Flash Method ◽  
Carbon Composites ◽  
Energy Storage Devices ◽  
Graphitized Carbon

Thermal properties of materials such as specific heat, thermal diffusivity, and thermal conductivity are very important in the engineering design process and analysis of aerospace vehicles as well as space systems. These properties are also important in power generation, transportation, and energy storage devices including fuel cells and solar cells. Thermal conductivity plays a critical role in the performance of materials in high temperature applications. Thermal conductivity is the property that determines the working temperature levels of the material, and it is an important parameter in problems involving heat transfer and thermal structures. The objective of this research is to develop thermal properties data base for carbon-carbon and graphitized carbon-carbon composite materials. The carbon-carbon composites tested were produced by the Resin Transfer Molding (RTM) process using T300 2-D carbon fabric and Primaset PT-30 cyanate ester. The graphitized carbon-carbon composite was heat treated to 2500°C. The flash method was used to measure the thermal diffusivity of the materials; this method is based on America Society for Testing and Materials, ASTM E1461 standard. In addition, the differential scanning calorimeter was used in accordance with the ASTM E1269 standard to determine the specific heat. The thermal conductivity was determined using the measured values of their thermal diffusivity, specific heat, and the density of the materials.

Experimental Study on Thermal Properties of Hollow Sphere Structures

2021 ◽  
Vol 407 ◽  
pp. 185-191
Author(s):  
Josef Tomas ◽  
Andreas Öchsner ◽  
Markus Merkel
Keyword(s):  
Thermal Conductivity ◽  
Experimental Study ◽  
Thermal Properties ◽  
Thermal Diffusivity ◽  
Specific Heat ◽  
Hollow Sphere ◽  
Plane Source ◽  
Source Method ◽  
Transient Plane Source ◽  
Transient Plane Source Method

Experimental analyses are performed to determine thermal conductivity, thermal diffusivity and volumetric specific heat with transient plane source method on hollow sphere structures. Single-sided testing is used on different samples and different surfaces. Results dependency on the surface is observed.

scholarly journals Application of sonication and freezing as initial treatments before microwave-vacuum drying of cranberries

2019 ◽  
Vol 2 (22) ◽  
pp. 151-167 ◽  
Author(s):  
Izabela Staniszewska ◽  
Szymon Staszyński ◽  
Magdalena Zielińska
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Thermal Diffusivity ◽  
Physical Properties ◽  
Color Change ◽  
Vacuum Drying ◽  
Drying Time ◽  
Dried Fruits ◽  
Microwave Vacuum Drying ◽  
Drying Kinetic

The aim of study was to determine the influence of sonication and freezing on the kinetic of the microwave-vacuum drying, energy consumption and physical properties of whole cranberries as well as evaluate the applicability of sonication instead of freezing in order to change their physical properties and the drying kinetic of whole cranberries. Microwave-vacuum drying of whole cranberries with/without initial treatments took from 12 ± 1 to 14.5 ± 0.5 minutes. All of treatments did not significantly shorten the drying time of cranberries. However, they increased SMER values even by 31%. Despite of cryogenic freezing, all of treatments significantly increased the values of Dew. Sonication combined with drying allowed to obtain dried berries characterized by the lowest cohesiveness (0.19±0.02), springiness (0.62±0.02) and chewiness (3.4±0.8 N), while cryogenic freezing combined with drying allowed to obtain dried fruits characterized by highest springiness (0.75±0.03) and low chewiness (3.3±0.5 N). The highest lightness (32.2±0.7), redness (32.6±0.8), and yellowness (11.1±0.7) were found for fruits subjected to initial convective freezing before drying. The efficiency of sonication in color change was comparable to cryogenic freezing and much lower than convective freezing. All of initial treatments increased such thermal properties of dried cranberries as thermal conductivity and thermal diffusivity.

Influence of Mesocarp Fibre Inclusion on Thermal Properties of Foamed Concrete

2021 ◽  
Vol 87 (1) ◽  
pp. 1-11
Author(s):  
Siti Shahirah Suhaili ◽  
Md Azree Othuman Mydin ◽  
Hanizam Awang
Keyword(s):  
Thermal Conductivity ◽  
Heat Capacity ◽  
Thermal Properties ◽  
Thermal Diffusivity ◽  
Specific Heat ◽  
Specific Heat Capacity ◽  
Volume Fraction ◽  
Thermal Constant ◽  
Volume Fractions ◽  
Foamed Concrete

The addition of mesocarp fibre as a bio-composite material in foamed concrete can be well used in building components to provide energy efficiency in the buildings if the fibre could also offer excellent thermal properties to the foamed concrete. It has practical significance as making it a suitable material for building that can reduce heat gain through the envelope into the building thus improved the internal thermal comfort. Hence, the aim of the present study is to investigate the influence of different volume fractions of mesocarp fibre on thermal properties of foamed concrete. The mesocarp fibre was prepared with 10, 20, 30, 40, 50 and 60% by volume fraction and then incorporated into the 600, 1200 and 1800 kg/m3 density of foamed concrete with constant cement-sand ratio of 1:1.5 and water-cement ratio of 0.45. Hot disk thermal constant analyser was used to attain the thermal conductivity, thermal diffusivity and specific heat capacity of foamed concrete of various volume fractions and densities. From the experimental results, it had shown that addition of mesocarp fibre of 10-40% by volume fraction resulting in low thermal conductivity and specific heat capacity and high the thermal diffusivity of foamed concrete with 600 and 1800 kg/m3 density compared to the control mix while the optimum amount of mesocarp fibre only limit up to 30% by volume fraction for 1200 kg/m3 density compared to control mix. The results demonstrated a very high correlation between thermal conductivity, thermal diffusivity and specific heat capacity which R2 value more than 90%.

Thermal Properties of Thin Metallic Layer Deposited on Insulators: Effect of the Interface on the Independent Determination of the Thermal Diffusivity and Conductivity of the Layer

2008 ◽  
Author(s):  
Danie`le Fournier ◽  
Jean Paul Roger ◽  
Christian Fretigny
Keyword(s):  
Thermal Conductivity ◽  
Thermal Properties ◽  
Thermal Diffusivity ◽  
Thermal Resistance ◽  
Thermal Contact ◽  
Heat Diffusion ◽  
Metallic Layer ◽  
Good Thermal Contact ◽  
Lateral Heat

Lateral heat diffusion thermoreflectance is a very powerful tool for determining directly the thermal diffusivity of layered structures. To do that, experimental data are fitted with the help of a heat diffusion model in which the ratio between the thermal conductivity k and the thermal diffusivity D of each layer is fixed, and the thermal properties of the substrate are known. We have shown in a previous work that it is possible to determine independently the thermal diffusivity and the thermal conductivity of a metallic layer deposited on an insulator, by taking into consideration all the data obtained at different modulation frequencies. Moreover, it is well known that to prevent a lack of adhesion of a gold film deposited on substrates like silica, an intermediate very thin (Cr or Ti) layer is deposited to assure a good thermal contact. We extend our previous work: the asymptotic behaviour determination of the surface temperature wave at large distances from the modulated point heat source for one layer deposited on the substrate to the two layers model. In this case (very thin adhesion coating whose thermal properties and thickness are known), it can be establish that the thermal diffusivity and the thermal conductivity of the top layer can still be determined independently. It is interesting to underline that the calculus can also be extended to the case of a thermal contact resistance which has often to be taken into account between two solids. We call thermal resistance a very thin layer exhibiting a very low thermal conductivity. In this case, the three parameters we have to determine are the thermal conductivity and the thermal diffusivity of the layer and the thermal resistance. We will show that, in this case, the thermal conductivity of the layer is always obtained independently of a bound of the couple thermal resistance – thermal diffusivity, the thermal diffusivity being under bounded and the thermal resistance lower bounded. Experimental results on thin gold layers deposited on silica with and without adhesion layers are presented to illustrate the method. Discussions on the accuracy will also be presented.

Thermal Properties of Tungsten SRM’S 730 and 799

1978 ◽  
Vol 100 (2) ◽  
pp. 330-333 ◽  
Author(s):  
R. E. Taylor
Keyword(s):  
Thermal Conductivity ◽  
Electrical Resistivity ◽  
Thermal Properties ◽  
High Temperature ◽  
Thermal Diffusivity ◽  
Thermophysical Properties ◽  
Room Temperature ◽  
Standard Material ◽  
International Program ◽  
Sintered Tungsten

Samples of sintered and arc-cast tungsten are available from NBS as thermal conductivity (SRM 730) and electrical resistivity (SRM 799) standards for the temperature range from 4 to 3000K. NBS recommended values for these properties above room temperature are based on results of various researchers during a previous international program which included arc-cast and sintered tungsten. The sintered tungsten used in this program was found to be unsuited for use as a standard material due to inhomogeneity and high temperature instability. The present paper gives results at high temperatures for thermal conductivity, electrical resistivity, specific heat, thermal diffusivity and Wiedemann-Franz-Lorenz ratio for a sample of the NBS sintered tungsten using the Properties Research Laboratory’s multiproperty apparatus. These results are compared to values recommended by the Thermophysical Properties Research Center, NBS, and an international program.

STUDY OF THERMAL TRANSPORT PARAMETERS IN PbI2 SINGLE CRYSTAL USING A PHOTOACOUSTIC TECHNIQUE

2006 ◽  
Vol 20 (20) ◽  
pp. 1253-1260 ◽  
Author(s):  
D. S. AHLAWAT ◽  
D. MOHAN ◽  
S. K. GHOSHAL ◽  
R. D. SINGH ◽  
MEENAKSHI SHARMA
Keyword(s):  
Thermal Conductivity ◽  
Thermal Diffusivity ◽  
Single Crystal ◽  
Characteristic Frequency ◽  
Modulation Frequency ◽  
Thermal Effusivity ◽  
Photoacoustic Signal ◽  
Photoacoustic Technique ◽  
Front Side ◽  
Transport Parameters

The present work discusses the study of the transport properties of the PbI 2 single crystal using an indigenously developed photoacoutistic spectrometer. The amplitude photoacoustic signal, being a function of the modulation frequency of the incident optical beam, has been measured by using the front-side detection configuration. The characteristic frequency (fc) of the single crystal has been found to be 55 Hz. The values of thermal diffusivity, thermal conductivity and thermal effusivity in the case of PbI 2 have been derived experimentally. Their values have been compared with the values reported in a case which studied other materials in the literature. Thermal diffusion lengths have also been calculated at different chopping frequencies from 15 Hz to 90 Hz.

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