Effect of Cu Particles Precipitation on Wear Behaviour of Fe-3mass%Cu under Dry Sliding Condition

2011 ◽  
Vol 462-463 ◽  
pp. 1224-1229 ◽  
Author(s):  
I. Agung ◽  
Junaidi Syarif ◽  
Mariyam Jameelah Ghazali ◽  
Z. Sajuri

Effect of peak-aged and over-aged Cu particles on wear behaviour of ferritic iron was investigated by means of Pin-on-Disc wear test under dry sliding condition. It was found that hardness of the peak-aged sample was higher than the over-aged sample. The specific wear rates of peak-aged samples were in the range of 0.20 × 10-4 to 0.89 × 10-4 mm3/(Nm) while the over-aged samples were in the range of 0.21 × 10-4 to 1.29 × 10-4 mm3/(Nm). Although both samples possessed moderate wear behaviours, the peak-aged samples had better wear resistance. Scanning Electron Microscopy observation found that most wear mechanism were due to plastic ploughing phenomenon. Transferred materials from the counterface tool was also proven by Energy Dispersive Spectroscopy test. However, the roughness test showed that the peak-aged sample surface was finer than the over-aged sample surface. Average roughness of peak-aged samples were in the range of 0.49 to 1.79 μm while the over-aged samples were in the range of 3.28 to 4.02 μm. Hence, it can be concluded that the peak-aged Cu particles can improve the wear resistance of steel.

Author(s):  
NAVEEN EASWARAN ◽  
Shanmugam Ramasamy ◽  
Roshan Nagarajan ◽  
Ramanan Nandagopal ◽  
Sripada Ragavendra Keshava Narasimha

Elemental powders of Atomized Iron (Fe), Carbon (C) and Molybdenum (Mo) were weighed and mixed in a pot mill to yield the composition of C45, C45-1%Mo and C45-2%Mo Steels, then compacted and sintered. The Sintered preforms had a density- 75% of the Theoretical Density. Then the Sintered preforms were subjected to densification to get two densities- 80% and 85% of the theoretical density through Forging. The sintered and densified preforms of alloy steels were subsequently machined to get the required wear test specimens.The experiments were conducted on a Pin-on-disc Tribometer, conforming to ASTM G99 standards, on a rotating EN32 disc. Using Minitab 16 software, the Dry Sliding wear experiments were planned using L27 Orthogonal Array.The % Theoretical Density of the Specimens (1-%Porosity), % Mo Addition, Load and Sliding Velocity were taken as input parameters, mass loss was the output parameter. It was observed that the increasing density of alloy steels adversely affects the wear resistance of the alloy steels and mass loss is increased. It was found that the addition of Mo significantly improves the wear resistance of the alloy steels irrespective of the densities .Empirical correlations for mass loss with respect to input parameters had been developed.


Author(s):  
Songbo Xu ◽  
Aydar Akchurin ◽  
Tian Liu ◽  
Weston Wood ◽  
X. W. Tangpong ◽  
...  

High density polyethylene (HDPE) is widely used as a bearing material in industrial application because of its low friction and high wear resistance properties. Carbon nanofiber (CNF) reinforced HDPE nanocomposites are promising materials for biomedical applications as well, such as being the bearing materials in total joint replacements. The main objective of the present study is to investigate how the wear of HDPE can be altered by the addition of either pristine or silane treated CNFs at different loading levels (0.5 wt. % and 3 wt. %). Two types of silane coating thicknesses, 2.8 nm and 46 nm, were applied on the surfaces of oxidized CNFs to improve the interfacial bonding strength between the CNFs and the matrix. The CNF/HDPE nanocomposites were prepared through melt mixing and hot-pressing. The coefficients of friction (COFs) and wear rates of the neat HDPE and CNF/HDPE nanocomposites were determined using a pin-on-disc tribometer under dry sliding conditions. The microstructures of the worn surfaces of the nanocomposites were characterized using both scanning electron microscope (SEM) and optical microscope to analyze their wear mechanisms. Compared with the neat HDPE, the COF of the nanocomposites were reduced. The nanocomposite reinforced with CNFs coated with the thicker silane coating (46 nm) at 0.5 wt. % loading level was found to yield the highest wear resistance with a wear rate reduction of nearly 68% compared to the neat HDPE.


2013 ◽  
Vol 2013 ◽  
pp. 1-8 ◽  
Author(s):  
P. Shanmughasundaram ◽  
R. Subramanian

Dry sliding wear behaviour of eutectic Al-Si alloy-graphite composites was investigated employing a pin-on-disc wear test rig. Results revealed that the wear and friction coefficients decreased linearly with increasing weight percentage of graphite particles. Wear resistance of the composite increased considerably with increasing sliding velocity at constant load. In contrast, the friction coefficient of Al-7.5 wt.% Gr composite increased when the sliding velocity was increased from 1 m/s to 2 m/s at 49 N. Worn-out surfaces of wear specimens after the test were examined by scanning electron microscopy to study the morphology of worn surfaces. EDS analysis was carried out to investigate the influence of mechanically mixed layer (MML) which comprises oxides and iron, and this acted as an effective tribolayer in enhancing the wear resistance at higher sliding velocity.


2014 ◽  
Vol 33 (3) ◽  
pp. 231-237 ◽  
Author(s):  
Dursun Özyürek ◽  
Tansel Tunçay ◽  
Hasan Kaya

AbstractIn this study, T5 heat treatment was applied to AA6063 alloy aged at 455 K for 2 hours after extrusion at 686 K. T6 heat treatment was also carried out by ageing at 455 K for 2 hours after solution heat treatment at 794 K for 1 hour. Heat treated T5 and T6 specimens were tested by pin-on-disc type wear equipment. Wear test was carried out by using 10, 20, 30 N loads and 400, 800, 1200 and 1600 m wear distance. T5 and T6 heat treated specimens were characterized with scanning electron microscope, X-ray diffraction (XRD), energy dispersive spectroscopy (EDS) and hardness measurements. Worn surfaces of the specimens was also characterised with SEM. The results indicated that small and homogenously dispersed Mg2Si precipitates formed in AA6063 aluminium alloy with T6 heat treatment were compared to the T5 heat treatment. As a result of increment precipitate size, wear resistance decreased. T6 heat treated specimens showed higher hardness compared to the T5 heat treated specimens. In addition wear resistance and friction coefficient of both T5 and T6 heat treated specimens decreased with increasing applied load.


2006 ◽  
Vol 317-318 ◽  
pp. 351-354
Author(s):  
Mark I. Jones ◽  
Kiyoshi Hirao ◽  
Hideki Hyuga ◽  
Yukihiko Yamauchi

The effects of microstructure and composition on the wear properties of Lu sialon ceramics have been studied under dry sliding conditions through block-on-ring wear tests. Microstructural and compositional effects on wear behaviour were studied by producing both equiaxed and elongated α sialons through the incorporation of additional oxides to promote extended liquid formation and grain growth, and by producing α / β composite materials with elongated β grains. The wear response of the materials is discussed in terms of the dominant wear mechanism under different experimental conditions. Under higher loads, where fracture dominates, materials with improved mechanical properties show better wear resistance and both the composite materials and the elongated α sialons showed lower wear rates than the equiaxed materials due to the elongated grain microstructures. Under low normal loads, fracture does not occur and the dominant wear mechanism is thought to be tribochemically assisted wear. Under these conditions, the equiaxed materials had better wear resistance than the composites, and the Lu-α sialon showed an order of magnitude lower wear rate than an equivalent Y-α sialon, thought to be due to better oxidation resistance and improved refractory nature afforded through the use of the smaller radius cation. The elongated Lu-α sialons under these low load conditions showed wear resistance that was to some extent dependent on the composition of the additional liquid phase, with high SiO2 contents leading to higher wear rates.


2015 ◽  
Vol 830-831 ◽  
pp. 358-361 ◽  
Author(s):  
D.G. Sondur ◽  
D.M. Goudar ◽  
D.G. Mallapur ◽  
G.B. Rudrakshi

In the present investigation, microstructural characteristics and dry sliding wear behaviour of T6 heat treated conventionally cast Al-25Mg2Si-2Cu alloy have been discussed. The as cast alloy was subjected to solutionizing at 500°C for 5h and isothermal aging treatment at 190°C for different aging times. The micro structural characterization was studied using Scanning Electron Microscope with EDS analysis. The microstructure of as cast alloy consists of intermetallics of coarse block like sharp edged β-(Mg2Si), θ-(Al2Cu) and Q-(Al-Mg-Cu-Si) in the form of Chinese scripts and needles distributed randomly in the Al-matrix. The microstructure of heat treated alloy shows spheroidization of β phase and fine precipitation of θ-(Al2Cu) and Q phases. The dry sliding wear test was carried out using pin-on-disc machine. Age hardened alloy exhibits high wear resistance and minimum coefficient of friction over the entire range of applied loads and sliding velocities. Furthermore, high wear resistance was observed in the under aged condition compared to over ageing conditions.


Lubricants ◽  
2021 ◽  
Vol 10 (1) ◽  
pp. 3
Author(s):  
Hamidreza Ghandvar ◽  
Mostafa Abbas Jabbar ◽  
Abdollah Bahador ◽  
Tuty Asma Abu Bakar ◽  
Nor Akmal Fadil ◽  
...  

In current study; the effect of various Gadolinium (Gd) additions on the microstructure and sliding wear behaviour of Al-15%Mg2Si composite before and after the hot extrusion process was examined. Optical microscopy (OM), scanning electron microscopy (SEM) equipped with EDX facility and X-ray diffraction (XRD) were used to characterize the microstructure. The results showed that with addition of 1.0 wt.% Gd to Al-15%Mg2Si composite, the primary Mg2Si particles size reduced from 44 µm to 23 µm and its morphology altered from dendritic to polygonal shape. Further refinement of primary Mg2Si particles was achieved after conducting hot extrusion which resulted in a decrease in its size to 19 µm with a transfer to near-spherical morphology. The Vickers hardness value increased from 55.6 HV in the as-cast and unmodified composite to 72.9 HV in the extruded 1.0% Gd modified composite. The wear test results revealed that composites treated with Gd possess higher wear resistance in comparison with those of without Gd. The highest wear resistance obtained with the lowest wear rates of 0.19 mm3/km and 0.14 mm3/km in the Al-15%Mg2Si-1.0% Gd before and after the hot extrusion, respectively. The high wear resistance of extruded Gd-modified Al-15%Mg2Si composite is due to the refinement of primary Mg2Si particles with uniform distribution in the composite matrix along with fragmentation of Gd intermetallic compounds.


Materials ◽  
2021 ◽  
Vol 14 (12) ◽  
pp. 3281
Author(s):  
Chiara Soffritti ◽  
Annalisa Fortini ◽  
Anna Nastruzzi ◽  
Ramona Sola ◽  
Mattia Merlin ◽  
...  

This work evaluates the dry sliding behavior of anodic aluminum oxides (AAO) formed during one traditional hard anodizing treatment (HA) and two golden hard anodizing treatments (named G and GP, respectively) on a EN AW-6060 aluminum alloy. Three different thicknesses of AAO layers were selected: 25, 50, and 100 μm. Prior to wear tests, microstructure and mechanical properties were determined by scanning electron microscopy (VPSEM/EDS), X-ray diffractometry, diffuse reflectance infrared Fourier transform (DRIFT-FTIR) spectroscopy, roughness, microhardness, and scratch tests. Wear tests were carried out by a pin-on-disc tribometer using a steel disc as the counterpart material. The friction coefficient was provided by the equipment. Anodized pins were weighed before and after tests to assess the wear rate. Worn surfaces were analyzed by VPSEM/EDS and DRITF-FTIR. Based on the results, the GP-treated surfaces with a thickness of 50 μm exhibit the lowest friction coefficients and wear rates. In any case, a tribofilm is observed on the wear tracks. During sliding, its detachment leads to delamination of the underlying anodic aluminum oxides and to abrasion of the aluminum substrate. Finally, the best tribological performance of G- and GP-treated surfaces may be related to the existence of a thin Ag-rich film at the coating/aluminum substrate interfaces.


Author(s):  
L.-M. Berger ◽  
P. Vuoristo ◽  
T. Mäntylä ◽  
W. Kunert ◽  
W. Lengauer ◽  
...  

Abstract WC-Co-Cr represents an important composition for hardmetal-like coatings which is appHed when simuhaneous wear and corrosion resistance is required. In this paper five commercially available spray powders obtained by various production techniques (sintered and crushed as well as agglomerated and plasma-densified) of the composition WC-10%Co- 4%Cr have been thoroughly characterized and were sprayed by DCS, HVOF (CDS process) and APS. The microstructures of the coatings were characterized and their wear behaviour was investigated by means of an abrasion wear test. For the best of these powders the wear resistance was nearly equal for the DGS and HVOF coatings. Other powders show significant differences with respect to their processabilities in these spray processes. APS coatings from all powders, obtained with an Ar/H2 plasma showed inferior microstructures and significant lower wear resistance. The spray powder compositions, grain sizes and structures were found to determine the processability of the powders and the microstructure and properties of the coatings. COMPOSITE MATERIALS of the type hard phase - metallic binder with WC and CoCr as constituents are widely used for the preparation of hardmetal-like coatings. The chromium addition to the metallic binder is thought to improve its corrosion resistance in comparison with pure WC-Co. This has led to many applications of WC-CoCr coatings where simultaneous wear and corrosion resistance is required. Despite of its significant practical importance only a limited number of publications is devoted to detailed questions of structure and properties of WC-CoCr coatings (1-3). In some comparative studies such coatings have been investigated together with WC-Co and Cr3C2-NiCr coatings (4-8). However, systematic investigations of spray powder compositions and morphologies as well as investigations of the influence of different thermal spray processes on coating structures and properties which have repeatedly been provided for WC-Co (for example (9, 10)) are missing for WC-CoCr. In this paper a short survey of literature on the phase relationships in the WC-CoCr system and the effect of chromium additions on the properties of sintered parts and thermally sprayed coatings compared to WC-Co is given. In the experimental part a systematic study of the influence of the preparation process on composition and morphology of commercially available WC-10%Co-4%Cr spray powders was provided. These powders have been sprayed by DGS, HVOF and APS and the microstructure and basic properties of the coatings have been studied.


Crystals ◽  
2020 ◽  
Vol 10 (4) ◽  
pp. 296 ◽  
Author(s):  
Chao Sun ◽  
Nannan Lu ◽  
Huan Liu ◽  
Xiaojun Wang ◽  
Xiaoshi Hu ◽  
...  

In this study, the dry sliding wear behaviors of SiC particle reinforced AZ91D matrix composites fabricated by stirring casting method were systematically investigated. The SiC particles in as-cast composites exhibited typical necklace-type distribution, which caused the weak interface bonding between SiC particles and matrix in particle-segregated zones. During dry sliding at higher applied loads, SiC particles were easy to debond from the matrix, which accelerated the wear rates of the composites. While at the lower load of 10 N, the presence of SiC particles improved the wear resistance. Moreover, the necklace-type distribution became more evident with the decrease of particle sizes and the increase of SiC volume fractions. Larger particles had better interface bonding with the matrix, which could delay the transition of wear mechanism from oxidation to delamination. Therefore, composites reinforced by larger SiC particles exhibited higher wear resistance. Similarly, owing to more weak interfaces in the composites with high content of SiC particles, more severe delamination occurred and the wear resistance of the composites was impaired.


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