Wear of Carbon Nanofiber Reinforced HDPE Nanocomposites Under Dry Sliding Condition

Author(s):  
Songbo Xu ◽  
Aydar Akchurin ◽  
Tian Liu ◽  
Weston Wood ◽  
X. W. Tangpong ◽  
...  

High density polyethylene (HDPE) is widely used as a bearing material in industrial application because of its low friction and high wear resistance properties. Carbon nanofiber (CNF) reinforced HDPE nanocomposites are promising materials for biomedical applications as well, such as being the bearing materials in total joint replacements. The main objective of the present study is to investigate how the wear of HDPE can be altered by the addition of either pristine or silane treated CNFs at different loading levels (0.5 wt. % and 3 wt. %). Two types of silane coating thicknesses, 2.8 nm and 46 nm, were applied on the surfaces of oxidized CNFs to improve the interfacial bonding strength between the CNFs and the matrix. The CNF/HDPE nanocomposites were prepared through melt mixing and hot-pressing. The coefficients of friction (COFs) and wear rates of the neat HDPE and CNF/HDPE nanocomposites were determined using a pin-on-disc tribometer under dry sliding conditions. The microstructures of the worn surfaces of the nanocomposites were characterized using both scanning electron microscope (SEM) and optical microscope to analyze their wear mechanisms. Compared with the neat HDPE, the COF of the nanocomposites were reduced. The nanocomposite reinforced with CNFs coated with the thicker silane coating (46 nm) at 0.5 wt. % loading level was found to yield the highest wear resistance with a wear rate reduction of nearly 68% compared to the neat HDPE.

Author(s):  
Songbo Xu ◽  
Aydar Akchurin ◽  
X. W. Tangpong ◽  
Tian Liu ◽  
Weston Wood ◽  
...  

High density polyethylene (HDPE) is widely used as bearing material in industrial application because of its low friction and high wear resistance properties. Carbon nanofiber (CNF) reinforced HDPE nanocomposites are promising materials for biomedical applications as well, such as being the bearing materials in total joint replacements. The main objective of the present study is to investigate how the wear of HDPE can be altered by the addition of either pristine or silane treated CNFs at different loading levels (0.5 wt.% and 3 wt.%). Two types of silane coating thicknesses, 2.8 nm and 46 nm, were applied on the surfaces of oxidized CNFs to improve the interfacial bonding strength between the CNFs and the matrix. The CNF/HDPE nanocomposites were prepared through melt mixing and hot-pressing. The coefficients of friction (COFs) and wear rates of the neat HDPE and CNF/HDPE nanocomposites were determined using a pin-on-disc tribometer under dry sliding conditions. The microstructures of the worn surfaces of the nanocomposites were characterized using both scanning electron microscope (SEM) and optical microscope to analyze their wear mechanisms. Compared with the neat HDPE, the COF of the nanocomposites were reduced. The nanocomposite reinforced with CNFs coated with the thicker silane coating (46 nm) at 0.5 wt.% loading level was found to yield the highest wear resistance with a wear rate reduction of nearly 68% compared to the neat HDPE.


2012 ◽  
Vol 134 (4) ◽  
Author(s):  
Songbo Xu ◽  
Aydar Akchurin ◽  
Tian Liu ◽  
Weston Wood ◽  
X. W. Tangpong ◽  
...  

New applications of carbon-based materials have been continuously developed in recent years. Carbon nanofibers (CNFs) with silane coatings were added into high density polyethylene (HDPE) to improve the tribological properties of the nanocomposite material. The nanocomposites were fabricated with various weight percentages of carbon nanofibers (0.5 wt.%, 1 wt.% and 3 wt.%) that were treated with different silane coating thicknesses (2.8 nm and 46 nm) through melt-mixing and compressive processing. The wear and friction tests were performed on a pin-on-disc tribometer under phosphate buffered saline lubricated condition. Compared with the neat HDPE, the friction coefficients of the nanocomposites were reduced in all samples, yet only a couple of nanocomposite samples showed lower wear rates. Micro-hardness measurements of the nanocomposites were carried out and CNFs were found to be capable of increasing the material’s micro-hardness. The effects of concentration and silane coating thickness of CNFs on the tribological properties of the resulting nanocomposites were analyzed and the wear mechanisms of the HDPE/CNF nanocomposites were discussed.


2011 ◽  
Vol 462-463 ◽  
pp. 1224-1229 ◽  
Author(s):  
I. Agung ◽  
Junaidi Syarif ◽  
Mariyam Jameelah Ghazali ◽  
Z. Sajuri

Effect of peak-aged and over-aged Cu particles on wear behaviour of ferritic iron was investigated by means of Pin-on-Disc wear test under dry sliding condition. It was found that hardness of the peak-aged sample was higher than the over-aged sample. The specific wear rates of peak-aged samples were in the range of 0.20 × 10-4 to 0.89 × 10-4 mm3/(Nm) while the over-aged samples were in the range of 0.21 × 10-4 to 1.29 × 10-4 mm3/(Nm). Although both samples possessed moderate wear behaviours, the peak-aged samples had better wear resistance. Scanning Electron Microscopy observation found that most wear mechanism were due to plastic ploughing phenomenon. Transferred materials from the counterface tool was also proven by Energy Dispersive Spectroscopy test. However, the roughness test showed that the peak-aged sample surface was finer than the over-aged sample surface. Average roughness of peak-aged samples were in the range of 0.49 to 1.79 μm while the over-aged samples were in the range of 3.28 to 4.02 μm. Hence, it can be concluded that the peak-aged Cu particles can improve the wear resistance of steel.


Materials ◽  
2021 ◽  
Vol 14 (3) ◽  
pp. 535
Author(s):  
Alexander Mironov ◽  
Iosif Gershman ◽  
Eugeniy Gershman ◽  
Pavel Podrabinnik ◽  
Ekaterina Kuznetsova ◽  
...  

Potential relations of tribological characteristics of aluminum antifriction alloys with their compositions and mechanical properties were investigated. In this regard, the properties of eight aluminum alloys containing tin from 5.4% to 11% doped with lead, copper, silicon, zinc, magnesium, and titanium were studied. Mechanical properties such as hardness, strength, relative extension, and impact strength were analyzed. Within the tribological tests seizure load and wear of material were evaluated and secondary structures were studied afterwards. The absence of a definitive correlation between tribological behavior and mechanical properties was shown. It was determined that doping tin over 6% is excessive. The seizure load of the alloys increases with the magnesium content. Secondary structures of the alloys with higher wear rates contain one order less magnesium and tin.


Materials ◽  
2021 ◽  
Vol 14 (12) ◽  
pp. 3281
Author(s):  
Chiara Soffritti ◽  
Annalisa Fortini ◽  
Anna Nastruzzi ◽  
Ramona Sola ◽  
Mattia Merlin ◽  
...  

This work evaluates the dry sliding behavior of anodic aluminum oxides (AAO) formed during one traditional hard anodizing treatment (HA) and two golden hard anodizing treatments (named G and GP, respectively) on a EN AW-6060 aluminum alloy. Three different thicknesses of AAO layers were selected: 25, 50, and 100 μm. Prior to wear tests, microstructure and mechanical properties were determined by scanning electron microscopy (VPSEM/EDS), X-ray diffractometry, diffuse reflectance infrared Fourier transform (DRIFT-FTIR) spectroscopy, roughness, microhardness, and scratch tests. Wear tests were carried out by a pin-on-disc tribometer using a steel disc as the counterpart material. The friction coefficient was provided by the equipment. Anodized pins were weighed before and after tests to assess the wear rate. Worn surfaces were analyzed by VPSEM/EDS and DRITF-FTIR. Based on the results, the GP-treated surfaces with a thickness of 50 μm exhibit the lowest friction coefficients and wear rates. In any case, a tribofilm is observed on the wear tracks. During sliding, its detachment leads to delamination of the underlying anodic aluminum oxides and to abrasion of the aluminum substrate. Finally, the best tribological performance of G- and GP-treated surfaces may be related to the existence of a thin Ag-rich film at the coating/aluminum substrate interfaces.


Crystals ◽  
2020 ◽  
Vol 10 (4) ◽  
pp. 296 ◽  
Author(s):  
Chao Sun ◽  
Nannan Lu ◽  
Huan Liu ◽  
Xiaojun Wang ◽  
Xiaoshi Hu ◽  
...  

In this study, the dry sliding wear behaviors of SiC particle reinforced AZ91D matrix composites fabricated by stirring casting method were systematically investigated. The SiC particles in as-cast composites exhibited typical necklace-type distribution, which caused the weak interface bonding between SiC particles and matrix in particle-segregated zones. During dry sliding at higher applied loads, SiC particles were easy to debond from the matrix, which accelerated the wear rates of the composites. While at the lower load of 10 N, the presence of SiC particles improved the wear resistance. Moreover, the necklace-type distribution became more evident with the decrease of particle sizes and the increase of SiC volume fractions. Larger particles had better interface bonding with the matrix, which could delay the transition of wear mechanism from oxidation to delamination. Therefore, composites reinforced by larger SiC particles exhibited higher wear resistance. Similarly, owing to more weak interfaces in the composites with high content of SiC particles, more severe delamination occurred and the wear resistance of the composites was impaired.


2015 ◽  
Vol 642 ◽  
pp. 55-59 ◽  
Author(s):  
Shueiwan Henry Juang ◽  
Liang Jing Fan ◽  
Hsu Shuo Chang

In this study, the multi-pass friction stir processing (MP-FSP) technique was performed on ADC6 aluminum alloy + 5 wt% fly ash composite (A5FC) castings to increase their surface area. The dry sliding wear behaviors of the ADC6 alloy, A5FCs, and MP-FSPed A5FCs were evaluated. Dry sliding wear tests were performed using a ring-on-washer machine at a constant rotation speed of 100 rpm for 60 min, and the normal load was 10, 20, 30, and 40 N. The results showed that the MP-FSPed A5FCs had the lowest wear rates in the load range from 10 to 40 N, and adhesive wear was the major wear mechanism in these tests. The increased wear resistance was mainly due to grain refinement and elimination of casting defects after subjecting the ash composite to MP-FSP. The microstructure of the MP-FSPed A5FCs reveals that the sizes of the added raw fly ash particles decreased from micro-to nanoscale levels, and the nanoscale fly ash was uniformly dispersed in the aluminum matrix.


Materials ◽  
2019 ◽  
Vol 12 (20) ◽  
pp. 3431 ◽  
Author(s):  
Daniel Toboła

We have evaluated phase composition changes in the surface layer (SL) and wear resistance of steels investigated after various mechanical processes such as a pre-sulphonitriding treatments. Two various paths of surface modification were employed: Grinding–sulphonitriding (G-SN) and hard turning–slide burnishing–sulphonitriding (T-B-SN). Studies were carried out on Vanadis 8 and Vancron 40 tool steels, which are classified as advanced powder metallurgy (P/M) high-alloyed steels with different types and amounts of carbides. Heat treatment to the final hardness of 64 ± 1 HRC (Vanadis 8) and 62 ± 1 HRC (Vancron 40) was performed in vacuum furnaces with gas quenching. Precipitation of different types such as sulfides, nitrides, and carbides was observed using X-ray diffraction analysis. Tribological properties of SL were evaluated by pin-on-disc experiments. Pins of Al2O3 and 19MnB4 steel were used as counterbodies materials. 3D surface geometrical structure measurements were also performed. Wear tracks and cross-sections of SL were observed using optical and scanning electron microscopy. The three-stage process increases the wear resistance about 37% and 30%, respectively for Vanadis 8 and Vancron 40 (in case of alumina pins), whereas values of wear rates after tests performed against steel pins were very similar for two compared processes for both steels.


2009 ◽  
Vol 83-86 ◽  
pp. 545-552 ◽  
Author(s):  
Majid Abbasi ◽  
S. Kheirandish ◽  
Y. Kharrazi ◽  
J. Hejazi

The abrasive wear behaviors of different types of steels were evaluated using the abrasive wheel as a new technique in the pin on disc method. It is shown that the abrasive studies using this test method is acceptable for high wear resistance metals such as Hadfield steels, while it is not proper for soft materials such as mild steel. The test results on the different materials also show that initial hardness of materials cannot merely determine the wear resistance. However, microstructural changes during the sliding have significant effect on the wear behavior and must be included.


2011 ◽  
Vol 415-417 ◽  
pp. 707-710
Author(s):  
Hua Chen ◽  
Hai Ying Sun

Fe-based system powder metallurgy in the as-sintered was investigated on pin-on-rolling wear tester for their dry sliding wear behaviour. The morphology of worn surfaces and wear mechanism were analysed by SEM. Results show the hot-forging deformation quenching and tempered considerably decreased the porosity and improved wear resistance, and compare with quenching microstructure, tempered microstructure has high wear resistance and match of strength-toughness. Fe-2.0Ni-0.4Mo-0.5C-0.6Cr alloy presented best wear characteristics. SEM observations of the worn surface revealed microploughing and plastic deformation and crack were the basic dry sliding wear morphology,and oxidative wear and delamination wear are dominant wear mechanism.


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