Evaluating Initial Content of the Slurry and Cooling Rate on the Microstructural and Mechanical Characteristics of Freeze Casted Hydroxyapatite Macroporous Scaffolds

2012 ◽  
Vol 529-530 ◽  
pp. 147-152 ◽  
Author(s):  
Sajad Farhangdoust ◽  
Sayed Mahmood Rabiee ◽  
Ali Zamanian ◽  
Mana Yasaei ◽  
Mina Khorami ◽  
...  
Keyword(s):  
Compressive Strength ◽  
Cooling Rate ◽  
Mechanical Characteristics ◽  
Proximal Tibia ◽  
Total Porosity ◽  
A Value ◽  
Physical Chemical ◽  
Freeze Dried ◽  
Biological Criteria ◽  
Initial Content

Scaffolds have to meet exacting physical, chemical, and biological criteria to function successfully, and those criteria vary with the type of tissue being repaired. In the present work, slurry with different initial content of 7.5-22.5 vol% HA prepared from calcinated hydroxyapatite. The prepared slurries freeze casted unidirectionally with the different cooling rate of 2-14°C/min with intervals of 3°C/min from the ambient temperature. Then, green bodies freeze-dried for 72h following with sintering at temperatures of 1350°C. The results showed that compressive strength goes up with cooling rate and initial content. Total porosity has a range of 66-88% while has a compressive strength of ~0.4-18 MPa. Porosity size has a value of 20-200 μm by initial content and cooling rate. Based on strength and porosity, the specimen with initial content and cooling rate of 15 vol% and 5°C/min, respectively, chose to be the optimum. This specimen has a compressive strength and porosity size of 5.26 MPa and 88 μm, respectively. The compressive strength value of the mentioned lamellar HA scaffolds was in the range of the values reported for human proximal tibia.

The Effect of Sintering Temperature on the Microstructural and Mechanical Characteristics of Hydroxyapatite Macroporous Scaffolds Prepared via Freeze-Casting

2012 ◽  
Vol 529-530 ◽  
pp. 133-137 ◽  
Author(s):  
Ali Zamanian ◽  
Sajad Farhangdoust ◽  
Mana Yasaei ◽  
Mina Khorami ◽  
Mohamad Abbasabadi
Keyword(s):  
Compressive Strength ◽  
Mechanical Characteristics ◽  
Sintering Temperature ◽  
Total Porosity ◽  
Sintered Sample ◽  
Dendritic Branch ◽  
Injured Tissue ◽  
Freeze Dried ◽  
Different Temperatures ◽  
Bone Repairing

The most important characteristic of biomaterial as bone-repairing material, in addition to biocompatibility and appropriate porosity, is providing mechanical strength complying with injured tissue. In the present work, slurry with 15 vol% HA prepared from calcinated hydroxyapatite. The prepared slurry freeze casted unidirectionally with the cooling rate of 8°C/min from the ambient temperature. Then, green bodies freeze-dried for 72h following with sintering at different temperatures of 1250-1350°C with intervals of 25°C. The results showed that lamella space and porosity decreases with temperature while compressive strength and shrinkage goes up. Total porosity has a range of 75-83% while has a compressive strength of ~2-8 MPa. The sintered sample at 1350°C, with 75% porosity, which has a ~ 8 MPa compressive strength, chose to be the optimum. Also, some dendritic branch like structure and bridges can be seen on the internal walls of lamellae which can improve mechanical properties. These features may improve adhesion and growth of osseous cells.

Obtaining and Characterisation of Starch-Based Edible Films Incorporating Honey, Propolis and Bee Bread

2019 ◽  
Vol 23 (2) ◽  
pp. 193-198
Author(s):  
Monica Mironescu ◽  
Laura Fratila ◽  
Alexandru Hupert ◽  
Ion Dan Mironescu
Keyword(s):  
Water Activity ◽  
Mechanical Characteristics ◽  
Edible Films ◽  
Ash Content ◽  
Colour Intensity ◽  
Sensorial Analysis ◽  
Physical Chemical ◽  
Control Film ◽  
Bee Bread

Abstract This research investigates the physical-chemical, sensorial and mechanical characteristics of starch-based edible films incorporating three types of bee hive products: honey, propolis and bee bread, in concentrations varying from 1% to 3%, reported to starch. The results indicates an increasing of films moisture, water activity, ash content and acidity, in the order: honey<propolis<bee bread, all values increasing with the increasing of hive products percentage into the control film; aw is remaining at very low values, under 0.4. Sensorial analysis indicated honey as the better suited for improving taste and flavour and bee bread for increasing colour intensity of the films; the sensorial characteristics are maintained during 30 days of films storage, in all cases. Compared with the control starch-based film (which is elastic, brittle and hard), the films containing 2% bee hive products are elasto-plastic and more resistant to penetration, the resistance increasing in the order: bee bread<propolis<honey.

scholarly journals Carbonization Durability of Two Generations of Recycled Coarse Aggregate Concrete with Effect of Chloride Ion Corrosion

2020 ◽  
Vol 12 (24) ◽  
pp. 10544
Author(s):  
Chunhong Chen ◽  
Ronggui Liu ◽  
Pinghua Zhu ◽  
Hui Liu ◽  
Xinjie Wang
Keyword(s):  
Compressive Strength ◽  
Coarse Aggregate ◽  
Chloride Ion ◽  
Total Porosity ◽  
Recycled Concrete ◽  
Carbonation Depth ◽  
Aggregate Concrete ◽  
Recycled Coarse Aggregate ◽  
Carbonation Resistance ◽  
Two Generations

Carbonation durability is an important subject for recycled coarse aggregate concrete (RAC) applied to structural concrete. Extensive studies were carried out on the carbonation resistance of RAC under general environmental conditions, but limited researches investigated carbonation resistance when exposed to chloride ion corrosion, which is an essential aspect for reinforced concrete materials to be adopted in real-world applications. This paper presents a study on the carbonation durability of two generations of 100% RAC with the effect of chloride ion corrosion. The quality evolution of recycled concrete coarse aggregate (RCA) with the increasing recycling cycles was analyzed, and carbonation depth, compressive strength and the porosity of RAC were measured before and after chloride ion corrosion. The results show that the effect of chloride ion corrosion negatively affected the carbonation resistance of RAC, and the negative effect was more severe with the increasing recycling cycles of RCA. Chloride ion corrosion led to a decrease in compressive strength, while an increase in carbonation depth and the porosity of RAC. The equation of concrete total porosity and carbonation depth was established, which could effectively judge the deterioration of carbonation resistance of RAC.

PEMANFAATAN LIMBAH KOTORAN SAPI SEBAGAI PENGGANTI SEBAGIAN SEMEN DALAM PEMBUATAN BATAKO

2020 ◽  
Vol 15 (2) ◽  
pp. 53-57
Author(s):  
Kiki Kurniawan ◽  
Prihantono Prihantono ◽  
Rosmawita Saleh
Keyword(s):  
Compressive Strength ◽  
Water Absorption ◽  
Mean Value ◽  
Cow Dung ◽  
A Value ◽  
Average Water ◽  
Hollow Brick ◽  
Average Compressive Strength

The results showed the use of cow dung waste can increase the compressive strength of hollow brick from any composition of waste. Hollow brick with cow dung substitution of 0% has an average compressive strength value 44.75 Kg/Cm2 has an average water absorption of 14.31%, hollow brick with cow dung substitution of 5% has a value of compressive strength average 47.47 Kg/Cm2 has an average water absorption of 15.67%, Batako perforation with cow dung substitution of 7.5% has an average compressive strength value of 51.83 Kg/Cm2 has the absorption water averaging 13.71%, batako perforated with substitution of cow dung waste of 10% has an average compressive strength value 53.81 Kg/Cm2 has an average water absorption of 10.04%, hollow brick with substitution cow dung waste of 12.5% has an average compressive strength value of 50.66 Kg/Cm2 has an average water absorption of 23.6%, hollow brick with cow dung substitution of 15% average 48.84 Kg/Cm2 has an average water absorption of 19.72%. The optimum compressive strength value was obtained from percentage substitution of cow dung waste at 10% with mean value of compressive strength 53,81 Kg/Cm2 with average water absorption 10,04%.

scholarly journals Amorphous fiber based on the Fe-B-C molten system for bulk reinforcement of concrete

2018 ◽  
Vol 245 ◽  
pp. 03019 ◽  
Author(s):  
Artemiy Cherkashin ◽  
Yasmin Begich ◽  
Polina Sherstobitova ◽  
Oleg Tolochko
Keyword(s):  
Tensile Strength ◽  
Compressive Strength ◽  
Mechanical Characteristics ◽  
Test Material ◽  
Comparative Tests ◽  
Physical And Mechanical Characteristics

The article deals with the use of amorphous fiber of the Fe-B-C system, which was obtained by spinning the melt. Comparative tests of the samples made on the basis of the test material on the compressive strength and tensile strength of the traditional destructive method were made. The conductivity of the samples was also tested. Physical and mechanical characteristics of the material are obtained.

scholarly journals Adherence between steel bars and lightweight concrete with EPS beads

2017 ◽  
Vol 10 (1) ◽  
pp. 122-140
Author(s):  
A. L. SARTORI ◽  
L. M. PINHEIRO ◽  
R. M. DA SILVA ◽  
S. B. FREITAS ◽  
T. G. CESAR
Keyword(s):  
Tensile Strength ◽  
Compressive Strength ◽  
Mechanical Characteristics ◽  
Lightweight Concrete ◽  
Monotonic Loading ◽  
Adherence Behavior ◽  
Ordinary Concrete ◽  
Cylinder Test ◽  
Pull Out ◽  
Steel Bars

Abstract This paper describes the adherence behavior of a structural lightweight concrete with EPS beads (SLCEB) in a monotonic loading, based in a bibliographic review and in pull-out tests. The results of these SLCEB tests were compared with those of an ordinary concrete (OC) and with the values based in indications of the Brazilian code ABNT NBR 6118:2014 - Design of concrete structures. The pull-out tests of two batches of SLCEB and one of OC were analyzed, in a total of 60 tests. Mechanical characteristics were determined too, such as: compressive strength and tensile strength in split cylinder test. The calculated results according to the above mentioned standard were very different from those obtained in the tests, indicating that the theoretical values are more conservative than the experimental ones. It was also verified that it is possible to use SLCEB in structures with respect to the adequate adherence of reinforcement in the concrete.

scholarly journals Strength Characteristics of High Strength Concrete (HSC) with and without Coarse Aggregate

2019 ◽  
Vol 9 (2) ◽  
pp. 4701-4704
Keyword(s):  
Mechanical Properties ◽  
Compressive Strength ◽  
Fly Ash ◽  
Flexural Strength ◽  
Silica Fume ◽  
High Strength Concrete ◽  
Mechanical Characteristics ◽  
Coarse Aggregate ◽  
High Strength ◽  
Set Up

This paper aimed to investigate the mechanical characteristics of HSC of M60 concrete adding 25% of fly ash to cement and sand and percentage variations of silica fumes 0%,5% and 10% to cement with varying sizes of 10mm,6mm,2mm and powder of granite aggregate with w/c of 0.32. Specimens are tested for compressive strength using 10cm X 10cmX10cm cubes for 7,14,28 days flexural strength was determined by using 10cmX10cmX50cm beam specimens at 28 days and 15cm diameter and 30cm height cylinder specimens at 28 days using super plasticizers of conplast 430 as a water reducing agent. In this paper the experimental set up is made to study the mechanical properties of HSC with and without coarse aggregate with varying sizes as 10mm, 6mm, 2mm and powder. Similarly, the effect of silica fume on HSC by varying its percentages as 0%, 5% and 10% in the mix studied. For all mixes 25% extra fly ash has been added for cement and sand.

Influence of Palm Oil Fibers Length Variation on Mechanical Properties of Reinforced Crude Bricks

2022 ◽  
Author(s):  
Mazhar Hussain ◽  
Daniel Levacher ◽  
Nathalie Leblanc ◽  
Hafida Zmamou ◽  
Irini Djeran Maigre ◽  
...  
Keyword(s):  
Thermal Conductivity ◽  
Tensile Strength ◽  
Compressive Strength ◽  
Thermal Properties ◽  
Composite Materials ◽  
Physical Properties ◽  
Palm Oil ◽  
Mechanical Characteristics ◽  
Natural Fibers ◽  
Indirect Tensile

Crude bricks are composite materials manufactured with sediments and natural fibers. Natural fibers are waste materials and used in construction materials for reinforcement. Their reuse in manufacturing reinforced crude bricks is eco-friendly and improves mechanical and thermal characteristics of crude bricks. Factors such as type of fibers, percentage of fibers, length of fibers and distribution of fibers inside the bricks have significant effect on mechanical, physical and thermal properties of biobased composite materials. It can be observed by tests such as indirect tensile strength, compressive strength for mechanical characteristics, density, shrinkage, color for physical properties, thermal conductivity and resistivity for thermal properties, and inundation test for durability of crude bricks. In this study, mechanical and physical characteristics of crude bricks reinforced with palm oil fibers are investigated and effect of change in percentage and length of fibers is observed. Crude bricks of size 4*4*16 cm3 are manufactured with dredged sediments from Usumacinta River, Mexico and reinforced with palm oil fibers at laboratory scale. For this purpose, sediments and palm oil fibers characteristics were studied. Length of fibers used is 2cm and 3cm. Bricks manufacturing steps such as sediments fibers mixing, moulding, compaction and drying are elaborated. Dynamic compaction is opted for compaction of crude bricks due to energy control. Indirect tensile strength and compressive strength tests are conducted to identify the mechanical characteristics of crude bricks. Physical properties of bricks are studied through density and shrinkage. Durability of crude bricks is observed with inundation test. Thermal properties are studied with thermal conductivity and resistivity test. Distribution and orientation of fibers and fibers counting are done to observe the homogeneity of fibers inside the crude bricks. Finally, comparison between the mechanical characteristics of crude bricks manufactured with 2cm and 3cm length with control specimen was made.

Effect of benzoyl treatment on the performance of sugar palm/kenaf fiber-reinforced polypropylene hybrid composites

2021 ◽  
pp. 004051752110432
Author(s):  
S Mohd Izwan ◽  
SM Sapuan ◽  
MYM Zuhri ◽  
AR Muhamed
Keyword(s):  
Mechanical Properties ◽  
Mechanical Characteristics ◽  
Hybrid Composites ◽  
Physical And Mechanical Properties ◽  
Morphological Properties ◽  
Fiber Reinforced ◽  
Kenaf Fiber ◽  
A Value ◽  
Hydrophobic Behavior ◽  
Sugar Palm Fiber

The main purpose of this work is to investigate the effect of benzoyl treatment on the performance of sugar palm/kenaf fiber-reinforced polypropylene hybrid composites. Water absorption tests were carried out to confirm the effect of benzoylation treatment toward fabricating a more hydrophobic behavior of the hybrid composites. Both treated and untreated composites that have 10 wt.% of fiber loading with three different fiber ratios between sugar palm and kenaf (7:3, 5:5, 3:7) were analyzed. Physical and mechanical properties such as tensile, flexural, and impact strength were determined from this study. Morphological properties were obtained using scanning electron microscopy (SEM). It was found that the tensile strength of sugar palm/kenaf-reinforced polypropylene hybrid composites was improved with the treatment of benzoyl with a value of 19.41 MPa. In addition, hybrid composite with treated sugar palm and kenaf fiber T-SP3K7 recorded the highest impact and flexural strength of 19.4 MPa and 18.4 MPa, respectively. In addition, SEM demonstrated that surface treatment enhanced the mechanical properties of the hybrid composites. Overall, it can be suggested that benzoyl-treated composites with a higher volume of kenaf fiber than sugar palm fiber will improve the mechanical characteristics of the hybrid composites.

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