Joining of C/SiC Composite and TC4 Alloy Using 70Ag28Cu2Ti Active Brazing Alloy

2013 ◽  
Vol 544 ◽  
pp. 167-171 ◽  
Author(s):  
Jia Ke Li ◽  
Xiu Liu ◽  
Jian Er Zhou

C/SiC composite and TC4 alloy were successfully brazed using 70Ag28Cu2Ti (wt. %) as filler metal at 820 °C~920 °C for 5 min ~30 min. The effects of brazing parameters on the microstructures, phase composition, shear strength of the brazed joints were investigated by SEM, XRD. The mechanical performances of the brazed joints were measured by a universal mechanical testing machine. The results show that successful joining of C/SiC composite and TC4 alloy owes to interfacial reactions between the brazing alloy and the parent materials, and resultantly produce TiC, Ti5Si3 and Ti-Cu serial compounds at the interfaces; the interfacial structure of the brazed joint is C/SiC composite / TiC / Ti5Si3 /Ag (s.s) +Cu (s.s) / TiCu2 / Ti3Cu4 / TiCu / Ti2Cu / TC4 from C/SiC composite side to TC4 alloy side; the maximum shear strength of the brazed joint is 53.3 MPa at 860°C for 10min.

2012 ◽  
Vol 512-515 ◽  
pp. 415-420
Author(s):  
Jia Ke Li ◽  
Xin Liu ◽  
Jian Er Zhou

C/C composite and TC4 alloy were successfully brazed using 70Ag28Cu2Ti (wt. %) as filler metal at brazing temperature 820 º°C~920 °C for soaking time 5 min ~30 min. The effects of brazing parameters on the microstructures and phase composition and the fracture modes of the brazed joints were investigated by SEM and XRD. The mechanical performances of the brazed joints were measured by a universal mechanical testing machine. The results show that the maximum shear strength of the brazed joint is 28 MPa at brazing temperature 860°C and soaking time 10min. Fracture surface analysis of the brazed joints indicates that the position of the fracture surface is related to the orientation of carbon fiber. The brazed joints are fractured in the C/C composite when the carbon fiber is parallel to the joined surface, and the brazed joints are fractured at the C/C composite / 70Ag28Cu2Ti interface when the carbon fiber is vertical to the joined surface.


Metals ◽  
2019 ◽  
Vol 9 (2) ◽  
pp. 198 ◽  
Author(s):  
Peng Xue ◽  
Yang Zou ◽  
Peng He ◽  
Yinyin Pei ◽  
Huawei Sun ◽  
...  

The microstructure and properties of a Cu/304 stainless steel dissimilar metal joint brazed with a low silver Ag16.5CuZnSn-xGa-yCe braze filler after aging treatment were investigated. The results indicated that the addition of Ce could reduce the intergranular penetration depth of the filler metal into the stainless steel during the aging process. The minimum penetration depth in the Ag16.5CuZnSn-0.15Ce brazed joint was decreased by 48.8% compared with the Ag16.5CuZnSn brazed joint. Moreover, the shear strength of the brazed joint decreased with aging time while the shear strength of the AgCuZnSn-xGa-yCe joint was still obviously higher than the Ag16.5CuZnSn joint after a 600 h aging treatment. The fracture type of the Ag16.5CuZnSn-xGa-yCe brazed joints before aging begins ductile and turns slightly brittle during the aging process. Compared to all the results, the Ag16.5CuZnSn-2Ga-0.15Ce brazed joints show the best performance and could satisfy the requirements for cost reduction and long-term use.


2005 ◽  
Vol 297-300 ◽  
pp. 2441-2446 ◽  
Author(s):  
Shi Yao Qu ◽  
Zeng Da Zou ◽  
Xin Hong Wang

Shear strength and fracture behavior of Al2O3 matrix ceramic composite brazed joints to carbon steel with Ag-Cu-Ti brazing alloy in flow argon have been studied by means of SEM, EDX and all-purpose testing machine. Results have shown that there is a close relationship between the shear strength and the fracture form of brazed joints. The fracture occurring completely in the composite near the composite/filler metal interface corresponds to the low strength of a joint, and the strength of the joint fractured partially in the composite usually increases with decreasing the proportion of the composite on the fracture surface in the steel side. When the fracture occurs in the reaction layer between the composite and the filler metal, the closer the fractured position comes to the composite/reaction layer interface, the higher the joint strength. The maximum shear strength is obtained when the fracture occurs fully at the interface.


Metals ◽  
2018 ◽  
Vol 8 (11) ◽  
pp. 896 ◽  
Author(s):  
Duo Dong ◽  
Dongdong Zhu ◽  
Ye Wang ◽  
Gang Wang ◽  
Peng Wu ◽  
...  

Vacuum brazing of TiAl intermetallic alloy to Si3N4 ceramics was performed using Ag-28Cu (wt.%) filler alloy. The brazing joints obtained at different brazing temperatures were studied in this work. The microstructure and the shear strength were analyzed in detail. The results show that the brazed joints could be divided into three regions: AlCu2Ti reaction layer near the Ti-48Al-2Cr-2Nb alloy, a typical Ag-Cu eutectic structure and a thin continuous TiN + Ti5Si3 reaction layer near the Si3N4 ceramics. The microstructure varied as the brazing temperature was increased from 1153 K/15 min to 1193 K/15 min. The shear strength of the joints first increased as the brazing temperature increased from 1153 K to 1173 K, and then decreased. The maximum shear strength reached 105.5 MPa at 1173 K/15 min and the mechanism was discussed.


Materials ◽  
2021 ◽  
Vol 14 (15) ◽  
pp. 4216
Author(s):  
Shubin Liu ◽  
Ikuo Shohji ◽  
Tatsuya Kobayashi ◽  
Katsuharu Osanai ◽  
Tetsuya Ando ◽  
...  

In this study, an amorphous Ni-13.4Cr-11.6P (mass%) alloy coating with a thickness of 30 μm was deposited on the surface of SUS304 stainless steel as a brazing filler metal to conduct brazing. The differential thermal analysis measurements indicate that the electrodeposited Ni-13.4Cr-11.6P alloy has a melting point of approximately 892 °C, which is almost consistent with that of the commercial BNi-7 filler metal. The microstructure, shear strength, and fracture mode of the brazed joint were investigated using an electron probe X-ray microanalyzer, a scanning electron microscope, an optical microscope, and a universal testing machine. The results showed that the brazed filler metal is filled between the SUS304 stainless steel plates without any flaws in the brazed seam. The P-containing phases, i.e., the Cr-P rich phase and the (Ni,Fe)3P phase, were formed in the brazed seam. The shear strength of the brazed joint obtained in this study is 59.0 MPa. The fracture occurs in the brazed filler zone, where the brittle P-containing phases are present. Galvanic current measurement results showed that the brazed Ni-13.4Cr-11.6P alloy coating has a better corrosion resistance than that of the brazed Ni-11P alloy coating, which can be attributed to the formation of a large amount of Ni-Fe solid solution and Cr-P rich phase in the top layer of the brazed Ni-13.4Cr-11.6P alloy coating.


2021 ◽  
Vol 2083 (2) ◽  
pp. 022086
Author(s):  
Xiupeng Li ◽  
Yunyue Li ◽  
Sujuan Zhong ◽  
Yuanxun Shen ◽  
Weimin Long ◽  
...  

Abstract In this paper, a new type of AlSiMgCuNiAg filler metal was developed. The solidus temperature of the filler metal is 509.1°C and the liquidus temperature is 531.3°C. The filler metal has a good wetting and spreading effect on the surface of 6061 aluminum alloy. The CuAl2 phase in the brazing seam was greatly aggregated after brazed, while the CuAl2 phase was reduced and Mg2Si strengthening phase was formed when the brazed joints with heat treatment. The average shear strength of the brazed joint without heat treatment was 47.1MPa, and the average shear strength of the brazed joint with heat treatment reached to 108.7Mpa. The strength of the brazed joint with heat treatment was increased by about 131% relative to the strength of the brazed joint without heat treatment.


2019 ◽  
Vol 91 (10) ◽  
pp. 35-41 ◽  
Author(s):  
Li Hong ◽  
Liu Xuan ◽  
Huang Haixin

Reliable ceramics/metal joints have an extensive application in the aerospace and biomedical area. However, ZrO2ceramic has not been investigated systematically compared to the Si3N4and Al2O3ceramic. Therefore, successful brazing of ZrO2ceramic and Ti-6A-4V alloy was achieved by using a binary active Ti-28Ni filler metal in this paper. The effect of holding time on the microstructure of ZrO2 ceramic/filler metal interface and mechanical properties of brazed joints was investigated. The results indicated that the representative interfacial microstructure was ZrO2ceramic/Ti2O/Ni2Ti4O/Ti-rich phase/Ti2Ni+α-Ti. With the increase of holding time, the thickness of Ti-rich layer in the interface of ZrO2/Ti-6Al-4Vjoint decreased obviously due to the diffusion of Ti atoms. Substantial brittle intermetallic compounds Ti2Ni and Ni2Ti4O were formed in the joint, which were detrimental to the mechanical properties of the brazed joints. The maximum shear strength of joint was 112.7 MPa when brazed at 1060 °C for 10 min.


2019 ◽  
Vol 9 (6) ◽  
pp. 1094
Author(s):  
Shubin Liu ◽  
Ikuo Shohji ◽  
Makoto Iioka ◽  
Anna Hashimoto ◽  
Junichiro Hirohashi ◽  
...  

A Ni-P plated layer of 20 μm thickness containing 11 wt.% P was formed on the surface of a stainless steel (SUS304) plate by electroplating. The microstructure and joint strength of the brazed joint with the electroplated Ni-11P layer were investigated. The results indicated that the filler metal was homogeneously distributed between the SUS304 plates and no voids or flaws formed in the brazed filler zone. Fe-Ni-Cr solid solutions were formed at the brazed interface. Moreover, P was mainly concentrated in such brazed filler zone to form P-containing phases. The average shear strength of the brazed joints was determined to be 47.3 MPa. The results demonstrated that the brazing of SUS304 plates using the electroplated Ni-11P layer as the filler metal was successfully realized.


2015 ◽  
Vol 1101 ◽  
pp. 99-103
Author(s):  
Cheng Yen Wang ◽  
Ren Kae Shiue

The purpose of this research is focused on vacuum furnace brazing Incoloy 800 (IN-800) using the copper filler foil. Microstructural evolution and shear strength of brazed joints for various brazing conditions has been evaluated in the experiment. The Cu-rich matrix dominates entire brazed joint. The width of Cu-rich matrix is decreased with increasing the brazing temperature and/or time. Average shear strength of the joint is approximately 215 MPa. Dimple dominated fracture is widely observed for the specimen brazed below 1160oC. However, cleavage dominated fracture is found for the specimen brazed at 1200oC. It is advised that copper brazing IN-800 alloy should be confined below 1160oC.


Metals ◽  
2022 ◽  
Vol 12 (1) ◽  
pp. 94
Author(s):  
Yuqing Chen ◽  
Guofeng Wang ◽  
Yongkang Liu ◽  
Liqiang Zhan ◽  
He Diao ◽  
...  

Titanium alloys used to be welded to gain good joint strength at 920 °C through diffusion bonding. However, due to the heat preservation at high temperatures for a long time, we obtain joints with great bond strength while the mechanical properties of the sheet are lost. In this paper, taking Ti6Al4V alloy as an example, we studied the microstructure of the surface under the different times of surface mechanical attrition treatment (SMAT). In addition, the microstructure and mechanical properties after diffusion bonding at 800 °C-5 MPa-1 h were also conducted. The results show that the shear strength of TC4 alloy welded joint after SMAT treatment is improved, and the maximum shear strength can reach 797.7 MPa, up about 32.4%


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