Microstructures and Mechanical Properties of Mg Alloy after Severe Torsion Straining Process

2006 ◽  
Vol 503-504 ◽  
pp. 949-954 ◽  
Author(s):  
Yuichi Miyahara ◽  
N. Emi ◽  
Koji Neishi ◽  
Katsuaki Nakamura ◽  
Kenji Kaneko ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
Grain Refinement ◽  
Room Temperature ◽  
Rotation Speed ◽  
Continuous Process ◽  
Mg Alloy ◽  
Compression Tests ◽  
Moving Speed ◽  
Az61 Mg Alloy

Grain refinement is attempted using severe plastic deformation (SPD) through the severe torsion straining process (STSP) which we have developed recently. The STSP is a continuous process for grain refinement without requirement of any die. In this study, an AZ61 Mg alloy was subjected to STSP at a temperature of 573 K with a rotation speed of 10 rpm and a moving speed of 200 mm/min. With this process, an initial grain size of ~20 μm was reduced to ~2~3 μm. Room temperature compression tests revealed that there were no cracks after 15% of compression for the STSP sample whereas fracture occurred for a conventionally extruded sample. For compression tests at 473 K, no cracks occurred in the STSP samples after 80% compression but compression was feasible without cracking only up to 20% for an extruded sample. It is shown that the STSP can be useful for grain refinement and ductility improvement of the AZ61 Mg alloy.

GRAIN REFINEMENT AND MICROSTRUCTURE EVOLUTION IN ALUMINUM A2618 ALLOY BY HIGH-PRESSURE TORSION

2016 ◽  
Vol 78 (6-9) ◽  
Author(s):  
Intan Fadhlina Mohamed ◽  
Seungwon Lee ◽  
Kaveh Edalati ◽  
Zenji Horita ◽  
Shahrum Abdullah ◽  
...  
Keyword(s):  
Plastic Deformation ◽  
High Pressure ◽  
Grain Refinement ◽  
Room Temperature ◽  
Rotation Speed ◽  
High Pressure Torsion ◽  
Applied Pressure ◽  
Saturation Level ◽  
Microstructural Refinement ◽  
Average Grain Size

This work presents a study related to the grain refinement of an aluminum A2618 alloy achieved by High-Pressure Torsion (HPT) known as a process of Severe Plastic Deformation (SPD). The HPT is conducted on disks of the alloy under an applied pressure of 6 GPa for 1 and 5 turns with a rotation speed of 1 rpm at room temperature. The HPT processing leads to microstructural refinement with an average grain size of ~250 nm at a saturation level after 5 turns. Gradual increases in hardness are observed from the beginning of straining up to a saturation level. This study thus suggests that hardening due to grain refinement is attained by the HPT processing of the A2618 alloy at room temperature.

Grain Refinement of Commercial Al-Mg Alloy Using Severe Torsion Straining Process

2006 ◽  
Vol 503-504 ◽  
pp. 955-960 ◽  
Author(s):  
Koji Neishi ◽  
Akihiko Higashino ◽  
Yuichi Miyahara ◽  
Katsuaki Nakamura ◽  
Kenji Kaneko ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Grain Size ◽  
Cooling Rate ◽  
Grain Refinement ◽  
Rotation Speed ◽  
Imaging System ◽  
Continuous Process ◽  
Critical Ratio ◽  
Heated Zone ◽  
Moving Speed

Severe plastic deformation (SPD) makes it possible to refine grain size in many metallic materials. Recently, we have developed a new SPD process designated the severe torsion straining process (STSP). This process requires no die but one side of a rod is rotated with respect to the other while producing a local heated zone in the rod and cooling both sides of the heated zone. Torsion strain is then introduced in the local heated zone. The STSP can be a continuous process because the rod is moved in the longitudinal direction while introducing torsion strain through the rotation. For grain refinement using the STSP, various factors may affect, which are the rotation speed, moving speed, straining temperature, cooling rate and diameter of the rod. In this study, the STSP is applied to grain refinement of an A5056 Al-Mg commercial alloy and the factors affecting the grain refinement are optimized. STSP was conducted at a temperature in the range from 573K to 723K. Microstructure was observed by optical microscopy, scanning electron microscopy with an orientation imaging system, and transmission electron microscopy. Microscopy observations revealed that the grain size was reduced to ~0.9 μm, when STSP was conducted at 573K with a rotation speed of 10 rpm and moving speed of 50 mm/min. There is a critical ratio of rotation speed to moving speed above which the rod breaks. The grain size tends to be finer as the straining temperature is lower, the cooling rate is faster and the ratio of rotation speed to moving speed is closer to the critical value.

Annealing Study of Al-Mg Wrought Alloys Using Two Different Techniques and Estimation of the Activation Enthalpy of Migrating Defects

2013 ◽  
Vol 337-338 ◽  
pp. 29-37
Author(s):  
Ahmed G. Attallah ◽  
M.A. Abdel-Rahman ◽  
M. El-Sayed ◽  
A.A. Ibhraim ◽  
S.A. Aly ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
Electrical Resistivity ◽  
Annealing Time ◽  
Room Temperature ◽  
Isothermal Annealing ◽  
Activation Enthalpy ◽  
Full Recovery ◽  
Mg Alloy ◽  
Annealing Study

The electrical resistivity and the corresponding mechanical properties (hardness) of some 5xxx Al-Mg alloy processed by plastic deformation were investigated. Plastic deformation was performed at room temperature. Isothermal annealing produced a significant change in both the electrical and mechanical properties of the samples. As the annealing time was increased, the resistivity and hardness up to full recovery. The activation enthalpy of migration of defects was determined, was found to be 0.234±0.06 eV, 0.218±0.049 eV, 0.316±0.016 eV 0.232±0.012 eV for 5005, 5251, 5052 and 5754 alloys, respectively.

Investigations on Microstructure Evolution and Deformation Behavior of Aged and Ultrafine Grained Al-Zn-Mg Alloy Subjected to Severe Plastic Deformation

2010 ◽  
Vol 667-669 ◽  
pp. 253-258
Author(s):  
Wei Ping Hu ◽  
Si Yuan Zhang ◽  
Xiao Yu He ◽  
Zhen Yang Liu ◽  
Rolf Berghammer ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Plastic Deformation ◽  
Grain Size ◽  
Severe Plastic Deformation ◽  
Microstructure Evolution ◽  
Deformation Behavior ◽  
Deformation Mechanisms ◽  
Mg Alloy ◽  
Ultrafine Grained

An aged Al-5Zn-1.6Mg alloy with fine η' precipitates was grain refined to ~100 nm grain size by severe plastic deformation (SPD). Microstructure evolution during SPD and mechanical behaviour after SPD of the alloy were characterized by electron microscopy and tensile, compression as well as nanoindentation tests. The influence of η' precipitates on microstructure and mechanical properties of ultrafine grained Al-Zn-Mg alloy is discussed with respect to their effect on dislocation configurations and deformation mechanisms during processing of the alloy.

scholarly journals Effect of Grain Refinement on the Dynamic, Mechanical Properties, and Corrosion Behaviour of Al-Mg Alloy

Metals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1825
Author(s):  
Haitham M. Ahmed ◽  
Hussin A. M. Ahmed ◽  
Mohammed Hefni ◽  
Essam B. Moustafa
Keyword(s):  
Mechanical Properties ◽  
Grain Refinement ◽  
Corrosion Behaviour ◽  
Cast Alloy ◽  
Dynamic Properties ◽  
Damping Ratio ◽  
Xrd Analysis ◽  
Optical Microscope ◽  
Mg Alloy ◽  
Resonance Frequencies

In this investigation, aluminium Al-2.5% Mg cast alloy was modified by adding 0.5 Ti and 0.1 B wt % modifiers to investigate their impact on the dynamic behaviour, as well as the mechanical and microstructure properties. The dynamic properties were analysed experimentally using a free vibration impact test and predicted using finite element methods. This study used a high-resolution polarised optical microscope to analyse the microstructure of the studied alloys and X-ray Powder Diffraction (XRD) analysis to determine the developed phases. Microstructure and mechanical properties were mostly enhanced as a result of grain refining during solidification and through the metal segregation process. The microstructure analysis of the modified alloy showed a significant improvement in the grain refinement; hence, the grains were 10 times finer than the cast alloy. The modified Al-2.5% Mg/Ti-B alloy demonstrated reduced inter-granular corrosion (IGC) than the Al-2.5% Mg standard cast alloy. By incorporating Ti-B modifiers into the composition of the cast Al-Mg alloy, the ultimate tensile strength (UTS), strain (ε), and hardness values (HV) were increased by 30.5%, 100%, and 18.18%, respectively. The dynamic properties of the modified alloy showed an enhancement in the resonant (fn) and damping ratio (ζ) by 7% and 68%, respectively. The predicted resonance frequencies of the investigated alloys showed results close to the experimental dynamic tests.

scholarly journals Low-temperature degradation resistance and plastic deformation of ATZ ceramics stabilized by CaO

2021 ◽  
Vol 2103 (1) ◽  
pp. 012075
Author(s):  
AA Dmitrievskiy ◽  
DG Zhigacheva ◽  
VM Vasyukov ◽  
PN Ovchinnikov
Keyword(s):  
Mechanical Properties ◽  
Fracture Toughness ◽  
Plastic Deformation ◽  
Compressive Strength ◽  
Phase Composition ◽  
Low Temperature ◽  
Uniaxial Compression ◽  
Calcium Oxide ◽  
Tetragonal Phase ◽  
Room Temperature

Abstract In this work, the phase composition (relative fractions of monoclinic m-ZrO2, tetragonal t-ZrO2, and cubic c-ZrO2 phases) and mechanical properties (hardness, fracture toughness, compressive strength) of alumina toughened zirconia (ATZ) ceramics, with an addition of silica were investigated. Calcium oxide was used as a stabilizer for the zirconia tetragonal phase. It was shown that CaO-ATZ+SiO2 ceramics demonstrate increased resistance to low-temperature degradation. The plasticity signs at room temperature were found due to the SiO2 addition to CaO-ATZ ceramics. A yield plateau appears in the uniaxial compression diagram at 5 mol. % SiO2 concentration. It is hypothesized that discovered plasticity is due to the increased t→m transformability.

Superplasticity of Aerospace 7075 (Al-Zn-Mg-Cu) Aluminium Alloy Obtained by Severe Plastic Deformation

2018 ◽  
Vol 385 ◽  
pp. 39-44 ◽  
Author(s):  
Fernando Carreño ◽  
Oscar A. Ruano
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
Severe Plastic Deformation ◽  
Aluminium Alloy ◽  
Room Temperature ◽  
Grain Boundary Sliding ◽  
Strain Rates ◽  
Aerospace Applications ◽  
Boundary Sliding ◽  
Processing Stress

The 7075 (Al-Zn-Mg-Cu) aluminium alloy is the reference alloy for aerospace applications due to its specific mechanical properties at room temperature, showing excellent tensile strength and sufficient ductility. Formability at high temperature can be improved by obtaining superplasticity as a result of fine, equiaxed and highly misoriented grains prone to deform by grain boundary sliding (GBS). Different severe plastic deformation (SPD) processing routes such as ECAP, ARB, HPT and FSP have been considered and their effect on mechanical properties, especially at intermediate to high temperatures, are studied. Refined grains as fine as 100 nm and average misorientations as high as 39o allow attainment of high strain rate superplasticity (HSRSP) at lower than usual temperatures (250-300oC). It is shown that increasing misorientations are obtained with increasing applied strain, and increasing grain refinement is obtained with increasing processing stress. Thus, increasing superplastic strains at higher strain rates, lower stresses and lower temperatures are obtained with increasing processing strain and, specially, processing stress.

Microstructures and Mechanical Properties of Solid-State Welded Steels

2021 ◽  
Vol 21 (9) ◽  
pp. 4877-4880
Author(s):  
Gyeong Woo Kim ◽  
Se Min Jeong
Keyword(s):  
Mechanical Properties ◽  
Solid State ◽  
Grain Refinement ◽  
Friction Welding ◽  
Vickers Microhardness ◽  
Rotation Speed ◽  
Base Material ◽  
Tensile Specimen ◽  
Refined Grains ◽  
Microstructures And Mechanical Properties

This study aimed to evaluate the soundness of solid-state welded steels. STS 430F alloy with a rod type was selected as experimental material, and the friction welding was conducted at a rotation speed of 2,000 RPM and upset length of 3 mm. The application of friction welding on STS 430F rods led to significant grain refinement in the welded zone (1.3 µm) compared to that observed in the base material (16.8 µm). The refined grains in the welds contributed to the development of the mechanical properties. In particular, the Vickers microhardness was increased by approximately 25% compared to the base material, and the fracture at the tensile specimen of the welds occurred at the base material zone and not in the welded zone, which suggests a soundly welded state on the STS 430F rods.

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