Effects of Microstructural Morphology on Mechanical Properties of Magnesium Alloys

2011 ◽  
Vol 686 ◽  
pp. 113-119
Author(s):  
Jing Yuan Li ◽  
Xiao Lei Du
Keyword(s):  
Mechanical Properties ◽  
Magnesium Alloys ◽  
Cross Section ◽  
High Strength ◽  
Second Phase ◽  
Al Content ◽  
Uniform Microstructure ◽  
Zn Content ◽  
Microstructural Morphology ◽  
The Difference

The mechanical property of magnesium alloy depends on the alloy elements and microstructure strongly. The multiple dependency relations are studied by investigating magnesium alloys with different Al and Zn contents. The semi-continuous casting billets exhibit quite different microstructural morphologies between the centre and edge of the cross section. The centre shows fine and uniform microstructure while the edge is coarse and reticular. However the difference is almost eliminated when the billets were homogenized at 380°C for 15h. The generation mechanism of casting microstructure is also discussed in this paper. The results show that the morphology of second phase and the size of grain have greater effect on the mechanical properties than the element Zn. The alloys with uniform, fine and non-dendrite microstructure exhibit both high strength and elongation when Al content is about 6% and Zn content is various from 0 to 3%. In contrast, the strength increases and elongation decreases significantly as Al content increases from 0 to 6%.

Effects of Al and Zn on the Microstructure and Mechanical Properties of Magnesium Alloys

2010 ◽  
Vol 97-101 ◽  
pp. 801-804
Author(s):  
Jing Yuan Li ◽  
Xiao Lei Du
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Yield Strength ◽  
Magnesium Alloys ◽  
High Strength ◽  
Al Content ◽  
Zn Content ◽  
Cast Magnesium Alloys ◽  
Cast Magnesium ◽  
Peak Value

Two groups of magnesium alloys with various Al and Zn components are studied in this paper. One group of alloys are constant Al content of about 6% and various Zn content from 0 to 3%, another group are constant Zn content of about 0.4% and various Al content from 0 to 6%. The microstructures and mechanical properties of these alloys are investigated in as-cast and homogenized at 380°C for 15h. The results show that the tensile strength increases but yield strength decreases after homogenizing treatment. It can also be found that the morphology of second phrase and the size of grain exert the more effect on the mechanical properties than Zn content does. The alloys with uniform, fine and non-dendrite microstructure exhibit both high strength and elongation regardless of Zn content. On the other hand, the tensile strength and yield strength elevate significantly as Al content increases, and the elongation has a peak value in Al content of about 1.90%. The results show that the as-cast magnesium alloys with Al content of 5.6~6.0% and Zn content of 0.6~1.0% exhibit the best comprehensive mechanical properties.

Microstructural Refinement in a Commercial Aluminum Alloy Processed by ECAP Using a Die Channel Angle of 110 Degrees

2015 ◽  
Vol 1114 ◽  
pp. 3-8
Author(s):  
Nicolae Şerban ◽  
Doina Răducanu ◽  
Nicolae Ghiban ◽  
Vasile Dănuţ Cojocaru
Keyword(s):  
Grain Refinement ◽  
Cross Section ◽  
High Strength ◽  
Secondary Phase ◽  
Coarse Grained ◽  
Metallographic Analysis ◽  
Second Phase ◽  
Channel Angle ◽  
Ambient Temperatures ◽  
Fine Grained

The properties of ultra-fine grained materials are superior to those of corresponding conventional coarse grained materials, being significantly improved as a result of grain refinement. Equal channel angular pressing (ECAP) is an efficient method for modifying the microstructure by refining grain size via severe plastic deformation (SPD) in producing ultra-fine grained materials (UFG) and nanomaterials (NM). The grain sizes produced by ECAP processing are typically in the submicrometer range and this leads to high strength at ambient temperatures. ECAP is performed by pressing test samples through a die containing two channels, equal in cross-section and intersecting at a certain angle. The billet experiences simple shear deformation at the intersection, without any precipitous change in the cross-section area because the die prevents lateral expansion and therefore the billet can be pressed more than once and it can be rotated around its pressing axis during subsequent passes. After ECAP significant grain refinement occurs together with dislocation strengthening, resulting in a considerable enhancement in the strength of the alloys. A commercial AlMgSi alloy (AA6063) was investigated in this study. The specimens were processed for a number of passes up to nine, using a die channel angle of 110°, applying the ECAP route BC. After ECAP, samples were cut from each specimen and prepared for metallographic analysis. The microstructure of the ECAP-ed and as-received material was investigated using optical (OLYMPUS – BX60M) and SEM microscopy (TESCAN VEGA II – XMU). It was determined that for the as-received material the microstructure shows a rough appearance, with large grains of dendritic or seaweed aspect and with a secondary phase at grain boundaries (continuous casting structure). For the ECAP processed samples, the microstructure shows a finished aspect, with refined, elongated grains, also with crumbled and uniformly distributed second phase particles after a typical ECAP texture.

Comparison of As-Cast Microstructures and Mechanical Properties for Mg-Ce-Mn-Sc and Mg-Ce-Mn-Zn Magnesium Alloys

2009 ◽  
Vol 610-613 ◽  
pp. 746-749 ◽  
Author(s):  
Jia Shen ◽  
Ming Bo Yang ◽  
Fu Sheng Pan ◽  
Ren Ju Cheng
Keyword(s):  
Mechanical Properties ◽  
Magnesium Alloys ◽  
Creep Properties ◽  
Microstructures And Mechanical Properties ◽  
The Difference ◽  
Cast Microstructure

The as-cast microstructures and mechanical properties of Mg-3Ce-1.2Mn-0.9Sc and Mg-3Ce-1.2Mn-1Zn magnesium alloys were investigated and compared. The results indicate that the as-cast microstructure of Mg-3Ce-1.2Mn-0.9Sc alloy was mainly composed of -Mg, Mg12Ce and Mn2Sc phases, and that the as-cast microstructure of Mg-3Ce-1.2Mn-1Zn alloy was mainly composed of -Mg, Mg12Ce and MgZn phases. In addition, the as-cast tensile and creep properties of Mg-3Ce-1.2Mn-0.9Sc alloy were higher than that of the Mg-3Ce-1.2Mn-1Zn alloy. The difference of the two alloys in as-cast tensile and creep properties may be related to the initial microstructures of the two alloys.

Development of a High Strength Mg-Zn-Y-Zr Wrought Alloy

2007 ◽  
Vol 539-543 ◽  
pp. 1701-1706
Author(s):  
Rong Shi Chen ◽  
Wei Neng Tang ◽  
Dao Kui Xu ◽  
En Hou Han
Keyword(s):  
Mechanical Properties ◽  
High Temperature ◽  
Fatigue Life ◽  
Deformation Behavior ◽  
Fatigue Behavior ◽  
High Strength ◽  
Zn Content ◽  
High Fatigue ◽  
Content Range ◽  
Zr Alloy

The effects of Y addition to the Mg-Zn-Y-Zr alloy on the change of the microstructure and the mechanical properties (with the Y content range of 1 to 3 wt%) have been investigated. It shows that when Zn content is constant (5.65wt%), the alloys with Y content between 1.17 and 1.72wt% nearly reach its highest strength. With the composition near the optimums, the extruded Mg-6%Zn-1%Y-Zr alloy shows high strength and excellent ductility. The deformation behavior of this new alloy at high temperature has also been studied. Moreover, the super-long fatigue behavior of the Mg-6%Zn-1%Y-Zr alloy has also been tested, the results show the alloy with a high fatigue strength of about 85-90MPa in the super-long fatigue life regime of 1×109 cycles.

scholarly journals Effect of Zn Content on the Microstructure and Mechanical Properties of Mg–Al–Sn–Mn Alloys

Materials ◽  
2019 ◽  
Vol 12 (19) ◽  
pp. 3102
Author(s):  
Tianshuo Zhao ◽  
Yaobo Hu ◽  
Fusheng Pan ◽  
Bing He ◽  
Maosheng Guan ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
High Performance ◽  
Dendritic Structure ◽  
Second Phase ◽  
Microstructure And Mechanical Properties ◽  
Zn Content ◽  
Dislocation Movement ◽  
Cast Alloys ◽  
Complete Recrystallization ◽  
Second Phases

High performance Mg–6Al–3Sn–0.25Mn–xZn alloys (x = 0, 0.5, 1.0, 1.5, and 2.0 wt %) without rare earth were designed. The effects of different Zn contents on the microstructure and mechanical properties were systematically investigated. The addition of Zn obviously refines the as-cast alloys dendritic structure because of the increase in the number in the second phase. For the as-extruded alloys, an appropriate amount of Zn promotes complete recrystallization, thus increasing the grain size. As the Zn content increases, the texture gradually evolves into a typical strong basal texture, which means that the basal slip is difficult to initiate. Meanwhile, the addition of Zn promotes the precipitation of small-sized second phases, which can hinder the dislocation movement. The combination of texture strengthening and precipitation strengthening is the main reason for the improvement of alloys’ strength.

scholarly journals Alloying and Processing Effects on the Microstructure, Mechanical Properties, and Degradation Behavior of Extruded Magnesium Alloys Containing Calcium, Cerium, or Silver

Materials ◽  
2020 ◽  
Vol 13 (2) ◽  
pp. 391 ◽  
Author(s):  
Jan Bohlen ◽  
Sebastian Meyer ◽  
Björn Wiese ◽  
Bérengère J. C. Luthringer-Feyerabend ◽  
Regine Willumeit-Römer ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Magnesium Alloys ◽  
Processing Parameters ◽  
Second Phase ◽  
Degradation Behavior ◽  
Microstructure Development ◽  
Corrosion Properties ◽  
Second Phase Particles ◽  
Degradation Rates ◽  
The Relationship

Magnesium alloys attract attention as degradable implant materials due to their adjustable corrosion properties and biocompatibility. In the last few decades, especially wrought magnesium alloys with enhanced mechanical properties have been developed, with the main aim of increasing ductility and formability. Alloying and processing studies allowed demonstrating the relationship between the processing and the microstructure development for many new magnesium alloys. Based on this experience, magnesium alloy compositions need adjustment to elements improving mechanical properties while being suitable for biomaterial applications. In this work, magnesium alloys from two Mg-Zn series with Ce (ZE) or Ca (ZX) as additional elements and a series of alloys with Ag and Ca (QX) as alloying elements are suggested. The microstructure development was studied after the extrusion of round bars with varied processing parameters and was related to the mechanical properties and the degradation behavior of the alloys. Grain refinement and texture weakening mechanisms could be improved based on the alloy composition for enhancing the mechanical properties. Degradation rates largely depended on the nature of second phase particles rather than on the grain size, but remained suitable for biological applications. Furthermore, all alloy compositions exhibited promising cytocompatibility.

Research of reinforcement phase formation on the borders of sintered berillium grains

2020 ◽  
pp. 25-33
Author(s):  
A. V. Revutsky ◽  
V. Yu. Syrnev ◽  
V. Yu. Lopatin ◽  
O. V. Semilutskaya ◽  
T. A. Segeda
Keyword(s):  
Mechanical Properties ◽  
Grain Boundaries ◽  
High Strength ◽  
Beryllium Oxide ◽  
Research Problem ◽  
Strength Properties ◽  
Reinforcing Particles ◽  
Morphology And Structure ◽  
The Difference ◽  
Devitrification Mechanism

The paper presents the results of studying the effect of the state of grain boundaries (formed in the consolidation of beryllium powders by vacuum hot pressing on the strength properties of sintered beryllium. Scanning electron microscopy and X-ray spectral microanalysis were used to study the dependences of the morphology, elemental composition and structure of a dispersion hardening phase - beryllium oxide – on the content of low-melting impurities at the grain boundaries of sintered beryllium. A new hypothesis is proposed to explain the difference in the morphology and structure of reinforcing particles based on the transition features of amorphous beryllium oxide to a crystalline state (devitrification) at the grain boundaries of metallic beryllium. It is theoretically substantiated and experimentally confirmed that the devitrification mechanism can be homogeneous or heterogeneous depending on the content and ratio of silicon and aluminum impurities. This difference leads to the formation of either finely dispersed high-strength reinforcing particles of beryllium oxide or large, lower-strength oxide clusters. Changes in the morphology and structure of reinforcing oxide particles at the metallic beryllium grain boundaries, in its turn, influence the dynamics of beryllium microstructure grain growth during vacuum hot forming and, ultimately, the effect of dispersed grain-boundary hardening of sintered n beryllium. The paper provides the statistically processed results of testing the mechanical properties of industrial hot-pressed blanks produced of less than 56 μm powders to determine the effect of various factors (the content of impurities, their ratio and particle size of the initial powders) on the strength properties of hot-pressed beryllium. The adequacy of the obtained regularities was evaluated using the approximation confidence coefficients and confirmed the conclusions made in the theoretical and experimental analysis of the research problem. The statistical studies substantiated a comprehensive quality indicator of initial powders in order to predict the strength properties of hot-pressed beryllium. The results obtained substantiate new possibilities for controlling the mechanical properties of sintered beryllium for various purposes.

Effect of Casting Method and Al Contents on Microstructure in AM-Type Magnesium Alloys

2010 ◽  
Vol 654-656 ◽  
pp. 663-666 ◽  
Author(s):  
Katsumi Watanabe ◽  
Kenji Matsuda ◽  
Takumi Gonoji ◽  
Tokimasa Kawabata ◽  
Katsuya Sakakibara ◽  
...  
Keyword(s):  
Magnesium Alloys ◽  
Hardness Test ◽  
Al Alloys ◽  
Age Hardening ◽  
Casting Method ◽  
Absorption Properties ◽  
Al Content ◽  
Hardening Behavior ◽  
The Difference ◽  
Impact Absorption

Magnesium alloys have received considerable attention because of their lightweight and recyclability. AM-type and AZ-type Mg-Al alloys have been used for industrial products widely, particularly for AM-type alloys because of the better toughness and impact absorption properties than AZ-type alloys. However, there is little report about the effect of casting method on age-hardening behavior and microstructure of AM-type alloys. The purpose of this study is to investigate the difference of the age-hardening behavior and microstructures of three AM-type alloys cast with steel, copper and sand molds using hardness test and scanning electron microscopy (SEM) observation. Furthermore, the effect of Al content is also investigated in this study using three alloys of AM30 (3%Al), AM60 (6%Al) and AM90 (9%Al).

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