Evolution of Microstructure during Hot Deformation of Pearlitic Steel

2013 ◽  
Vol 753 ◽  
pp. 459-462
Author(s):  
Rama Krushna Sabat ◽  
Sajal Hatwal ◽  
Bharath Dixit ◽  
Satyam Suwas
Keyword(s):  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Texture Evolution ◽  
Pearlitic Steel ◽  
Strain Rates ◽  
Compression Tests ◽  
Flow Curves ◽  
X Ray ◽  
Deformation Response ◽  
Evolution Of Microstructure

Hot deformation of pearlitic steel was carried out to examine the overall deformation response to micro structural and texture evolution. To understand the mechanisms operative during hot deformation, compression tests were carried out at various temperatures in the range 400 - 600o C and strain rates in the range 0.001-10 s-1. The flow curves were analyzed to examine the occurrence of dynamic recrystallization. The evolution of microstructure and texture of hot deformed sample is analysed using EBSD and X-ray texture goniometer respectively.

Characteristics of Dynamic Recrystallization during Hot Deformation for High Nitrogen Stainless Steels

2012 ◽  
Vol 715-716 ◽  
pp. 115-121
Author(s):  
Hai Wen Luo ◽  
Xu Dong Fang ◽  
Rui Zhen Wang ◽  
Zhan Yin Diao
Keyword(s):  
Dynamic Recrystallization ◽  
Stainless Steels ◽  
Hot Deformation ◽  
Strain Rates ◽  
Peak Strain ◽  
High Nitrogen ◽  
Flow Curves ◽  
Grain Sizes ◽  
Nitrogen Contents ◽  
High Nitrogen Stainless Steel

Dynamic recrystallization was studied for the stainless steels with nitrogen contents of 0.56% to 1.08% during hot deformation at temperatures of 900~1200 with strain rates ranging from 0.003 to 42 s-1. It was found that flow stress could increase remarkably with increasing nitrogen content. Flow curves during the deformation by 0.1~42/s at temperatures of 900~1200°C show a single peak, indicating the occurrence of dynamic recrystallization during deformation. The peak strain seems to decrease with increasing N content, suggesting that higher content of N facilitates dynamic recrystallization. The quenched microstructures were analyzed by optical microscopy, EBSD and TEM. The recrystallized grain sizes on the quenched specimens were measured and its dependence on temperature and strain rate was analyzed. At high temperature, continuously dynamically recrystallized microstructures were observed; whilst at low temperature, necklace-like partially recrystallized microstructures were found. Key words: High nitrogen stainless steel; dynamic recrystallization; stress-strain curves

scholarly journals Hot Deformation Behavior of a Ni-Based Superalloy with Suppressed Precipitation

Metals ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 605
Author(s):  
Franco Lizzi ◽  
Kashyap Pradeep ◽  
Aleksandar Stanojevic ◽  
Silvana Sommadossi ◽  
Maria Cecilia Poletti
Keyword(s):  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Hot Deformation ◽  
Strain Rates ◽  
Compression Tests ◽  
Deformation Bands ◽  
Stress Softening ◽  
Relative Stress ◽  
The Matrix ◽  
Thermomechanical Processes

Inconel®718 is a well-known nickel-based super-alloy used for high-temperature applications after thermomechanical processes followed by heat treatments. This work describes the evolution of the microstructure and the stresses during hot deformation of a prototype alloy named IN718WP produced by powder metallurgy with similar chemical composition to the matrix of Inconel®718. Compression tests were performed by the thermomechanical simulator Gleeble®3800 in a temperature range from 900 to 1025 °C, and strain rates scaled from 0.001 to 10 s−1. Flow curves of IN718WP showed similar features to those of Inconel®718. The relative stress softening of the IN718WP was comparable to standard alloy Inconel®718 for the highest strain rates. Large stress softening at low strain rates may be related to two phenomena: the fast recrystallization rate, and the coarsening of micropores driven by diffusion. Dynamic recrystallization grade and grain size were quantified using metallography. The recrystallization grade increased as the strain rate decreased, although showed less dependency on the temperature. Dynamic recrystallization occurred after the formation of deformation bands at strain rates above 0.1 s−1 and after the formation of subgrains when deforming at low strain rates. Recrystallized grains had a large number of sigma 3 boundaries, and their percentage increased with strain rate and temperature. The calculated apparent activation energy and strain rate exponent value were similar to those found for Inconel®718 when deforming above the solvus temperature.

Kinetics of Dynamic Recrystallization of 18 Ni Maraging Steels

2016 ◽  
Vol 850 ◽  
pp. 13-20 ◽  
Author(s):  
Ni Li ◽  
Fei Zhao ◽  
Huan Zhang ◽  
Yong Hai Ren
Keyword(s):  
Dynamic Recrystallization ◽  
Peak Stress ◽  
Strain Rates ◽  
Recrystallization Behavior ◽  
Compression Tests ◽  
Flow Curves ◽  
Maraging Steels ◽  
Dynamic Recrystallization Behavior ◽  
Characteristic Values ◽  
Kinetics Of

The dynamic recrystallization behavior of 18 Ni maraging steels was investigated by hot compression tests at temperatures ranging from 900 °C to 1100 °C and strain rates ranging from 0.001 to 1 s-1. Based on the flow curves from the tests, the effects of temperatures and strain rates on the dynamic recrystallization behavior were analyzed. The strain-hardening rates versus stress curves were used to determine to the critical strain, the peak stress (strain), the saturated stress and the steady stress. With the assistance of the process parameters, constitutive equations were obtained and the activation energy was determined to be 413544.96 J/mol. The dependence of the characteristic values on Zener-Hollomon was found. The dynamic recrystallization kinetics model of the tested steels was constructed and the validity was confirmed based on the experimental results.

scholarly journals Hot Deformation Behavior and Processing Maps of Fe-30Mn-0.11C Steel

Materials ◽  
2018 ◽  
Vol 11 (10) ◽  
pp. 1940 ◽  
Author(s):  
Jianmei Kang ◽  
Yuhui Wang ◽  
Zhimeng Wang ◽  
Yiming Zhao ◽  
Yan Peng ◽  
...  
Keyword(s):  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Deformation Behavior ◽  
True Strain ◽  
Peak Stress ◽  
Strain Rates ◽  
Processing Maps ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
High Deformation

Hot deformation behavior of Fe-30Mn-0.11C steel was investigated. Hot compression tests were carried out at various temperatures ranging from 800 °C to 1200 °C and at different strain rates of 0.01 s−1 to 10 s−1. The constitutive equation based on peak stress was established. Hot processing maps at different strains and recrystallization diagrams were also established and analyzed. The results show that dynamic recrystallization easily occur at high deformation temperatures and low strain rates. Safe and unstable zones are determined at the true strain of 0.6 and 0.7, and the hot deformation process parameters of partial dynamic recrystallization of the tested steel are also obtained.

The effects of temperature and strain rate on the hot deformation behavior of AISI H10 tool steel

2020 ◽  
Vol 118 (1) ◽  
pp. 107
Author(s):  
Maryam Kamali Ardakani ◽  
Maryam Morakabati
Keyword(s):  
Grain Size ◽  
Dynamic Recrystallization ◽  
Strain Rate ◽  
Tool Steel ◽  
Hot Deformation ◽  
Deformation Behavior ◽  
Strain Rates ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
Temperature Range

The hot deformation behavior of a H10 hot work tool steel was studied by performing hot compression tests over the temperature range of 900 to 1200 °C and strain rates of 0.001–1 s−1 and total strain of 0.7. At temperatures below 1100 °C, the grain size is fine and below 20 μm. In this temperature range, grain size increase with temperature due to dissolution of carbides. Then by increasing temperature to 1150 and 1200 °C, the grain size is increased significantly due to growth of grains. The study on the effect of strain rate showed that at constant temperature of 1000 °C, the grain size increased from 4.8 to 6 μm with increasing strain rate from 0.001 to 1 s−1. Also, this increase in the strain rate at temperature of 1100 °C lead to increase the grain size from 5.9 to 17 μm, due to the occurrence of dynamic recrystallization. At 1200 °C growth of grains causes to decrease grain size from 112 to 87 μm by increasing strain rate. According to the microstructural investigations, at the temperatures of 1000 and 1100 °C and strain rates of 0.01 and 0.1 s−1 dynamic recrystallization was the main softening mechanism. As a result, the most suitable range for hot deformation was obtained at the temperature range of 1000–1100 °C and strain rates of 0.01–0.1 s−1.

Dynamic Recrystallization Behaviour of Twin Roll Cast AZ31 Strips during Hot Deformation

2014 ◽  
Vol 622-623 ◽  
pp. 569-574 ◽  
Author(s):  
Madlen Ullmann ◽  
Matthias Schmidtchen ◽  
Rudolf Kawalla
Keyword(s):  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Volume Fraction ◽  
Az31 Alloy ◽  
Rolling Process ◽  
Recrystallization Process ◽  
Strain Rates ◽  
Compression Tests ◽  
Twin Roll Cast ◽  
Twin Roll

The recrystallization behaviour of a Twin Roll Cast AZ31 alloy, under deformation conditions corresponding to the initial stands of a magnesium hot rolling process, has been investigated. A set of strain levels, beginning at the critical strain for the onset of dynamic recrystallization has been studied. The dynamic recrystallization, taking place during hot deformation of magnesium alloy AZ31 is analyzed with help of plane strain compression tests conducted together with microscopic examination. Dynamically recrystallized volume fraction and size of dynamically recrystallized grains increase with increasing strain. When the strain is constant, the dynamically recrystallized volume fraction is higher at higher deformation temperatures or lower strain rates. Furthermore, it has been found out that deformation temperature plays a major role, rather than strain rates, in activating the dynamic recrystallization process during deformation. The results were used to identify the coefficients for the JMAK-model approach on the dynamic recrystallization of an AZ31 TRC-sheet.

scholarly journals Investigation into Microstructure Evolution of Co–Ni–Cr–W–Based Superalloy During Hot Deformation

2021 ◽  
Vol 8 ◽  
Author(s):  
Wei Zhang ◽  
Baohong Zhu ◽  
Shuaishuai Wu ◽  
Shutian Tao
Keyword(s):  
Dynamic Recrystallization ◽  
Microstructure Evolution ◽  
Hot Deformation ◽  
Electron Backscatter Diffraction ◽  
Strain Rates ◽  
Compression Tests ◽  
Continuous Dynamic Recrystallization ◽  
Nucleation Mechanisms ◽  
Ebsd Technique ◽  
Continuous Dynamic

Hot compression tests were conducted using a Gleeble 3500 thermomechanical simulator at temperatures ranging from 1,000 to 1,200°C with the strain rate ranging from 0.1 to 10 s−1. Electron backscatter diffraction (EBSD) technique was employed by investigating the microstructure evolution during hot deformation. Microstructure observations reveal that deformation temperatures and strain rates have a significant effect on the DRX process. It is found that the fraction and grain size of DRX increase with the decreasing deformation temperature, along with the increasing high-angle grain boundaries (HAGBs). The fraction of DRX first decreases and then increases with the increase of strain rates. It is noted that there are both the nucleation mechanisms of discontinuous dynamic recrystallization (DDRX) and continuous dynamic recrystallization (CDRX) during the DRX process for Co–Ni–Cr–W–based superalloys. DDRX and CDRX are the primary and subsidiary nucleation mechanisms of DRX, respectively. It is also found that deformation temperatures and strain rates have almost no effect on the primary and subsidiary nucleation mechanisms of DRX. At the temperature above 1,150°C, the complete DRX occurred with the average grain sizes of about 25.32–29.01 μm. The homogeneity and refinement of microstructure can be obtained by selecting the suitable hot deformation parameters.

Study on Hot Deformation Behavior of Cast-and-Homogenized Superalloy GH706

2015 ◽  
Vol 816 ◽  
pp. 648-654
Author(s):  
Yan Hui Yang ◽  
Dong Liu ◽  
Jian Bing Peng ◽  
Jian Guo Wang ◽  
Guo Wei Liu ◽  
...  
Keyword(s):  
Experimental Data ◽  
Hot Deformation ◽  
Deformation Behavior ◽  
Linear Regression Analysis ◽  
Constitutive Relationship ◽  
Strain Rates ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
Flow Curves ◽  
Relationship Of

Hot deformation behavior of cast-and-homogenized GH706-ingot material was studied in this work. Isothermal uniaxial compression tests were performed at temperatures (°C): 990, 1020, 1050, 1080 and 1100 with strain rates (s-1): 0.01, 0.1 and 1. The stress-strain curves as well as changes in microstructures of various hot deformed specimens were analyzed. Inhomogeneous microstructures were found in the specimens and the flow curves were resulted from the comprehensive functions of microstructures change in all part of the specimens. The constitutive relationship of alloy GH706 has been established by linear regression analysis of the experimental data taken from the Arrhenius equations as a model. Then hot compression tests were carried out to estimate the allowable reductions, and 52.5% and 50.6% are suggested as the allowable reductions during cogging processing of GH706 alloy in each blow at 1110°C and 1130°C.

scholarly journals Effect of Trace Magnesium Additions on the Dynamic Recrystallization in Cast Alloy 825 after One-Hit Hot-Deformation

Metals ◽  
2020 ◽  
Vol 11 (1) ◽  
pp. 36
Author(s):  
Munir Al-Saadi ◽  
Wangzhong Mu ◽  
Christopher N. Hulme-Smith ◽  
Fredrik Sandberg ◽  
Pär G. Jönsson
Keyword(s):  
Service Life ◽  
Dynamic Recrystallization ◽  
Hot Deformation ◽  
Cast Alloy ◽  
True Strain ◽  
Peak Strain ◽  
Compression Tests ◽  
Electron Backscattered Diffraction ◽  
Hollomon Parameter ◽  
Test Conditions

Alloy 825 is widely used in several industries, but its useful service life is limited by both mechanical properties and corrosion resistance. The current work explores the effect of the addition of magnesium on the recrystallization and mechanical behavior of alloy 825 under hot compression. Compression tests were performed under conditions representative of typical forming processes: temperatures between 1100 and 1250 °C and at strain rates of 0.1–10 s−1 to a true strain of 0.7. Microstructural evolution was characterized by electron backscattered diffraction. Dynamic recrystallization was found to be more prevalent under all test conditions in samples containing magnesium, but not in all cases of conventional alloy 825. The texture direction ⟨101⟩ was the dominant orientation parallel to the longitudinal direction of casting (also the direction in which the samples were compressed) in samples that contained magnesium under all test conditions, but not in any sample that did not contain magnesium. For all deformation conditions, the peak stress was approximately 10% lower in material with the addition of magnesium. Furthermore, the differences in the peak strain between different temperatures are approximately 85% smaller if magnesium is present. The average activation energy for hot deformation was calculated to be 430 kJ mol−1 with the addition of magnesium and 450 kJ mol−1 without magnesium. The average size of dynamically recrystallized grains in both alloys showed a power law relation with the Zener–Hollomon parameter, DD~Z−n, and the exponent of value, n, is found to be 0.12. These results can be used to design optimized compositions and thermomechanical treatments of alloy 825 to maximize the useful service life under current service conditions. No experiments were conducted to investigate the effects of such changes on the service life and such experiments should now be performed.

Constitutive Equation for 3104 Alloy at High Temperatures in Consideration of Strain

2016 ◽  
Vol 35 (6) ◽  
pp. 599-605 ◽  
Author(s):  
Fuqiang Zhen ◽  
Jianlin Sun ◽  
Jian Li
Keyword(s):  
Hot Deformation ◽  
Flow Behavior ◽  
Temperature Correction ◽  
Strain Rates ◽  
Compression Tests ◽  
Hot Deformation Behavior ◽  
Element Analysis ◽  
Hollomon Parameter ◽  
The Finite Element Analysis ◽  
Effects Of Temperature

AbstractThe flow behavior of 3104 aluminum alloy was investigated at temperatures ranging from 250°C to 500°C, and strain rates from 0.01 to 10 s−1 by isothermal compression tests. The true stress–strain curves were obtained from the measured load–stroke data and then modified by friction and temperature correction. The effects of temperature and strain rate on hot deformation behavior were represented by Zener–Hollomon parameter including Arrhenius term. Additionally, the influence of strain was incorporated considering the effect of strain on material constants. The derived constitution equation was applied to the finite element analysis of hot compression. The results show that the simulated force is consistent with the measured one. Consequently, the developed constitution equation is valid and feasible for numerical simulation in hot deformation process of 3104 alloy.

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