Study of Texture in 6016 Aluminum Alloy during Processing

2016 ◽  
Vol 877 ◽  
pp. 356-362
Author(s):  
Zhang Wen ◽  
Ying Ying Liu ◽  
Zhi Hong Jia ◽  
Pi Zhi Zhao ◽  
Zhi Qing Zhang ◽  
...  
Keyword(s):  
Cold Rolling ◽  
Shear Bands ◽  
Deformation Texture ◽  
Continuous Annealing ◽  
Intermediate Annealing ◽  
X Ray Diffraction ◽  
6016 Aluminum Alloy ◽  
Cold Rolled ◽  
Hot Rolled ◽  
Rolled Plates

The evolution of texture in AA6016 alloy during processing was systematically investigated. The hot-rolled 6016 plates were cold-rolled to 0.9mm through three different rolling processes. One was directly rolled to 0.9mm, the other two were rolled to 1.8mm and 2.3mm, respectively, followed by intermediate annealing at 360°C for 2h, and then rolled to 0.9mm. Finally, the three kinds of cold rolled plates were performed continuous annealing at 560oC. The textures and microstructures of each stage were characterized by the X-ray diffraction and electron back scattering diffraction (EBSD) techniques. The results show that the texture of hot-rolled sample is mainly composed of Brass, S and Copper; the relative amount and maximum density changed after 1st cold-rolling. After intermediate annealing, the Cube and Cube+ND20 texture replace the deformation texture and rise with the rolling reduction. Then the conducting of final cold rolling results in the decrease of Cube and Cube+ND20 component and increase of deformation texture. After the continuous annealing, R, Brass-R, Goss, Cube and Cube+ND20 components are observed. Particle stimulated nucleation (PSN) and nucleation at shear bands dominate the competition of recrystallization.

scholarly journals Effect of cold rolling and annealing temperature to the characteristics of α + β' phases in Cu-29.5Zn-2.5Al alloy produced by gravity casting

2020 ◽  
Vol 56 (1) ◽  
pp. 89-97
Author(s):  
I. Angela ◽  
I. Basori ◽  
B.T. Sofyan
Keyword(s):  
Cold Rolling ◽  
Shear Bands ◽  
X Ray Diffraction ◽  
Gravity Casting ◽  
X Ray ◽  
Low Temperature Annealing ◽  
Slip Bands ◽  
Cold Rolling And Annealing ◽  
Higher Temperature ◽  
Cold Rolled

Al-brass alloys (Cu29.5Zn2.5Al wt. %) were produced by gravity casting and homogenized at 800?C for 2 h, resulting in a binary phase morphology identified as cubic ? and martensitic ?? phases through X-ray diffraction (XRD). Samples were then subsequently cold rolled and annealed at 150, 300, 400, and 600?C for 30 minutes. Visible traces of slip, intersecting slip bands, and shear bands were observed in microstructure images of the samples after each progressive deformation stage. Deformation-induced martensites were present after 20 % cold rolling. Higher thickness reduction resulted in simultaneous strain hardening of the phases. Low temperature annealing slightly increased microhardness, of both ? and ??, due to the formation of precipitates. SEM-EDX analysis showed that no solute segregation was found in annealed samples. Annealing at higher temperature resulted in conventional softening. Recrystallized equiaxed ?? phase grains were visible after annealing at 600?C.

Micro Beam Orientation Determinations in Highly Deformed Cu - 12.5% Ni Alloy

1985 ◽  
Vol 43 ◽  
pp. 352-353
Author(s):  
P.G. Caceres ◽  
R.D. Garwood
Keyword(s):  
Shear Bands ◽  
Pure Metal ◽  
Deformation Texture ◽  
X Ray Diffraction ◽  
X Ray ◽  
Pole Figures ◽  
Ni Alloy ◽  
Beam Orientation ◽  
Cold Rolled ◽  
Convergent Beam

Convergent beam microdiffraction (CBD) techniques have been used to determine changes in orientation along and across subs truetural regions such as microbands, shear bands, crystallites, etc., in a heavily cold rolled Cu - 12.5% Ni alloy of high purity. The investigation is an extension of similar studies on copper and alpha brass (see eg. 1, 2 and 3).Pole figures and inverse pole figures determined by x-ray diffraction techniques have shown (see 4 and 5) that this alloy develops a copper-type deformation texture, although, more slowly than the pure metal since a substantial increase of the 422 reflection, arising from a (112) [111] end orientation, occurs only at deformations greater than 90% (ε ∼2.30).

scholarly journals Microstructure And Texture Evolution During Cold-Rolling In The Fe-23Mn-3Si-3Al Alloy

2015 ◽  
Vol 60 (3) ◽  
pp. 1789-1794 ◽  
Author(s):  
J. Kowalska ◽  
W. Ratuszek ◽  
M. Witkowska ◽  
A. Zielińska-Lipiec ◽  
M. Kowalski
Keyword(s):  
Cold Rolling ◽  
Texture Evolution ◽  
Martensitic Transformations ◽  
Mechanical Twinning ◽  
Al Alloy ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Cold Rolled ◽  
Hot Rolled

Abstract Fe–23wt.%Mn–3wt.%Si–3wt.%Al alloy was cast, homogenized at 1150ºC, hot-rolled at temperatures between 1200ºC and 900ºC and next cold-rolled from 5% up to 40% reductions in thickness. Microstructure and texture of this alloy, which has a low stacking fault energy, were defined after cold-rolling. Investigation of transmission electron microscopy and X-ray diffraction showed that mechanical twinning and martensitic transformations (γfcc→εhcp and γfcc→εhcp→α′bcc) took place during cold-rolling. The crystallographic Shoji-Nishiyama (S-N) {00.2}ε║{111}γ, <11.0>ε ║ <110>γ and Kurdjumov-Sachs (K-S) {111}γ║{101}α’, <101>γ║<111>α’ relations between martensite (ε, α’) and austenite (γ), were found in the coldrolled material.

Effect of Hot-Rolled Microstructure on the Recrystallization Texture of Cold-Rolled Non-Oriented Electrical Steel

2011 ◽  
Vol 298 ◽  
pp. 203-208 ◽  
Author(s):  
Zi Li Jin ◽  
Wei Li ◽  
Yi Ming Li
Keyword(s):  
Cold Rolling ◽  
Electrical Steel ◽  
Texture Evolution ◽  
Steel Strip ◽  
Silicon Steel ◽  
Grain Structure ◽  
Recrystallization Annealing ◽  
Rolled Sheet ◽  
Cold Rolled ◽  
Hot Rolled

With the help of orientation distribution function (ODF) analysis, experiments of different hot band grain microstructure 0.33% silicon steel were cold-rolled and annealed in the laboratory，to study the effect of the microstructure hot-rolled steel strip for cold rolled non-oriented silicon steel microstructure and texture of recrystallization annealing. The results show that hot rolled microstructure on cold rolled Non-Oriented Electrical Steel cold-rolled sheet evolution of texture and recrystallization have important influence, the quiaxed grain structure of steel by cold rolling and recrystallization annealing, the recrystallization speed than the fiber grain-based mixed crystals recrystallization fast , With the equiaxed grains made of cold rolled silicon steel after annealing the {110}<UVW> texture components was enhanced and {100}<uwv> texture components weakened. Different microstructure condition prior to cold rolling in the recrystallization annealing process the texture evolution has the obvious difference, the equiaxial grain steel belt cold rolling and annealing, has the strong crystal orientation. This shows that the equiaxed grain when hot microstructure is detrimental to the magnetic properties of cold-rolled non-oriented silicon steel to improve and increase.

scholarly journals Microstructure and Mechanical Properties of 4Al Alumina-Forming Austenitic Steel after Cold-Rolling Deformation and Annealing

Materials ◽  
2020 ◽  
Vol 13 (12) ◽  
pp. 2767 ◽  
Author(s):  
Chenchen Jiang ◽  
Qiuzhi Gao ◽  
Hailian Zhang ◽  
Ziyun Liu ◽  
Huijun Li
Keyword(s):  
Grain Size ◽  
Cold Rolling ◽  
Grain Boundaries ◽  
Austenitic Steel ◽  
Rolling Reduction ◽  
X Ray Diffraction ◽  
Transmission Electron ◽  
Cold Rolling Reduction ◽  
Average Grain Size ◽  
Cold Rolled

Microstructural evolutions of the 4Al alumina-forming austenitic steel after cold rolling with different reductions from 5% to 30% and then annealing were investigated using electron backscattering diffraction (EBSD), X-ray diffraction (XRD) and transmission electron microscopy (TEM). Tensile properties and hardness were also measured. The results show that the average grain size gradually decreases with an increase in the cold-rolling reduction. The low angle grain boundaries (LAGBs) are dominant in the cold-rolled samples, but high angle grain boundaries (HAGBs) form in the annealed samples, indicating that the grains are refined under the action of dislocations. During cold rolling, high-density dislocations are initially introduced in the samples, which contributes to a large number of dislocations remaining after annealing. With the sustaining increase in cold-rolled deformation, the samples exhibit more excellent tensile strength and hardness due to the decrease in grain size and increase in dislocation density, especially for the samples subjected to 30% cold-rolling reduction. The contribution of dislocations on yield strength is more than 60%.

Survival of Goss Grains during Cold Rolling of a Silicon Steel Single Crystal

2005 ◽  
Vol 495-497 ◽  
pp. 1061-1066 ◽  
Author(s):  
Dorothée Dorner ◽  
Ludger Lahn ◽  
Stefan Zaefferer
Keyword(s):  
Cold Rolling ◽  
Single Crystal ◽  
High Strain ◽  
Shear Bands ◽  
Rolling Process ◽  
Silicon Steel ◽  
Oriented Crystal ◽  
Cold Rolled ◽  
Goss Orientation ◽  
Crystal Volume

A silicon steel single crystal with initial Goss orientation, i.e. the {110}<001> orientation, was cold rolled up to 89 % thickness reduction. Most of the crystal volume rotates into the two symmetrical equivalent {111}<112> orientations. However, a weak Goss component is still present after high strain, although the Goss orientation is mechanically instable under plane strain loading. Two types of Goss-oriented crystal volumes are found in the highly deformed material. We suggest that their origin is different. The Goss-oriented regions that are observed within shear bands form during the cold rolling process. In contrast, those Goss-oriented crystal volumes that are found inside of microbands survive the cold rolling.

scholarly journals An assessment of static recrystallization in L-605 Cobalt-based superalloy

10.30544/231 ◽  
2016 ◽  
Vol 22 (4) ◽  
pp. 221-236
Author(s):  
Padina Ajami Ghaleh Rashidi ◽  
Hossein Arabi ◽  
Seyed Mehdi Abbasi
Keyword(s):  
Cold Rolling ◽  
Annealing Time ◽  
Annealing Temperature ◽  
Static Recrystallization ◽  
Microstructural Analysis ◽  
High Annealing ◽  
Microstructural Evaluation ◽  
Cold Rolled ◽  
Lower Temperature ◽  
Hot Rolled

In this research, the effect of cold rolling, annealing time and temperature on microstructure and hardness were studied in L-605 superalloy. A cast bar of L-605 alloy was hot rolled at 1200ºC. As the following, it was solutionized at 1230 ºC for 1 hour and finally was cold rolled by different amounts (i.e. 5-35 percent thickness reduction). The cold-rolled samples were heat treated for different times (i.e. 2-120 min.) at temperature range of 1068-1230 ºC in order to study their recrystallization behavior. The results of microstructural analysis indicated that static recrystallization is responsible for microstructural refinement and coarsening, so that an increase in the amounts of cold rolling resulted in a fully recrystallized microstructure at lower temperature. This analysis also indicated that annealing temperature is more effective than annealing time in grain growth. Microstructural evaluation as well as showed that carbides such as M7C3 and M23C6 which have been reported in some literature were not observed during rolling or annealing in this research. It is perhaps due to usage of high annealing temperatures or possibly due to their very low contents which was not possible for us to evaluate their formation with conventional methods. Hardness results revealed that higher annealing temperature lead to lower hardness values as expected.

Effect of Annealing Temperature on the Transformation Temperature and Texture of Ni47Ti44Nb9 Cold-Rolled Plate

2012 ◽  
Vol 557-559 ◽  
pp. 1281-1287 ◽  
Author(s):  
Zhao Wei Feng ◽  
Xu Jun Mi ◽  
Jiang Bo Wang ◽  
Zhi Shan Yuan ◽  
Jin Zhou
Keyword(s):  
Transformation Temperature ◽  
Martensite Transformation ◽  
Annealing Temperature ◽  
Rolled Plate ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Cold Rolled ◽  
Reverse Martensite Transformation ◽  
Rolled Plates

Transformation behaviors and texture of Ni47Ti44Nb9 cold-rolled plates were studied by differential scanning calorimetry and X-ray diffraction test. R phase transformation does not occur in Ni47Ti44Nb9cold-rolled plate annealed at 350°C-750°C followed by quenching into the water. Martensite transformation temperature first increases and then decreases with increment of annealing temperature, and the maximum achieves at 700°C. The heat of reverse martensite transformation increases, while hardness decreases as annealing temperature increases. The major texture of cold-rolled plate is {332} and spread from {332} to {110}. When the annealing temperature is above 600°C, the major textures are {332} and {111} recrystallization texture in secondary cold-rolled plate.

Bending Ductility of Heavily Cold-Rolled Ni3Al Thin Foils

2002 ◽  
Vol 753 ◽  
Author(s):  
Satoru Kobayashi ◽  
Masahiko Demura ◽  
Kyosuke Kishida ◽  
Toshiyuki Hirano
Keyword(s):  
Cold Rolling ◽  
Shear Bands ◽  
Slip Systems ◽  
Dislocation Interaction ◽  
Fracture Elongation ◽  
Thin Foils ◽  
Slip Planes ◽  
Cold Rolled ◽  
Bending Mechanism ◽  
Slip Deformation

ABSTRACTOur recent studies revealed that heavily cold-rolled Ni3Al foils have a good bending ductility in spite of almost no elongation in tensile test. In this paper, bending characteristics of 95% cold-rolled foils around transverse and rolling directions (TD and RD, respectively) were examined to understand the bending mechanism. Fracture elongation on the tension surface shows a large bending anisotropy: 5 % for the TD bending, while less than 1% for the RD bending. The bending ductility is due to {111}<110> slip deformation. In the TD bending, slip occurs on the slip systems operated during cold rolling, and cracks initiate along the shear bands. In the RD bending, slip occurs on the other {111} planes besides the slip planes operated during cold rolling, and fracture occurs as a result of the dislocation interaction in the both planes.

Analysis of Deformation Texture in AISI 304 Steel Sheets

2013 ◽  
Vol 203-204 ◽  
pp. 105-110 ◽  
Author(s):  
Agnieszka Kurc-Lisiecka ◽  
Wojciech Ozgowicz ◽  
Wiktoria Ratuszek ◽  
Joanna Kowalska
Keyword(s):  
Cold Rolling ◽  
Rolling Texture ◽  
Orientation Distribution ◽  
Deformation Texture ◽  
Distribution Functions ◽  
Rolled Strip ◽  
Aisi 304 ◽  
Aisi 304 Steel ◽  
Cold Rolled ◽  
Two Phases

The textures of cold-rolled AISI 304 austenitic steel were the object of the investigations. The austenite steel was deformed by cold-rolling to 20, 40 and 70% reduction. A significant amount of martensite, formed due to the strain induced (γ®a’) transformation, was detected in the deformed structure by applying magnetic and X-ray diffraction methods. Texture analysis was performed on the basis of the orientation distribution functions (ODFs) calculated from the experimental pole figures. The texture measurements of both phases were conducted from the center layers of the cold-rolled strip. In the case of metastable austenite AISI 304 steel the texture development was very complex because three processes were proceded simultaneously during the cold-rolling, namely: plastic deformation of the austenitic g-phase, strain induced phase transformation γ®a’ and deformation of the formed a’-martensite. These processes resulted in the presence of two phases in the structure of the steel with a definite crystallographic relationship and orientation changes of both phases with increasing of the deformation. Thus, the resultant deformation texture of the investigated steels is described by the austenite and martensite texture components. The rolling texture of γ-phase describes mainly orientations from the fiber α =<110>║ND and the major components of the martensite deformation texture are orientations from the fibers α1=<110>║RD and γ ={111}║ND.

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