Influence of Nano Reinforcement Volume Percentage on Fabrication of Surface Nanocomposite by FSP

2016 ◽  
Vol 879 ◽  
pp. 1369-1374
Author(s):  
P. Naresh ◽  
Adepu Kumar ◽  
M. Krishna Kishore

This work deals with the effect of volume percentage of nanoreinforcement to fabricate nanosurface composite by Friction Stir Processing (FSP) and also studied the role of tool rotational speed and traverse speed to get the defect free condition to fabricate successful surface composite. The material flow pattern, dispersion of the reinforcement particles in the stir zone was examined. From the phase/volume fraction analysis, it was observed that the nanoAl2O3 particles were well dispersed in the stir zone. The results indicate that the better microstructural, mechanical properties were obtained at 1150rpm /15mm/min condition. A significant improvement in microhardness was exhibited by surface nanocomposite as compared to the as - received aluminum.

2017 ◽  
Vol 15 ◽  
pp. 36-45
Author(s):  
A. Karthikeyan ◽  
S. Nallusamy

In present scenario, nanocomposites are playing an imperative role in most of the industrial application due to their outstanding performances with good mechanical properties. The aim of this research is to study the effect of tool rotational speed and traverse speed on micro structural and hardness properties of fabricated surface nanocomposites of Al-Al2O3. By varying tool rotational and traverse speed at a constant volume percentage the surface nanocomposites were produced by applying one pass of friction stir processing. A clear view of material flow and defect characterization in the stir zone were studied. Optimum condition of tool rotational speed of 1120 rpm and tool traverse speed of 16 mm/min was obtained to produce a defect free surface nanocomposite. Microstructure observations were carried out through optical microscope and micro hardness test were conducted by using Vickers micro hardness tester. From the phase volume fraction analysis, it was observed that the Al2O3 nanoparticles were well dispersed in the stir zone. It was found that, the tool speed and traverse speed had a significant impact on microstructure properties as well as mechanical properties of the fabricated surface nanocomposite. From the final results it was found that a mixture of dynamically restored ultra fine grins with a mean size of ~80 nm and the average micro hardness value of 130HV were achieved through a fabricated aluminium Al2O3 nanocomposite.


2014 ◽  
Vol 592-594 ◽  
pp. 234-239 ◽  
Author(s):  
A. Thangarasu ◽  
N. Murugan ◽  
I. Dinaharan ◽  
S.J. Vijay

Friction stir processing (FSP) is as a novel modifying technique to synthesize surface composites. An attempt has been made to synthesis AA6082/TiC surface composite using FSP and to analyze the effect of tool rotational speed on microstructure and microhardness of the same. The tool rotational speed was varied from 800 rpm to 1600 rpm in steps of 400 rpm. The traverse speed, axial force, groove width and tool pin profile were kept constant. Scanning electron microscopy was employed to study the microstructure of the fabricated surface composites. The results indicated that the tool rotational speed significantly influenced the area of the surface composite and distribution of TiC particles. Higher rotational speed provided homogenous distribution of TiC particles while lower rotational speed caused poor distribution of TiC particles in the surface composite. The effect of the tool rotational speed on microhardness is also reported in this paper.


2015 ◽  
Vol 830-831 ◽  
pp. 467-471 ◽  
Author(s):  
P. Naresh ◽  
Adepu Kumar

In this investigation, the effect of nanoreinforcement particles such as Al2O3, tool rotational speed and traverse speed on microstructure and mechanical properties of Al/Al2O3surface nanocomposites fabricated by friction stir processing was studied. The surface nanocomposites were produced by varying volume percentage of nanoreinforcement, tool rotational speed and traverse speed to attain the best outcome. The fabricated composites were characterized through microstructural evaluation, microhardness measurements and energy dispersive spectroscopy analysis. Microstructural evaluation of the composites revealed that the composites were produced finer grain structure in this stir zone and it is evident for, a dynamic recrystallization was taken place. Higher hardness values were found at the stir zone of the entire composite because of the equiaxed and well dispersion of reinforced particles. The energy dispersive spectroscopy analysis revealed the presence of various elements at the stir zone. A defect free parameter setting for friction stir processing of Al/Al2O3was obtained at 1120 rpm and 16 mm/min.


2014 ◽  
Vol 592-594 ◽  
pp. 776-780
Author(s):  
L. John Baruch ◽  
R. Raju ◽  
V. Balasubramanian ◽  
I. Dinaharan

Friction stir processing (FSP) is a solid-state process leading to very significant microstructural modifications. Despite the large number of studies, most of the work that has been done in the FSP field focuses on microstructural evolution, tensile properties, hardness, fatigue strength, corrosion resistance etc. However there is not much information available on correlation of FSP parameters with evolution of defect free processed zone. In order to produce a defect free processed zone, selecting the best processing parameters is very important. In this investigation, the effect of two main FSP parameters (such as tool rotational speed which was kept constant and tool transverse speed which was varied) on the formation/ evolution of defect free processed zone was studied. It is found that at a tool rotational speed 600 rpm and a traverse speed of 12 mm/min the processed zone is defect free. Numerous investigations have been conducted to understand material flow behavior during FSW/FSP. However, the flow process of material during FSW/FSP is still not well-understood, and different explanations have been proposed. In this investigation an attempt has been made to understand the flow of material during FSP and it is reported.


2011 ◽  
Vol 312-315 ◽  
pp. 500-505 ◽  
Author(s):  
Parviz Asadi ◽  
M.K. Besharati Givi ◽  
Mohsen Barmouz

In this study, friction stir processing (FSP) was applied to fabricate a Cu/SiC surface composite layer by incorporation of 5 µm SiC particles. Effects of the traverse speed and SiC volume fraction on the microstructure, hardness and powder distribution pattern of the developed surface layer were investigated. Optical and scanning electron microscopy (SEM) was employed to carry out the microstructural observations. Results show that increasing the volume fraction causes an intense decrease in the grain size and increase in the hardness of the developed surface. To achieve a uniform distribution of particles and uniform microstructure, the traverse speed should decrease as far as possible.


Author(s):  
Sumit Jain ◽  
R.S. Mishra

In this research, a defect-free dissimilar weld joint of AA7075-T6 and AA6061-T6 reinforced with Al2O3 nanoparticles was fabricated via friction stir welding (FSW). The influence of tool rotational speed (700, 900 and 1100 rpm), traverse speed (40, 50 and 60 mm/min) with varying volume fractions of Al2O3 nanoparticles (4%, 7% and 10%) on microstructural evolution and mechanical properties were investigated. The augmentation of various mechanical properties is based on the homogeneity of particle dispersion and grains refinement in the SZ of the FSWed joint. The findings revealed that the remarkable reduction in grain size in the SZ was observed owing to the incorporation of Al2O3 nanoparticles produces the pinning effect, which prevents the growth of grain boundaries by dynamic recrystallization (DRX). The increasing volume fraction of Al2O3 nanoparticles enhanced the mechanical properties such as tensile strength, % elongation and micro-hardness. Agglomeration of particles was observed in the SZ of the FSWed joints produced at lower tool rotational speed of 700 rpm and higher traverse speed of 60 mm/min due to unusual material flow. Homogenous particle dispersion and enhanced material mixing ensue at higher rotational speed of 1100 rpm and lower traverse speed of 40 mm/min exhibit higher tensile strength and micro-hardness.


2017 ◽  
Vol 62 (3) ◽  
pp. 1819-1825
Author(s):  
V.C. Sinha ◽  
S. Kundu ◽  
S. Chatterjee

AbstractIn the present study, the effect of tool rotational speed on microstructure and mechanical properties of friction stir welded joints between commercially pure copper and 6351 Al alloy was carried out in the range of tool rotational speeds of 300-900 rpm in steps of 150 rpm at 30 mm/minutes travel speed. Up to 450 rpm, the interface of the joints is free from intermetallics and Al4Cu9intermetallic has been observed at the stir zone. However, Al4Cu9intermetallic was observed both at the interface and the stir zone at 600 rpm. At 750 and 900 rpm tool rotational speed, the layers of AlCu, Al2Cu3and Al4Cu9intermetallics were observed at the interface and only Al4Cu9intermetallics has been observed in the stir zone. The maximum ultimate tensile strength of ~207 MPa and yield strength of ~168 MPa along with ~6.2% elongation at fracture of the joint have been obtained when processed at 450 rpm tool rotational speed.


Author(s):  
Xun Liu ◽  
Sheng Zhao ◽  
Kai Chen ◽  
Jun Ni

In this study, the friction stir welding (FSW) of aluminum alloy 6061-T6511 to TRIP 780 steel is analyzed under various process conditions. Two FSW tools with different sizes are used. To understand the underlying joining mechanisms and material flow behavior, nano-computed tomography (nano-CT) is applied for a 3D visualization of material distribution in the weld. With insufficient heat input, steel fragments are generally scattered in the weld zone in large pieces. This is observed in a combined condition of big tool, small tool offset, and low rotating speed or a small tool with low rotating speed. Higher heat input improves the material flowability and generates a continuous strip of steel. The remaining steel fragments are much finer. When the volume fraction of steel involved in the stirring nugget is small, this steel strip can be in a flat shape near the bottom, which generally corresponds to a better joint quality and the joint would fracture in the base aluminum side. Otherwise, a hook structure is formed and reduces the joint strength. The joint would fail with a combined brittle behavior on the steel hook and a ductile behavior in the surrounding aluminum matrix.


2020 ◽  
Vol 17 (4) ◽  
pp. 491-507 ◽  
Author(s):  
Nitin Panaskar ◽  
Ravi Prakash Terkar

Purpose Recently, several studies have been performed on lap welding of aluminum and copper using friction stir welding (FSW). The formation of intermetallic compounds at the weld interface hampers the weld quality. The use of an intermediate layer of a compatible material during welding reduces the formation of intermetallic compounds. The purpose of this paper is to optimize the FSW process parameters for AA6063-ETP copper weld, using a compatible zinc intermediate filler metal. Design/methodology/approach In the present study, a three-level, three-factor central composite design (CCD) has been used to determine the effect of various process parameters, namely, tool rotational speed, tool traverse speed and thickness of inter-filler zinc foil on ultimate tensile strength of the weld. A total of 60 experimental data were fitted in the CCD. The experiments were performed with tool rotational speeds of 1,000, 1,200 and 1,400 rpm each of them with tool traverse speeds of 5, 10 and 15 mm/min. A zinc inter-filler foil of 0.2 and 0.4 mm was also used. The macrograph of the weld surface under different process parameters and the tensile strength of the weld have been investigated. Findings The feasibility of joining 3 mm thick AA6063-ETP copper using zinc inter-filler is established. The regression analysis showed a good fit of the experimental data to the second-order polynomial model with a coefficient of determination (R2) value of 0.9759 and model F-value of 240.33. A good agreement between the prediction model and experimental findings validates the reliability of the developed model. The tool rotational speed, tool traverse speed and thickness of inter-filler zinc foil significantly affected the tensile strength of the weld. The optimal conditions found for the weld were, rotational speed of 1,212.83 rpm and traverse speed of 9.63 mm/min and zinc foil thickness is 0.157 mm; by using optimized values, ultimate tensile strength of 122.87 MPa was achieved, from the desirability function. Originality/value Aluminium and copper sheets could be joined feasibly using a zinc inter-filler. The maximum tensile strength of joints formed by inter-filler (122.87 MPa) was significantly better as compared to those without using inter-filler (83.78 MPa). The optimum process parameters to achieve maximum tensile strength were found by CCD.


Author(s):  
P. Sagar ◽  
A. Handa

Purpose: A new composite material was prepared and Different properties such as hardness and tribological behaviour of the fabricated metal matrix composite (MMC) was investigated and compared with the base AZ61A magnesium alloy. Design/methodology/approach: For the current research work, state-of-the-art technology, Friction stir processing (FSP) was performed to develop magnesium based AZ61A/TiC composite at optimized set of machine parameters. Findings: Increasing tool rotational speed ultimately leads in enhanced hardness, which further gives superior tribological properties as compared to base AZ61A alloy. Wear observations suggests a combination of abrasive and adhesive wear mechanism. Research limitations/implications: More microstructural and mechanical properties can be examined. Practical implications: The idea behind selecting AZ61A is mainly due to its increasing use in bicycle pedals and military equipment’s where at certain places it needs to encounter friction. In this current work, microhardness study and wear behaviour of AZ61A/TiC composite processed via FSP were examined. Originality/value: Paper is completely new and no work has been done till date considering this material and preparing composite with nanoparticles TiC.


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