Investigation of microstructural and wear behavior of Al6061 surface composites fabricated by friction stir process using Taguchi approach

The surface composites of aluminum alloys have a higher scope of applications encountering surface interactions in the aerospace, automobile, and other industries compared to the base aluminum alloys. The friction stir process (FSP) is recently the preferred method to prepare aluminum-based surface composites due to its capability to produce improved physical properties and refined microstructure at the surface. The study examines the Al6061 alloy-based surface composite fabricated by FSP for their wear behavior and microstructure. In this study, the Al6061 alloy-based hybrid surface composites are prepared with varying weight% of copper and graphite microparticles mixture as reinforcement by FSP with two tools having unique pin profiles, i.e., threaded cylindrical and plain cylindrical. These prepared composites are investigated for the dry sliding wear test on a pin-on-disc test set-up. The experiments are designed using the L9 orthogonal array and analyzed by the Taguchi approach to obtain the influence of disc speed, load, and reinforcement weight% on wear rate. The significant parameters influencing the wear rate of the samples tested are obtained using ANOVA. Later the effects of the friction stir process and the wear tests on the microstructure of the workpieces are investigated using FE-SEM/EDS tests. It is concluded that the decrease in wear rate with the rise in reinforcement weight% (Cu + graphite) from 2% to 6%. The load has the maximum effect on the wear rate for the samples prepared by threaded cylindrical FSP tool pin profile, while reinforcement weight% affects significantly the wear rate of the samples prepared by FSP with plain cylindrical pin profile tool.

Influence of Fly Ash and Emery based particulate reinforced AA7075 surface composite processed through friction stir processing

The novel friction stir technology is adopted in modern automotive industries to meet the desired properties like hardness, impact toughness and tribological behaviour over the conventional techniques like stir casting, compo casting, squeeze casting, electroplating and infiltration methods. AA7075 surface composites fabricated with different volume fractions of fly ash and emery particles is said to enhance the aforementioned properties. The composites are processed through friction stir process (rotational speed −1200 rpm, transverse speed – 56 mm/min, tool tilt angle – 2 °). During characterization, the Microstructural examination of surface composites depicts fine and homogenous distribution of reinforcements in the friction stir process region owing to severe plastic deformation and dynamic recrystallization process. Substantially, good interface is formed between the reinforcement particulates and base substrate. Inclusion of Fe3O4, Al2O3 and SiO2 constituents through fly ash and emery reinforcements associated with the homogenous dispersion strengthening mechanism favours for the superior hardness of surface hybrid composite specimen 50E50FA. Decremented grain size and load bearing capacity of the reinforcements is beneficial for the crack propagation resistance that enhances the impact toughness behaviour (17.4 J/cm2) of the same specimen. Wear rate of the specimens are evaluated through pin on disc tribometer. The decrease in the wear rate of hard specimen 50E50FA is observed due to the reduced contact area between its surface and counter disc. The morphology of worn specimens using SEM analysis shows the combined abrasive and adhesive wear as the worn mechanism.

Testing novel multicomposite materials for electromethanogenesis

Electromethanogenesis is an innovative technology that uses a microbial electrochemical system to produce methane from CO2, in a power-to-gas (BEP2G) concept. The results of experimental tests of new and cost-effective carbonaceous materials for electrode are presented here. The study aims at optimizing electromethanogenesis processes at laboratory level in mesothermic condition. As part of the experiments, hydrogenotrophic microorganisms (Family Metanobacteriaceae of Archaea domains) were selected from a mixed consortium taken from a biogas digestate and inoculated in double-chamber bioelectrochemical systems. The maximum amount of methane produced was 0.3 - 0.8 mol/m2g (normalized to the cathode area) with carbon cloth electrodes. Aiming at improving the methane productivity, innovative materials for the electrodes were now studied, creating porous high-surface composites, and studying nitrogen carbons doped with Cu and hydroxyapatite (Multicomposite Cu@/HAP/C), as chemical catalysts for CO2 reduction (CO2RR). The description of the procedure for the Multicomposite Cu@/HAP/C production is reported in detail.

Design of Functionally Graded Composites through Friction Stir Processing

An Investigation was conducted to produce Aluminium based Functionally graded material (FGM) composites by Friction stir processing (FSP). A reinforcement strategy featuring the use of Alumina and TiC reinforcements was investigated, where holes were drilled in an Aluminium plate, filled with reinforcements and stirred using FSP. A mathematical model was formulated for positioning of holes in such a manner that the composition of the reinforcements varies from maximum to minimum over a given length. Samples were subjected to various number of FSP passes from one to three with 100% overlap and its influence on particle distribution and homogeneity was studied using Scanning electron microscopy (SEM) at cross sections parallel to the tool traverse direction. A progressive gradient in hardness values was observed for the surface composites at all the passes.

The Effect of Incorporating Ceramic Particles with Different Morphologies on the Microstructure, Mechanical and Tribological Behavior of Hybrid TaC_ BN/AA2024 Nanocomposites

Improving the mechanical durability and wear resistance of aluminum alloys is a research challenge that can be solved by their reinforcement with ceramics. This article is concerned with the improvement of the mechanical properties and wear resistance of the AA2024 aluminum alloy surface. Surface composites were prepared by incorporating a hybrid of heavy particles (tantalum carbide (TaC), light nanoparticles, and boron nitride (BN)) into the AA2024 alloy using the friction stir process (FSP) approach. Three pattern holes were milled in the base metal to produce the composites with different volume fractions of the reinforcements. The effects of the FSP and the reinforcements on the microstructure, mechanical properties, and wear resistance are investigated. In addition to the FSP, the reinforced particles contributed to greater grain refinement. The rolled elongated grains became equiaxed ultrafine grains reaching 6 ± 1 µm. The refinement and acceptable distribution in the reinforcements significantly improved the hardness and wear resistance of the produced composites. Overall, the hardness was increased by 60% and the wear resistance increased by 40 times compared to the base alloy.

Mechanical and microstructural characterization of Ti-SiC reinforced AA5083 surface composites fabricated via friction stir process

A mixture of Titanium and silicon-carbide powders was embedded in the AA5083 matrix by Friction Stir Processing (FSP). Experiments were performed as per Taguchi L8 orthogonal array, and the effect of reinforcement on hot strength (at 100oC), processed zone (PZ) geometry, and microstructure were investigated. The effect of PZ geometry on the surface properties was also analyzed. The effect of heating the tensile test specimens to 540ºC on the strength at 100oC was also separately investigated. It was observed that surface hardness was significantly enhanced by FSP, and the highest mean hardness of 90.4 HV was observed. Furthermore, it was observed that the surface properties also significantly depend on PZ geometry. From experimental results, it was found that the specimens with the lowest width to depth ratio bears the highest hardness and vice versa. A clear effect of parameters was evident on the geometry of processed zones with a deep bowl, and shallow cup-shaped zones were formed with smaller and larger shoulder diameters, respectively. The samples were processed at 355 rpm, 63 mm/min, 17 mm shoulder, and 355 rpm, 80 mm/min. The 20 mm shoulder showed high tensile strength 292 MPa and 294 Mpa, respectively. The strength of these samples did not reduce much even after heating to 540oC.

Technological Aspects of Producing Surface Composites by Friction Stir Processing—A Review

FSP (friction stir processing) technology is a modern grain refinement method that is setting new trends in surface engineering. This technology is used not only to modify the microstructure of the surface layer of engineering materials, but increasingly more often also to produce surface composites. The application potential of FSP technology lies in its simplicity and speed of processing and in the wide range of materials that can be used as reinforcement in the composite. There are a number of solutions enabling the effective and controlled introduction of the reinforcing phase into the plasticized matrix and the production of the composite microstructure in it. The most important of them are the groove and hole methods, as well as direct friction stir processing. This review article discusses the main and less frequently used methods of producing surface composites using friction stir processing, indicates the main advantages, disadvantages and application limitations of the individual solutions, in addition to potential difficulties in effective processing. This information can be helpful in choosing a solution for a specific application.