Effects of Precipitation of Al3Zr Particles on Microstructures and Properties of the Al-3.55Cu-1.51Li-0.11Zr Alloy

2018 ◽  
Vol 921 ◽  
pp. 214-221
Author(s):  
Mang Jiang ◽  
Jin Jun Xu
Keyword(s):  
Heat Treatment ◽  
Grain Boundary ◽  
Tensile Properties ◽  
Solution Heat Treatment ◽  
Thermal Activation ◽  
Single Step ◽  
Aged Sample ◽  
Precipitation Behavior ◽  
Double Step ◽  
The Matrix

Under single-step and double-step homogenization conditions, the precipitation behavior of Al3Zr dispersoids and its effects on the microstructures and tensile properties of an Al-3.5Cu-1.5Li-0.11Zr alloy were investigated in the current study. It was found that a double-stage homogenization (460 °C/16 h, 520 °C/24 h) enhanced the uniformity of the Al3Zr dispersoids distribution compared with the single-stage homogenized samples. Al3Zr particles which are coherent with the matrix would inhibit the movement of dislocation induced by stress and also the migration of sub-grain boundary and grain boundary induced by thermal activation. The finer particle size and distribution more diffuse of Al3Zr particles reduced recrystallization during hot rolling and solution heat treatment, improving the tensile properties of the as-aged sample.

Effect of the Two-Step Solution Heat Treatment on the Microstructure of Semisolid Cast 7075 Aluminum Alloy

2012 ◽  
Vol 488-489 ◽  
pp. 243-247 ◽  
Author(s):  
Saowalak Kongiang ◽  
Thawatchai Plookphol ◽  
Jessada Wannasin ◽  
Sirikul Wisutmethangoon
Keyword(s):  
Heat Treatment ◽  
Treatment Condition ◽  
Solution Heat Treatment ◽  
Solution Treatment ◽  
Heat Treatment Condition ◽  
Single Step ◽  
Eutectic Phase ◽  
Solution Treated ◽  
The Matrix ◽  
Black Particle

Effect of the two-step solution heat treatment on the microstructure of semisolid cast 7075 aluminium alloy has been studied. The microstructure of the as-cast specimens mainly consisted of matrix-α (Al) and grain boundary (GB)-eutectic phase (α-Al + Mg(Zn,Cu,Al)2). After solution treating, coarse black particles were found to form in the single-step solution treated specimens at the condition of 450 °C for 8 h and 480 °C for 1 h, respectively. Two-step solution heat treatment resulted in the reduction of coarse black particle formation while maintaining the same amount of eutectic MgZn2phase dissolution as the high temperature single-step solution treatment. Therefore, the two-step solution heat treatment enables alloying elements dissolved into the matrix without overheating and hence decreases coarse black particles. The optimum two-step solution heat treatment condition derived from this study was 400 °C for 8 h + 450 °C for 4 h.

Effect of Addition of Al & Ca and Heat Treatment on the Cast Mg-6Zn Alloy

2013 ◽  
Vol 765 ◽  
pp. 33-37 ◽  
Author(s):  
S.S. Joshi ◽  
M.S. Mohan ◽  
S. Seshan ◽  
S. Kumar ◽  
S. Suwas
Keyword(s):  
Heat Treatment ◽  
Grain Size ◽  
Grain Boundary ◽  
Tensile Properties ◽  
Volume Fraction ◽  
Corrosion Behaviour ◽  
Boundary Phase ◽  
Al Content ◽  
Β Phase ◽  
The Matrix

In the present investigation, the effect of addition of Al and small amounts of Ca as well as the effect of heat treatment has been investigated on microstructure, tensile properties and corrosion behaviour of Mg-6Zn alloy produced by squeeze casting. The Mg-6Zn-1Al (ZA61) alloy consisted of α-Mg grains and MgZn (β) phase at the grain boundaries with a much higher strength and ductility than pure Mg. The addition of 0.1 and 0.5 wt% Ca to the ZA61 alloy refined the grain size and increased the volume fraction of the grain boundary phase but did not change the nature of the phase. Consequently, strength increased without much reduction in ductility. The increase in Al content of the alloy to 4 wt% (ZA64) changed the grain boundary phase to Al5Mg11Zn4 (Φ) phase, increased its volume fraction and refined the grain size as compared to ZA61 alloy. Consequently, strength increased with a reduction in ductility. On heat treatment of ZA61+0.5Ca and ZA64 alloys, the volume fraction of grain boundary phases decreased, fine precipitates were obtained in the matrix and the grain size increased. Thus, higher strength with a lower ductility was obtained on heat treatment but the ductility of both the alloys was still higher than that of pure Mg. Thus, 130 MPa 0.2%PS, 225 MPa UTS and 4.9% elongation to fracture could be obtained for the squeeze cast ZA64 alloy in the T6 condition, which are very good tensile properties for a cast Mg alloy. Increase in Al content and heat treatment reduced the corrosion resistance and addition of Ca improved it. The highest corrosion rate was observed to be 0.85 mm/year for the ZA64 alloy in the T6 condition.

Effect of Grain Boundary Serration on the Tensile Properties of the Super 304H Heat Resistant Austenitic Stainless Steel

2010 ◽  
Vol 654-656 ◽  
pp. 170-173 ◽  
Author(s):  
Sung Min Hong ◽  
Dong Joon Min ◽  
Eric Fleury
Keyword(s):  
Heat Treatment ◽  
Tensile Strength ◽  
Stainless Steel ◽  
Austenitic Stainless Steel ◽  
Grain Boundary ◽  
Tensile Properties ◽  
Solution Heat Treatment ◽  
Room Temperature ◽  
Tensile Ductility ◽  
Heat Resistant

Grain boundary serrations were produced in heat-resistant austenitic stainless steel containing Cu by applying after solution heat-treatment a holding time in the range 700-800oC between 30 minutes to 3 hours. These special treatments provide an enhancement of the tensile ductility of about 40 and 113%at room temperature and 750oC, respectively, while no significant change in the yield stress and tensile strength could be observed.

Influence of Solution Heat Treatment on Microstructures of Semisolid Cast 7075 Aluminium Alloy

2011 ◽  
Vol 339 ◽  
pp. 371-374 ◽  
Author(s):  
Narissara Mahathaninwong ◽  
Sirikul Wisutmethangoon ◽  
Thawatchai Plookphol ◽  
Jessada Wannasin
Keyword(s):  
Heat Treatment ◽  
Grain Boundary ◽  
Aluminium Alloy ◽  
Solution Heat Treatment ◽  
Treatment Time ◽  
Solution Treatment ◽  
Treated Sample ◽  
The Matrix ◽  
Semi Solid ◽  
Mgzn2 Phase

Influence of temperature and time of solution heat treatment on the microstructures of rheo-casting 7075 aluminium alloy produced by a novel technique, the Gas Induced Semi Solid (GISS) technique, had been investigated in this study. The microstructure of the as-cast specimens mainly consisted of matrix-α (Al) and grain boundary (GB)-eutectic phase (α-Al + Mg(Zn,Cu,Al)2). After solution heat treatment at 480 °C for 1 h, MgZn2 phase at the grain boundary was observed to have dissolved and coarse black particles of Mg2Si were observed to form in the matrix. In comparison, when solutionizing temperature of 450 °C was applied, it took 4 h of solution treatment time in order to dissolve the same portion of GB phase and MgZn2 phase, and coarse black particles of Mg2Si were found to form in the 8 h solution treated sample.

scholarly journals The Effect of Aging on Precipitates, Mechanical and Magnetic Properties of Fe-21Cr-15Ni-6Mn-Nb Low Magnetic Stainless Steel

Metals ◽  
2021 ◽  
Vol 11 (5) ◽  
pp. 819
Author(s):  
Changsheng Li ◽  
Kun Li ◽  
Jingbo Dong ◽  
Jinyi Ren ◽  
Yanlei Song
Keyword(s):  
Heat Treatment ◽  
Tensile Strength ◽  
Stainless Steel ◽  
Magnetic Properties ◽  
Solution Heat Treatment ◽  
Aging Treatment ◽  
Relative Magnetic Permeability ◽  
Coarsening Behavior ◽  
The Matrix ◽  
Coherent Orientation

The effect of aging on the precipitates, mechanical and magnetic properties of Fe-21Cr-15Ni-6Mn-Nb low magnetic stainless steel were investigated. The steel was aged at 550–750 °C for 2 h after solution heat treatment at 1100 °C for 1 h. During the aging treatment, the (Nb, V)(C, N) particles gradually precipitated in the grain, which were coherent or semi-coherent with the matrix. When the aging temperature was beyond 650 °C, the coarsening rate of (Nb, V)(C, N) particles increase rapidly and the coherent orientation between (Nb, V)(C, N) particles and the matrix was lost gradually. Meanwhile, coarse M23C6 was distributed at the grain boundary with chain shape, which was non-coherent with the matrix. The coarsening behavior of (Nb, V)(C, N) precipitates in the grain was analyzed, and the size of the particles precipitated after aging treatment at 650°C for different time was calculated and studied. After aging treatment at 650 °C for 2 h, the yield strength and tensile strength of the stainless steel was 705.6 MPa and 1002.3 MPa, the elongation and the relative magnetic permeability was 37.8% and 1.0035, respectively.

Optimizing the tensile properties of Al–Si–Cu–Mg 319-type alloys: Role of solution heat treatment

2014 ◽  
Vol 58 ◽  
pp. 426-438 ◽  
Author(s):  
Y. Han ◽  
A.M. Samuel ◽  
H.W. Doty ◽  
S. Valtierra ◽  
F.H. Samuel
Keyword(s):  
Heat Treatment ◽  
Tensile Properties ◽  
Solution Heat Treatment

Effect of Heat-Treatment Time on Microstructure and Mechanical Properties of Mg-5Gd-2Y-2Zn-0.5Zr Alloy

2012 ◽  
Vol 482-484 ◽  
pp. 1384-1389 ◽  
Author(s):  
Ling Gang Meng ◽  
Can Feng Fang ◽  
Peng Peng ◽  
Nai Pu Li ◽  
Qiong Zhu ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Grain Boundary ◽  
Treatment Time ◽  
Time Range ◽  
Lpso Phase ◽  
High Temperature Heat Treatment ◽  
Lpso Structure ◽  
The Matrix ◽  
New Type ◽  
The Stability

Microstructure evolution of Mg-5Gd-2Y-2Zn-0.5Zr alloy during high temperature heat-treatment at 500°C in the time range 10-70h was investigated. The results show that after adding the element Y, the as-cast Mg-5Gd-2Y-2Zn-0.5Zr alloy forms the Mg12Zn(Y,Gd) phase with 18R-LPSO structure at the grain boundary. During heat-treatment at 500°C, the stability of 18R-LPSO structure is weakened by Gd atoms, parts of LPSO phases dissolve gradually into the matrix with time prolonged and a new type Mg(Y,Gd)Zn phase come into being. LPSO phase in the grain boundary can ensure the ultimate tensile strength and elongation of the alloy, and effect of dissevering on the LPSO phase by Mg(Gd,Y)Zn phase results the decrease of UTS and elongation.

Effect of Two-Stage Aging on Microstructure and Properties of Al-Mg-Si Alloys

2022 ◽  
Vol 905 ◽  
pp. 51-55
Author(s):  
Li Wang ◽  
Ya Ya Zheng ◽  
Shi Hu Hu
Keyword(s):  
Growth Rate ◽  
Grain Boundary ◽  
Tensile Properties ◽  
Tensile Testing ◽  
Diffusion Rate ◽  
Two Stage ◽  
Precipitated Phase ◽  
Transmission Electron ◽  
The Matrix ◽  
Microstructure Characteristic

The effects of two-stage aging on the microstructures, tensile properties and intergranular corrosion (IGC) sensitivity of Al-Mg-Si alloys were studied by tensile testing and IGC experiments and transmission electron microscope (TEM). The results show that the two-stage aging (180°C, 2h+160°C, 120h) can reduce the IGC sensitivity without decrease the tensile properties. The grain is distributed with high-density β′′ phases, and the grain boundary phases are spherical and intermittently distributed. The formation of the microstructure characteristic is due to the lower re-aging temperature, which results in a decline differences in the diffusion rate between the matrix and grain boundaries. As a result, the pre-precipitated phase can maintain a better strengthening effects due to the slower growth rate. The pre-precipitated phase of the grain boundary presents a spherical and intermittent distribution due to the fast coarsening speed.

Effect of Double-Step Solution Treatment on Rejuvenation Heat Treated Microstructure of IN-738 Superalloy

2020 ◽  
Vol 856 ◽  
pp. 36-42
Author(s):  
Chuleeporn Paa-Rai
Keyword(s):  
Heat Treatment ◽  
Image Analysis ◽  
Electron Microscope ◽  
Solution Treatment ◽  
Single Step ◽  
Double Step ◽  
Heat Treated ◽  
Cast Superalloy ◽  
Scanning Electron

This work investigates the effect of rejuvenation heat treatment, with double-step solution treatment at the temperature from 1150 °C to 1200 °C, on the recovered microstructure of IN-738 cast superalloy. The superalloy has been long-term exposed as a turbine blade in a gas turbine prior to this study. After double solution treatment and aging at 845 °C for 12 h and 24 h, the recovered microstructures were examined by using a scanning electron microscope. Coarse γ΄ particles, that have presented in damaged microstructures, could not be observed in the samples after the rejuvenation heat treatment. In addition, the image analysis illustrates that the reprecipitated γ΄ particles in the samples with double-step solution treatments increase significantly in sizes during aging than that in the samples with the single-step solution treatment. Furthermore, the measurement of the samples hardness presents that the as-receive sample hardness is improved after rejuvenation heat treatment studied in this work.

Effect of Non-Conventional Aging Treatments on the Tensile Properties of Non-Hipped Castings of Aluminum Alloy 354

2014 ◽  
Vol 875-877 ◽  
pp. 1397-1405 ◽  
Author(s):  
G. Dinesh Babu ◽  
M. Nageswara Rao
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Aluminum Alloy ◽  
Tensile Properties ◽  
Artificial Aging ◽  
Natural Aging ◽  
Single Step ◽  
Cast Aluminum Alloy ◽  
Cast Aluminum ◽  
Automobile Components

Cast aluminum alloy 354 is used extensively for production of critical automobile components, owing to its excellent castability and attractive combination of mechanical properties after heat-treatment. With the advent of higher performance engines, there has been a steady demand to further improve the mechanical behavior of the castings made of the alloy, among others, through improvements in processing. The present study explores the possibility of improving tensile properties of the alloy by adopting certain non-conventional aging treatments. The non-conventional treatments include aging cycles similar to T6I4 and T6I6 referred to in the published literature, artificial aging in two steps instead of in single step and artificial aging preceded by various natural aging times. The results show that none of these non-conventional treatments leads to improvement of all tensile properties compared to the standard T61 treatment. Significant hardening takes place in the alloy due to natural aging. Changing the time of natural aging preceding artificial aging was found to have little effect on tensile properties.

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