Increased Antibacterial Activity by Photoactivation of Composites Based on ZnO Nanoparticles

2020 ◽  
Vol 312 ◽  
pp. 303-308
Author(s):  
Darya A. Goncharova ◽  
Sergei A. Kulinich ◽  
Anna L. Nemoykina ◽  
Valery A. Svetlichnyi

Antibacterial composites based on linen and NPs obtained by pulsed laser ablation of a zinc target in air were synthesized at various concentrations of the active component (ZnO NPs). The surface morphology and optical properties of ZnO/linen composites were investigated by scanning electron microscopy and UV-visible spectroscopy. The antibacterial activity of ZnO/linen composites was tested on S.aureus in accordance with ISO 20743:2013. It was found that the antibacterial activity depends on the concentration of ZnO NPs. High antibacterial activity of the composites was achieved when the concentration of the active component was of 0.25 mg/cm2. At a concentration of 0.1 mg/cm2 the composites showed only a bacteriostatic effect. The use of photoactivation of composites by LED radiation of 365 nm for 10 min led to an increase in antibacterial activity about 1.5 times for the samples in both concentrations.

2018 ◽  
Vol 243 ◽  
pp. 00017 ◽  
Author(s):  
Daria Goncharova ◽  
Ekaterina Gavrilenko ◽  
Anna Nemoykina ◽  
Valery Svetlichnyi

The paper studies physicochemical and antibacterial properties of ZnO nanoparticles obtained by pulsed laser ablation in water and air. Their composition and structure were studied by X-ray diffraction, transmission and scanning electron microscopy. Antibacterial activity of the nanoparticles was examined by its affection on Gram-positive Staphylococcus aureus (S.aureus). The dependence of nanoparticles’ physical and chemical antibacterial properties on the conditions of the ablation was shown. The model materials for the antibacterial bandage were made of cotton, filter paper and biodegradable polymer scaffolds (poly-l-lactide acid), and then they were coated with the obtained ZnO nanoparticles. The model bandage materials were examined by the scanning electron microscopy method and their antibacterial activity (ISO 20743:2013) was determined. High activity of all the samples against S.aureus was proved.


2016 ◽  
Vol 372 ◽  
pp. 20-29 ◽  
Author(s):  
Valery Svetlichnyi ◽  
Anastasiia Shabalina ◽  
Ivan Lapin ◽  
Daria Goncharova ◽  
Anna Nemoykina

2021 ◽  
Author(s):  
Ahmed ZITI ◽  
Bouchaib HARTITI ◽  
Amine BELAFHAILI ◽  
Hicham LABRIM ◽  
Salah FADILI ◽  
...  

Abstract Quaternary semiconductor Cu2NiSnS4 thin film was made by the sol-gel method associated to dip-coating technique on ordinary glass substrates. In this paper, we have studied the impact of dip-coating cycle at different cycles: 4, 5 and 6 on the structural, compositional, morphological, optical and electrical characteristics. CNTS thin films have been analyzed by various characterization techniques including: X-ray diffractometer (XRD), Raman measurements, scanning electron microscope (SEM), energy dispersive X-ray spectroscope (EDS), UV-visible spectroscopy and four-point probe method. XRD spectra demonstrated the formation of cubic Cu2NiSnS4 with privileged orientation at (111) plane. Crystallite size of cubic CNTS thin films increase with from 6.30 to 9.52 with dip-coating cycle augmented. Raman scattering confirmed the existence of CNTS thin films by Raman vibrational mode positioned at 332 cm− 1. EDS investigations showed near-stoichiometry of CNTS sample deposited at 5 cycles. Scanning electron microscope showed uniform surface morphologies without any crack. UV-visible spectroscopy indicated that the optical absorption values are larger than 104 cm− 1, Estimated band gap energy of CNTS absorber layers decrease from 1.64 to 1.5 eV with dip-coating cycle increased. The electrical conductivity of CNTS thin films increase from 0.19 to 4.16 (Ω cm)-1. These characteristics are suitable for solar cells applications.


2019 ◽  
Vol 824 ◽  
pp. 163-167
Author(s):  
Pema Dechen ◽  
Ekasith Somsook

In this report, synthesis and characterization of gold nanoparticles (AuNPs) from gold leaf by electrolysis in two different media (gel and paper) in presence of sodium chloride (NaCl), glucose (C6H12O6) and polyvinyl pyrrolidone (PVP) at room temperature were investigated. Graphite was used as two electrodes, NaCl was used as an electrolyte, C6H12O6 was used as reducing agent and PVP was used as stabilizer to control the aggregation of the nanoparticles. UV-Visible spectroscopy (UV-Vis) and scanning electron microscopy (SEM) were used to confirm the characteristics and morphologies of the synthesized AuNPs.


2016 ◽  
Vol 122 (7) ◽  
Author(s):  
R. K. Swarnkar ◽  
J. K. Pandey ◽  
K. K. Soumya ◽  
P. Dwivedi ◽  
S. Sundaram ◽  
...  

2017 ◽  
Vol 123 (3) ◽  
Author(s):  
Khawla S. Khashan ◽  
Ghassan M. Sulaiman ◽  
Abubaker H. Hamad ◽  
Farah A. Abdulameer ◽  
Assel Hadi

2021 ◽  
Vol 16 ◽  
pp. 155892502110438
Author(s):  
Parshuram Singh ◽  
Sapna Balayan ◽  
Rajendra Kumar Sarin ◽  
Utkarsh Jain

Fibers are the unit component for product development. They can be divided into two types: synthetic and natural fibers. Recently, emerging nanotechnology has played a vital role in advancing next-generation fabrics. The nanomaterials provide several unique properties such as higher conductivity, self-cleaning, water-resistant, and others. Owing to their advanced properties, the fabrics are being developed by coating and integrating with nanomaterials. Therefore, in the presented work two cotton samples were modified with titanium dioxide (TiO2) and zinc oxide (ZnO). These samples were further examined under various techniques including scanning electron microscopy (SEM), UV-visible spectroscopy, X-ray fluorescence (XRF), and Fourier-transform infrared spectroscopy (FTIR). Furthermore, these samples were evaluated at varying wavelengths with UV light and the obtained results demonstrated that the nano-coated fiber samples can be differentiated at 365 nm.


2020 ◽  
Vol 27 (09) ◽  
pp. 1950214 ◽  
Author(s):  
A. ATTA ◽  
A. M. ABDEL REHEEM ◽  
E. ABDELTWAB

Polymer nanocomposites composed of zinc oxide nanoparticles (ZnO NPs)-doped polyvinyl alcohol (PVA) polymer matrix have been synthesized using solvent casting preparation method. The ZnO/PVA polymer nanocomposite films are irradiated with different argon ion beam fluences using broad-beam ion source. The prepared films are characterized using X-ray diffraction (XRD), Fourier-transform infrared spectroscopy (FTIR), scanning electron microscopy (SEM) and UV–visible spectroscopy. The XRD shows that ZnO NPs are successfully formed on PVA polymer and the mean size of ZnO NPs is 31.2[Formula: see text]nm. The FTIR peaks indicate that ZnO NPs are attached to the polymer chains, whereas the SEM analysis shows that ZnO NPs are homogeneously dispersed into the PVA polymer surface. The optical bandgap, band tail width and number of carbon atoms in cluster are obtained and discussed using UV–visible spectroscopy. The transmittance is shown with low transmittance intensity in the UV region with the addition of ZnO NPs and ion beam irradiation. The optical bandgap [Formula: see text] showed significant decrease from 5.25[Formula: see text]eV for pristine PVA to 3.10[Formula: see text]eV by adding ZnO and from 3.10[Formula: see text]eV for un-irradiated ZnO/PVA to 2.98[Formula: see text]eV after being irradiated by [Formula: see text][Formula: see text]cm[Formula: see text]. The number of carbon atoms in cluster [Formula: see text] is increased by ZnO addition, whereas the Urbach energy [Formula: see text] is decreased. These results confirmed that there are significant modifications in PVA polymer, and the produced flexible ZnO/PVA is a good polymer nanocomposite film for technological applications.


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