Effect of a heterogeneity on tensile failure: interaction between fractures in a limestone

Author(s):  
Anne Pluymakers ◽  
Auke Barnhoorn ◽  
Richard Bakker

<p>Not all rocks are perfect. Frequently heterogeneities will be present, either in the form of pre-existing fractures, or in the form of sealed fractures. To date, investigation of sample heterogeneity, specifically tensile strength and strength anisotropy has focused on layered rocks, such as shales, sandstones and gneisses. Data is lacking on the effect of single planar heterogeneities, such as pre-existing fractures or stylolites, even though these frequently occur in geo-energy settings.</p><p>We have performed Brazilian Disc tests on limestone samples containing planar heterogeneities, investigating Brazilian test Strength (BtS) and the effects of orientation on strength. We used prefractured Indiana limestone to represent a planar heterogeneity without cohesion and Treuchtlinger Marmor samples with central stylolites to represent a planar heterogeneity of unknown strength (as an example of a sealed fracture). The planar discontinuity was set at different rotation angles of approximately 0–20–30–45–60–90⁰, where 90⁰ (steep angle) is parallel to the principal loading direction, and 0⁰ (low angle) to the horizontal axis of the sample. All experiments were filmed, and where possible Particle Image Velocimetry was used to determine internal particle motion. Moreover, we used a 2D Comsol model in which we simplified the stylolite surface as a sinusoid. The model was used to qualitatively determine how i) a different period of the sinusoid and ii) relative strength of sinusoid/matrix affect the results.</p><p>Our results show that all imperfect samples are weaker than intact samples. The 2D Comsol model indicates that the qualitative results remain unaffected by changing the period (assumed to be representative of roughness) of the cohesive heterogeneity, nor by the relative strength contrast: the location of the first fracture remains unaffected. For both heterogeneity types, the fracture patterns can be divided into four categories, with two clear endmembers, and a more diffusive subdivision in between.</p><p>For a cohesion-less heterogeneity:</p><ul><li>steep angles lead to frictional sliding along the interface, and only a small hypothesized permeability increase.</li> <li>Intermediate angles lead to a combination of tensile failure of the matrix and sliding along the interface, where for steeper angles more new fractures form which follow the path of the existing fracture.</li> <li>Low angles lead to closure of the old fracture and new tensile failure.</li> </ul><p>For a cohesive heterogeneity of unknown cohesion:</p><ul><li>Steep angles lead to intensive failure of the heterogeneous zone, attributed to the presence of a stress concentrator.</li> <li>Intermediate angles lead to partial failure along the heterogeneous zone, and the formation of new fractures in the matrix, potentially instigated by mode II failure to accommodate motion.</li> <li>Low angles lead to the formation of a new fracture plus opening within the heterogeneous zone.</li> </ul><p>These results imply that hydrofracture (i.e. creating tensile stresses) of a stylolite-rich zone will lead to more fractures than fractures in a homogeneous zone, where the orientation of the stylolites and bedding will control the orientation of the permeable pathways.</p>

2020 ◽  
Author(s):  
Anne Pluymakers ◽  
Richard Bakker ◽  
Auke Barnhoorn

<p>Not all rocks are perfect. Frequently heterogeneities will be present, either in the form of pre-existing fractures, or in the form of sealed fractures. Tensile strength and strength anisotropy of rocks has been investigated for strongly layered rocks, such as shales, sandstones and gneisses, but data is lacking on the effect of single planar heterogeneities, such as pre-existing fractures or stylolites. We have performed Brazilian Disc tests on limestone samples containing pre-existing fractures and stylolites, investigating Brazilian test Strength (BtS) and fracture orientation. We used Indiana limestone samples, pre-fractured with the Brazilian Disc method, and Treuchtlinger Marmor samples which contained central stylolites. All experiments were filmed. The planar discontinuity was set at different rotation angles of approximately 0–20–30–45–60–90⁰, where 90⁰ is parallel to the principal loading direction, and 0⁰ to the horizontal axis of the sample. Pre-fracturing Indiana limestone samples results in a cohesion-less planar discontinuity, whereas the stylolites in the Treuchtlinger Marmor samples are discontinuities which have some strength.</p><p>The results show that our imperfect samples with a planar discontinuity are always weaker than an intact sample. For the Indiana limestone, with a cohesion-less interface, there is 10 to 75% of weakening, which is angle-dependent. Once the angle is 30 or lower there is no influence from the initial fracture for the orientation of the new fracture. The stress-displacement pattern followed the expectation for Brazilian Disc testing. However, in the samples with a stylolite, strength is isotropic and between 25 and 65% of the strength of an intact sample. For all cases several new cracks appeared, of which the orientation is influenced by the orientation of the stylolite. The fracture pattern and associated stress drops are more complex for high angles. Interestingly, in the samples with stylolites, always more than one fracture was formed, whereas in the samples with a cohesionless interface usually only one new fracture formed, which for natural settings suggests a potential for higher fracture density when hydrofracturing a stylolite-rich interval.</p><p>A second difference between these datasets is the amplitude of the pre-existing interface. The effect of amplitude will be qualitatively investigated with a 2D Comsol model, to investigate the location of the first fracture occurring, which can then be compared to the camera data of the experiments.</p>


2016 ◽  
Vol 83 (5) ◽  
Author(s):  
Brian Nyvang Legarth ◽  
Qingda Yang

Failure in elastic dual-phase materials under transverse tension is studied numerically. Cohesive zones represent failure along the interface and the augmented finite element method (A-FEM) is used for matrix cracking. Matrix cracks are formed at an angle of 55 deg−60 deg relative to the loading direction, which is in good agreement with experiments. Matrix cracks initiate at the tip of the debond, and for equi-biaxial loading cracks are formed at both tips. For elliptical reinforcement the matrix cracks initiate at the narrow end of the ellipse. The load carrying capacity is highest for ligaments in the loading direction greater than that of the transverse direction.


1977 ◽  
Vol 99 (4) ◽  
pp. 634-640
Author(s):  
T. W. Thompson ◽  
S. Sen ◽  
K. E. Gray ◽  
T. F. Edgar

Tests have been carried out to quantify the variation in permeability of Texas lignite with drying and with applied stress. It has been shown that the matrix permeability of lignite may be increased from effectively zero to the order of 10 darcies by removing about 20 percent by weight of water. In addition, an increase of confining pressure after drying will reduce the permeability, but only by about one order of magnitude. Drying of the matrix thus may produce matrix permeabilities of the same order as the undried field fracture permeability. The permeability increase of the matrix is initially greater parallel to the bedding than perpendicular, but after further drying the two orientations show similar final permeabilities. This drying effect could have a significant influence on the operation of an in-situ gasification process by increasing the transmissivity and injectivity of the producing seam. Drying of the seam could occur by the flow of unsaturated gas and will be enhanced by combustion.


1993 ◽  
Vol 264 (4) ◽  
pp. L401-L405 ◽  
Author(s):  
R. A. Kaslovsky ◽  
L. Lai ◽  
K. Parker ◽  
A. B. Malik

Since polymorphonuclear leukocytes (PMN) rapidly migrate across the endothelial barrier and attach to extracellular matrix components, we tested the hypothesis that adhesion of PMN to matrix proteins can mediate endothelial injury following PMN activation. Studies were made using gelatin- and fibronectin-coated polycarbonate microporous filters (10 microns thick) on which confluent monolayers of bovine pulmonary microvessel endothelial cells were grown. PMN were layered either directly onto endothelial cells (at a ratio of 10:1) (“upright system”) or onto gelatin- and fibronectin-coated filters with the endothelial monolayer grown on the underside of the filter without contact between PMN and endothelial cells (“inverted system”). PMN were activated with phorbol 12-myristate 13-acetate (PMA; 5 x 10(-9) M) in both systems. PMN activation increased endothelial permeability to 125I-labeled albumin in upright as well as inverted systems. Pretreatment of PMN with anti-CD18 monoclonal antibodies IB4 or R15.7, which inhibited PMN adherence to matrix constituents as well as to endothelial cells, prevented the permeability increase in both configurations. This effect of anti-CD18 monoclonal antibodies (mAbs) was not ascribed to a reduction in PMN activation, since PMA-induced superoxide generation was unaffected. We conclude that activation of PMN adherent to extracellular matrix proteins increases endothelial permeability to albumin and that this response is dependent on PMN adhesion to the matrix. The results support the concept that PMN-mediated increase in endothelial permeability is the result of “targeted” release of PMN products independent of whether the PMN are adherent to the extracellular matrix or the endothelium.


1998 ◽  
Vol 275 (1) ◽  
pp. L126-L138 ◽  
Author(s):  
Theresa M. Curtis ◽  
Robert F. Rotundo ◽  
Peter A. Vincent ◽  
Paula J. McKeown-Longo ◽  
Thomas M. Saba

Exposure of confluent pulmonary arterial endothelial monolayers to tumor necrosis factor (TNF)-α causes both a reorganization and/or disruption of fibronectin (Fn) in the extracellular matrix and an increase in transendothelial protein permeability. However, the factors initiating this response to TNF-α have not been defined. Because TNF-α can induce proteinase expression in endothelial cells, we determined whether proteinases cause both the alteration of the Fn matrix and the permeability increase as is often speculated. Incubation of calf pulmonary arterial endothelial monolayers with TNF-α (200 U/ml) for 18 h caused a disruption of the Fn matrix and an increase in transendothelial protein permeability. A reduced colocalization of cell-surface α5β1-Fn integrins with the Fn fibers in focal contacts was also observed. TNF-α treatment of endothelial monolayers with matrices prelabeled with125I-human Fn (hFn) did not cause the release of Fn fragments or alter the content of Fn antigen in the medium as analyzed by SDS-PAGE coupled with autoradiography. Both the content and fragmentation pattern of Fn within the cell layer and the insoluble Fn matrix also appeared unchanged after TNF-α exposure as confirmed by Western immunoblot. Fn-substrate zymography revealed that TNF-α increased the expression of two proteinases within the conditioned medium in which activity could be blocked by aprotinin but not by EDTA, 1,10-phenanthroline, leupeptin, or pepstatin. However, inhibition of the Fn proteolytic activity of these two serine proteinases did not prevent either the TNF-α-induced disruption of the Fn matrix or the increase in permeability. Thus the reorganization and/or disruption of the Fn matrix and the temporally associated increase in endothelial permeability caused by TNF-α appear not to be due to proteolytic degradation of Fn within the extracellular matrix. In contrast, decreased α5β1-Fn integrin interaction with Fn fibers in the matrix may be important in the response to TNF-α exposure.


2008 ◽  
Vol 368-372 ◽  
pp. 713-716 ◽  
Author(s):  
Jiang Tao Zhang ◽  
Li Sheng Liu ◽  
Peng Cheng Zhai ◽  
Qing Jie Zhang

The dynamic compressive behavior of Al2O3 (10% vol.) / TiB2 ceramic composite had been tested by using a split Hopkinson pressure bar in this paper. The results show that the main failure modes of the ceramic composite include crushed failure and split fracture along the loading direction. The former is the typical compressive failure of brittle materials. The later is tensile failure along the flaws produced during the composite manufacturing. The numerical simulation was also used to study the effect of the diameter/length ratio of the samples on the experimental results. The effect of the deformation in the bars’ ends, which contacted with the samples, was also studied in the numerical models.


1994 ◽  
Vol 364 ◽  
Author(s):  
W. M. Yin ◽  
J. T. Guo ◽  
S. H. Wang ◽  
H. Li ◽  
M. H. Tan ◽  
...  

AbstractThe microstructure and mechanical properties of Ni3Al-based composites reinforced with TiC particles have been investigated. The composites, which contained 2, 6, 10 vol.%TiC particulate reinforcement, were fabricated by solidification processing method. The matrix alloy selected for this study was the advanced nickel-aluminide (Ni-16Al-8Cr-1Zr-0.8Mo-0.04B at.%).The optical micrographs revealed that the carbides in the composites distributed uniformly in the martix and appeared as fairly equiaxed particles. SEM observation showed that the interface between TiC and matrix is quite smooth, sharp and free of any phase. The test results indicated that the hardness was increased with increasing volume fraction of TiC particles at ambient temperature, and the composites exhibited higher hardness after 1100°C × 8h heat treatment. The yield strength has been improved due to reinforcement by the TiC particles at ambient and elevated temperature, but their ductility was reduced obviously. From SEM fractography, it could be seen that tensile failure occurred at the matrix / particulate interface.


1990 ◽  
Vol 5 (8) ◽  
pp. 1649-1655 ◽  
Author(s):  
G. E. Fuchs

The chemical compatibility and tensile properties of a powder processed intermetallic matrix composite (IMC) were investigated in the temperature range 298–1373 K. The matrix alloy selected for this study was the ORNL developed advanced nickel-aluminide IC-221 (Ni-16Al-8Cr-1Zr-0.05B at. %). The composite contained 25 vol. % TiC particulate reinforcement. TiC/IC-221 compatibility samples were heat treated at 1373 K for up to 1000 h. A layer enriched in Zr and Ti formed at the TiC/IC-221 interface after heat treatment. In addition, Ti was observed to diffuse into the matrix. The composite exhibited higher yield strength and lower ductility than a similarly processed matrix alloy at all test temperatures. Heat treatment of the composite improved the tensile properties due to particulate/matrix interaction, resulting in improved load transfer. SEM fractography revealed that tensile failure occurred at the matrix/prticulate interface. Remnants of the matrix were observed on TiC particles on the fracture surface, suggesting good matrix/particulate bonding. The mechanical properties of the composite were very competitive with Ni-base superalloys.


SPE Journal ◽  
2020 ◽  
Vol 25 (05) ◽  
pp. 2281-2295
Author(s):  
Abhishek Sarmah ◽  
Ahmed Farid Ibrahim ◽  
Hisham Nasr-El-Din ◽  
Jennifer Jackson

Summary In-situ gelled acids are used for acid diversion in heterogeneous carbonate reservoirs. However, most of the gelled systems are based on anionic polymers that are difficult to clean up after the acid treatments. Residual polymer deposition leads to formation damage by blocking pore throats in the matrix. This work evaluates a new cationic-polymer acid system with self-breaking ability for application as an acid diverter in carbonate reservoirs. Experimental studies have been conducted to examine the rheological properties of these polymer-based acid systems. The apparent viscosities of the live and the partially neutralized acids at pH from 0 to 5 were measured against the shear rate (0 to 1000 s−1). The effects of salinity and temperature (80 to 250°F) on the rheological properties of the acid system were also studied. The viscoelastic properties of the gelled acid system were evaluated using an oscillatory rheometer. Dynamic sweep tests were used to determine the elastic (G′) and viscous (G″) moduli of the system. Single-coreflood experiments were conducted on Indiana limestone cores to study the nature of diversion caused by the polymer-acid system. The effect of permeability contrast on the process of diversion was investigated by conducting dual-coreflood experiments on Indiana limestone cores that had permeability contrasts of 1.5 to 20. Computed tomography (CT) scans were conducted to study wormhole propagation after acid injection for both single and dual cores. The live acid system displayed a non-Newtonian shear-thinning behavior with the viscosity declining as temperature increased. For 5 wt% hydrochloric acid (HCl) and 20 gal/t polymer content at 10 s−1, the viscosity decreased from 230 to 40 cp as the temperature increased from 88 to 250°F. Acid-spending tests demonstrated that the acid generated a gel with improved viscosity of 260 cp (at 250°F and 10 s−1) after it reached a pH of 2. The highly viscous gel plugged the wormhole and forced the acid that followed to the next higher-permeability zone. The viscosity of the gel continued to increase until it broke down to 69 cp (at 250°F and 10 s−1) at a pH of 4.8, which indicates a self-breaking system and more thorough cleanup potential. Coreflood studies indicated that the wormhole and the diversion process are dependent on the temperature and the flow rate. There was no indication of any damage caused by the system. The injected acid pore volume to breakthrough (PVBT) decreased from 2.2 to 1.4 when the temperature increased from 150 to 250°F. The strong elastic nature of the gel (G′ = 3.976 Pa at 1 Hz) formed by the partially neutralized acid system proves its suitability as a candidate for use as a diverting agent. This new acid-polymer system has significant promise for use in acid diversion to improve stimulation of carbonate reservoirs.


2007 ◽  
Vol 04 (02) ◽  
pp. 249-275 ◽  
Author(s):  
A. TROISI ◽  
E. SÉRIÉ ◽  
R. KERNER

The non-abelian generalization of the Born–Infeld non-linear lagrangian is extended to the non-commutative geometry of matrices on a manifold. In this case, not only do the usual SU(n) gauge fields appear, but also a natural generalization of the multiplet of scalar Higgs fields, with the double-well potential as a first approximation. The matrix realization of non-commutative geometry provides a natural framework in which the notion of a determinant can be easily generalized and used as the lowest-order term in a gravitational lagrangian of a new kind. As a result, we obtain a Born–Infeld-like lagrangian as a root of sufficiently high order of a combination of metric, gauge potentials and the scalar field interactions. We then analyze the behavior of cosmological models based on this lagrangian. It leads to primordial inflation with varying speed, with possibility of early deceleration ruled by the relative strength of the Higgs field.


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