Incorporation of Carbon Nanotubes on Strategically De-Sized Carbon Fibers for Enhanced Interlaminar Shear Strength of Epoxy Matrix Composites

2019 ◽  
Vol 41 (4) ◽  
pp. 655-655
Author(s):  
Muhammad Abdul Basit Muhammad Abdul Basit ◽  
Sybt e anwar Qais Sybt e anwar Qais ◽  
Muhammad Saffee Ullah Malik and Ghufran Ur Rehman Muhammad Saffee Ullah Malik and Ghufran Ur Rehman ◽  
Faizan Siddique Awan Faizan Siddique Awan ◽  
Laraib Alam Khan and Tayyab Subhani Laraib Alam Khan and Tayyab Subhani

Carbon fiber reinforced polymeric matrix composites are enormously used in aerospace and automotive industries due to their enhanced specific properties. However, the area of interlaminar shear properties still needs investigation so as to produce composites with improved through-the-thickness properties. To improve interlaminar shear properties of these composites, acid-functionalized multiwalled carbon nanotubes were deposited on de-sized carbon fibers through electrophoretic deposition. De-sizing of carbon fabric was performed through three different methods: furnace heating, acidic treatment and chloroform usage. As the acid-treatment provided better results than other two techniques, the acid-de-sized carbon fibers were coated with nanotubes and subsequently incorporated in epoxy matrix to prepare a novel class of multiscale composites using vacuum assisted resin transfer molding technique. Nearly 30% rise in the interlaminar shear strength of the composites was obtained which was credited to the coating of nanotubes on the surface of carbon fibers. The increased adhesion between carbon fibers and epoxy matrix due to mechanical interlocking of nanotubes was found to be the possible reason of improved interlaminar shear properties.

2017 ◽  
Vol 36 (9) ◽  
pp. 640-654 ◽  
Author(s):  
Mateusz Koziol ◽  
Marcin Jesionek ◽  
Piotr Szperlich

The paper presents an attempt to evaluate the technically important properties of epoxy resin modified alternatively with multi-walled carbon nanotubes and flaked graphene. It is a presentation of experimental results supported by extensive referring to the professional literature. The nano-components were added in the amount which was economically justified and provides hope for a significant improvement of some of the properties of pure resin. Flowability, glass wettability, curing process and gelation time and curing shrinkage of the resin were evaluated. After the resin was cured, inner and outer hardness, thermal conductivity, flexural strength and impact resistance were measured. Glass fibre-reinforced laminates were also prepared with use of the nano-modified resin. The mechanical properties, interlaminar shear strength and flexural strength of the laminates, were evaluated for them. The obtained results showed either no effect or only technically slight effect of the nano-modification on the evaluated properties. Noticeable improvement in interlaminar shear strength and impact resistance for laminates containing resin filled with graphene can predestine this kind of modification as a method of increasing the delamination resistance of laminates.


2009 ◽  
Vol 79-82 ◽  
pp. 497-500 ◽  
Author(s):  
Lei Chen ◽  
Zhi Wei Xu ◽  
Jia Lu Li ◽  
Xiao Qing Wu ◽  
Li Chen

The γ-ray co-irradiation method was employed to study the effect of diethanolamine modification on the surface of carbon fiber (CF) and the interfacial properties of CF/epoxy composites. Compared with the original carbon fiber, the surface of modified fibers became rougher. The amount of oxygen-containing functional groups was increased and the nitrogen element was detected after irradiation grafting. The interlaminar shear strength (ILSS) of composites reinforced by carbon fibers irradiated in diethanolamine solution was increased and then decreased as the irradiation dose increased. The ILSS of CF/epoxy composites was enhanced by 16.1% at 200kGy dose, compared with that of untreated one. The γ-ray irradiation grafting is expected to be a promising method for the industrialized modification of carbon fibers.


2021 ◽  
pp. 152808372110523
Author(s):  
Kumaresan Gladys Ashok ◽  
Kalaichelvan Kani

In the present study, the significance of nanofiller lead oxide (PbO) on the dynamic mechanical analysis (DMA) and interlaminar shear strength (ILSS) performance of luffa fiber–reinforced epoxy composites was investigated. The epoxy matrix was altered with nanofiller PbO of different weight percent through a mechanical stirring process. The PbO-added luffa fiber epoxy composites were made through hand layup preceded by the compression molding method. The prepared composite samples were investigated for ILSS and DMA. The test results lead to the inference that the 1.25 wt% PbO nanofiller–added composite samples attained 25%, 17%, and 55% of higher loss modulus, storage modulus, and ILSS, respectively, as compared with the other prepared samples. The morphological investigation was conducted on the fractured surface of the interlaminar tested samples. The micrographic images show the bonding nature of the luffa fiber with the epoxy matrix, fiber breakage, and fiber pullouts. The characterization studies such as FTIR, XRD, and EDX were conducted on the fabricated composite samples. The XRD studies show that the rise in weight percent of the nanofiller PbO enhances the crystallinity of the composite samples. Moreover, the composite sample prepared with 1.25 wt% nanofiller PbO can be used to prepare low-cost roofing materials for sustainable housing projects.


Materials ◽  
2019 ◽  
Vol 12 (5) ◽  
pp. 778 ◽  
Author(s):  
Elwathig. Hassan ◽  
Tienah. Elagib ◽  
Hafeezullah Memon ◽  
Muhuo Yu ◽  
Shu Zhu

Due to the non-polar nature and low wettability of carbon fibers (CFs), the interfacial adhesion between CFs and the polyetheretherketone (PEEK) matrix is poor, and this has negative effects on the mechanical properties of CF/PEEK composites. In this work, we established a modification method to improve the interface between CFs and PEEK based chemical grafting of aminated polyetheretherketone (PEEK-NH2) on CFs to create an interfacial layer which has competency with the PEEK matrix. The changed chemical composition, surface morphology, surface energy, and interlaminar shear strength were investigated. After grafting, the interlaminar shear strength (ILSS) was improved by 33.4% due to the covalent bonds in the interface region, as well as having good compatibility between the interface modifier and PEEK. Finally, Dynamic Mechanical Analysis (DMA) and Scanning Electron Microscopy (SEM) observation also confirmed that the properties of the modified CF/PEEK composites interface were enhanced. This work is, therefore, a beneficial approach towards enhancing the mechanical properties of thermoplastic composites by controlling the interface between CFs and the PEEK matrix.


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