Addition of a small amount of multiwalled carbon nanotubes and flaked graphene to epoxy resin

2017 ◽  
Vol 36 (9) ◽  
pp. 640-654 ◽  
Author(s):  
Mateusz Koziol ◽  
Marcin Jesionek ◽  
Piotr Szperlich
Keyword(s):  
Carbon Nanotubes ◽  
Shear Strength ◽  
Flexural Strength ◽  
Epoxy Resin ◽  
Impact Resistance ◽  
Gelation Time ◽  
Interlaminar Shear Strength ◽  
Multiwalled Carbon ◽  
Professional Literature ◽  
Interlaminar Shear

The paper presents an attempt to evaluate the technically important properties of epoxy resin modified alternatively with multi-walled carbon nanotubes and flaked graphene. It is a presentation of experimental results supported by extensive referring to the professional literature. The nano-components were added in the amount which was economically justified and provides hope for a significant improvement of some of the properties of pure resin. Flowability, glass wettability, curing process and gelation time and curing shrinkage of the resin were evaluated. After the resin was cured, inner and outer hardness, thermal conductivity, flexural strength and impact resistance were measured. Glass fibre-reinforced laminates were also prepared with use of the nano-modified resin. The mechanical properties, interlaminar shear strength and flexural strength of the laminates, were evaluated for them. The obtained results showed either no effect or only technically slight effect of the nano-modification on the evaluated properties. Noticeable improvement in interlaminar shear strength and impact resistance for laminates containing resin filled with graphene can predestine this kind of modification as a method of increasing the delamination resistance of laminates.

Incorporation of Carbon Nanotubes on Strategically De-Sized Carbon Fibers for Enhanced Interlaminar Shear Strength of Epoxy Matrix Composites

2019 ◽  
Vol 41 (4) ◽  
pp. 655-655
Author(s):  
Muhammad Abdul Basit Muhammad Abdul Basit ◽  
Sybt e anwar Qais Sybt e anwar Qais ◽  
Muhammad Saffee Ullah Malik and Ghufran Ur Rehman Muhammad Saffee Ullah Malik and Ghufran Ur Rehman ◽  
Faizan Siddique Awan Faizan Siddique Awan ◽  
Laraib Alam Khan and Tayyab Subhani Laraib Alam Khan and Tayyab Subhani
Keyword(s):  
Carbon Nanotubes ◽  
Shear Strength ◽  
Carbon Fibers ◽  
Epoxy Matrix ◽  
Interlaminar Shear Strength ◽  
Matrix Composites ◽  
Multiwalled Carbon ◽  
Shear Properties ◽  
Functionalized Multiwalled Carbon Nanotubes ◽  
Interlaminar Shear

Carbon fiber reinforced polymeric matrix composites are enormously used in aerospace and automotive industries due to their enhanced specific properties. However, the area of interlaminar shear properties still needs investigation so as to produce composites with improved through-the-thickness properties. To improve interlaminar shear properties of these composites, acid-functionalized multiwalled carbon nanotubes were deposited on de-sized carbon fibers through electrophoretic deposition. De-sizing of carbon fabric was performed through three different methods: furnace heating, acidic treatment and chloroform usage. As the acid-treatment provided better results than other two techniques, the acid-de-sized carbon fibers were coated with nanotubes and subsequently incorporated in epoxy matrix to prepare a novel class of multiscale composites using vacuum assisted resin transfer molding technique. Nearly 30% rise in the interlaminar shear strength of the composites was obtained which was credited to the coating of nanotubes on the surface of carbon fibers. The increased adhesion between carbon fibers and epoxy matrix due to mechanical interlocking of nanotubes was found to be the possible reason of improved interlaminar shear properties.

Mechanical properties of multiwall carbon nanotubes/unidirectional carbon fiber-reinforced epoxy hybrid nanocomposites in transverse and longitudinal fiber directions

2021 ◽  
pp. 096739112098651
Author(s):  
Saeedeh Saadatyar ◽  
Mohammad Hosain Beheshty ◽  
Razi Sahraeian
Keyword(s):  
Mechanical Properties ◽  
Shear Strength ◽  
Epoxy Resin ◽  
Interlaminar Shear Strength ◽  
Lap Shear Strength ◽  
Transverse Tensile ◽  
Lap Shear ◽  
Longitudinal Fiber ◽  
Interlaminar Shear ◽  
Multiwall Carbon

Unidirectional carbon fiber-reinforced epoxy (UCFRE) is suffering from weak transverse mechanical properties and through-thickness properties. The effect of different amount (0.1, 0.3 and 0.5 phr which is proportional to 0.09, 0.27 and 0.46 wt%, respectively) of multiwall carbon nanotube (MWCNT), on transverse tensile properties, flexural strength, fracture toughness in transverse and longitudinal fiber directions, interlaminar shear strength and lap shear strength of UCFRE has been investigated. Dicyandiamide was used as a thermal curing agent of epoxy resin. MWCNT was dispersed in the epoxy resin by ultrasonic instrument and their dispersion state was investigated by scanning electron microscopy (SEM). The curing behavior of epoxy resin and its nanocomposites was assessed by differential scanning calorimetry. Results show that transverse tensile strength, modulus and strain-at-break were increased by 28.5%, 25% and 14%, respectively by adding 0.1 phr of MWCNT. Longitudinal flexural properties of UCFRE was not changed by adding different amount of MWCNT. Although longitudinal flexural strength was increased by 5% by adding 0.1 phr of MWCNT. Fracture toughness in transverse and longitudinal fiber directions was increased by 39% and 9%, respectively at 0.3 phr of MWCNT. Results also show that interlaminar shear strength and lap shear strength were increased at 0.3 phr of MWCNT by 8% and 5%, respectively. These increases in mechanical properties were due to the good adhesion of fibers to the matrix, interlocking and toughening action of MWCNT as revealed by SEM.

scholarly journals Chopped Strand/Plain Weave E-Glass as Reinforcement in Vacuum Bagged Epoxy Composites

2015 ◽  
Vol 2015 ◽  
pp. 1-7 ◽  
Author(s):  
Srinivas Shenoy Heckadka ◽  
Suhas Yeshwant Nayak ◽  
Karan Narang ◽  
Kirti Vardhan Pant
Keyword(s):  
Shear Strength ◽  
Composite Laminates ◽  
Polymer Matrix Composites ◽  
Impact Resistance ◽  
Interlaminar Shear Strength ◽  
Fiber Volume ◽  
Glass Composites ◽  
Plain Weave ◽  
Specific Strength ◽  
Interlaminar Shear

Polymer matrix composites are one of the materials being extensively researched and are gaining a lot of importance due to advantages like high specific strength, greater flexibility in design, and reduced cost of manufacturing. In this study, tensile, flexural, impact, and interlaminar shear strength of chopped strand/plain weave E-glass composites were considered. Composite laminates with different stacking sequence were fabricated using Vacuum Assisted Resin Infusion Moulding (VARIM) technique. Fiber volume fractions (FVF) of 22%, 26%, and 30% were adopted. Experiments were conducted in accordance with ASTM standards. Results indicate that laminates with three layers of plain weave mat exhibited better tensile, flexural, and interlaminar shear strength. However, laminates with two layers of chopped strand mat and one layer of plain weave mat showed improved impact resistance. In addition, scanning electron microscopy was used to analyze the fracture surface.

scholarly journals Comparison of the Processing of Epoxy Resins in Pultrusion with Open Bath Impregnation and Closed-Injection Pultrusion

2019 ◽  
Vol 3 (3) ◽  
pp. 87 ◽  
Author(s):  
Sebastian Strauß ◽  
Andreas Senz ◽  
Jessica Ellinger
Keyword(s):  
Shear Strength ◽  
Epoxy Resin ◽  
Epoxy Resins ◽  
Interlaminar Shear Strength ◽  
Time Interval ◽  
Bending Stress ◽  
Epoxy Resin System ◽  
Pot Life ◽  
Interlaminar Shear ◽  
Composite Properties

In this study, the influence of the open bath and closed-injection pultrusion (CIP) processing methods of epoxy resins on the quality of glass fiber composites was investigated. In addition to the state-of-the-art epoxy resin system with long pot life, new resin systems with short pot life have recently been developed. These systems require processing by closed-injection pultrusion. The epoxies with long pot life allow both processing variants. The experimental work was carried out with two types of injection and impregnation chambers (ii_chamber), namely with a conical and a teardrop design. Fully impregnated composites, which were used for further analyses, could be produced by using the conical ii_chamber. The composite properties of the open bath and the conical ii_chamber impregnation methods were compared. No significant influence on the bending stress could be determined; the interlaminar shear strength was up to 10% better with open bath impregnation than with ii_chamber. For the composites investigated, it was shown that the open bath and ii_chamber impregnation methods can be used to produce parts with partially comparable properties, as demonstrated for the epoxy formulation with long pot life. These results indicate that processing of epoxy systems with a short pot life is also possible by closed-injection pultrusion. Furthermore, the influence on the composite properties of the time interval between the mixing of an epoxy resin and processing in an open bath was investigated. No significant effect on the bending stress and interlaminar shear strength could be determined.

scholarly journals Effect of Graphene Additive on Flexural and Interlaminar Shear Strength Properties of Carbon Fiber-Reinforced Polymer Composite

2020 ◽  
Vol 4 (4) ◽  
pp. 162
Author(s):  
Mohamed Ali Charfi ◽  
Ronan Mathieu ◽  
Jean-François Chatelain ◽  
Claudiane Ouellet-Plamondon ◽  
Gilbert Lebrun
Keyword(s):  
Mechanical Properties ◽  
Shear Strength ◽  
Carbon Fiber ◽  
Flexural Strength ◽  
Interlaminar Shear Strength ◽  
Fiber Reinforced Polymer ◽  
Carbon Fiber Reinforced Polymer ◽  
Adhesion Properties ◽  
Reinforced Polymer ◽  
Interlaminar Shear

Composite materials are widely used in various manufacturing fields from aeronautic and aerospace industries to the automotive industry. This is due to their outstanding mechanical properties with respect to their light weight. However, some studies showed that the major flaws of these materials are located at the fiber/matrix interface. Therefore, enhancing matrix adhesion properties could significantly improve the overall material characteristics. This study aims to analyze the effect of graphene particles on the adhesion properties of carbon fiber-reinforced polymer (CFRP) through interlaminar shear strength (ILSS) and flexural testing. Seven modified epoxy resins were prepared with different graphene contents. The CFRP laminates were next manufactured using a method that guarantees a repeatable and consistent fiber volume fraction with a low porosity level. Short beam shear and flexural tests were performed to compare the effect of graphene on the mechanical properties of the different laminates. It was found that 0.25 wt.% of graphene filler enhanced the flexural strength by 5%, whilst the higher concentrations (2 and 3 wt.%) decreased the flexural strength by about 7%. Regarding the ILSS, samples with low concentrations (0.25 and 0.5 wt.%) demonstrated a decent increase. Meanwhile, 3 wt.% slightly decreases the ILSS.

Preparation and Characterization of Structural Damping Composites Toughened by Polyamide Nonwoven Fabrics

2016 ◽  
Vol 848 ◽  
pp. 189-195
Author(s):  
Nan Nan Ni ◽  
Yue Fang Wen ◽  
De Long He ◽  
Miao Cai Guo ◽  
Xiao Su Yi
Keyword(s):  
Shear Strength ◽  
Composite Laminates ◽  
Impact Resistance ◽  
Nonwoven Fabric ◽  
Mechanical Analysis ◽  
Interlaminar Shear Strength ◽  
Structural Damping ◽  
Nonwoven Fabrics ◽  
Compression After Impact ◽  
Interlaminar Shear

A new kind of structural damping composites was prepared by interleaving polyamide nonwoven fabrics (PNF) between the carbon fiber reinforced epoxy composite laminates. The damping behaviors of the composites made were experimentally investigated using cantilever beam test and dynamic mechanical analysis. The damping ratios of the nonwoven fabrics interleaved composites were compared with the ones of non-interleaved composites. In addition, the interlaminar shear strength and flexible modulus of the composites were also investigated, as well as the composite compression after impact (CAI), Mode I and Mode II interlaminar fracture toughness (GIC and GIIC), in order to evaluate the influence of the polyamide nonwoven fabric layers on the composite mechanical properties. It has been observed that the interleaved polyamide nonwoven fabric layers greatly improved the composite damping loss factors, and the composites containing 7 layers of PNF showed the best damping behavior. Meanwhile, the addition of PNF showed a negligible influence on the composite flexible strength and modulus and interlaminar shear strength. Most importantly, the CAI, GIC and GIIC tests indicated that the composite interlaminar toughness and impact resistance were significantly improved by the interleaved PNF. Finally, the reinforcing mechanism of this kind of composites is discussed.

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