scholarly journals A Combination of Water-Steam Distillation and Solvent Extraction of Cananga Odorata Essential Oil

2012 ◽  
Vol 02 (10) ◽  
pp. 05-12
Author(s):  
Megawati Saputra
Keyword(s):  
Solvent Extraction ◽  
Essential Oil ◽  
Steam Distillation ◽  
Water Steam ◽  
Cananga Odorata

scholarly journals Kualitas, Komposisi Kimia, dan Aktivitas Anti Oksidan Minyak Kenanga (Cananga odorata)

2016 ◽  
Vol 9 (1) ◽  
pp. 3 ◽  
Author(s):  
Rini Pujiarti ◽  
Titis Budi Widowati ◽  
Kasmudjo ◽  
Sigit Sunarta
Keyword(s):  
Chemical Composition ◽  
Steam Distillation ◽  
Antioxidative Activity ◽  
Positive Control ◽  
Benzyl Benzoate ◽  
Water Steam ◽  
Germacrene D ◽  
Dpph Scavenging ◽  
Dpph Scavenging Assay ◽  
Cananga Odorata

Minyak kenanga pada penelitian ini diperoleh dari bunga kenanga segar dengan penyulingan cara pengukusan. Uji kualitas fisik minyak kenanga cukup memuaskan dan sesuai dengan standar SNI 06-3949-1005. Komposisi kimia minyak kenangan diuji menggunakan GC-MS. Hasil analisis GC-MS mengidentifikasikan adanya 23 komponen kimia penyusun minyak kenanga. Komponen utama penyusun minyak kenanga yang dihasilkan pada penelitian ini adalah caryophyllene (36,44%), â-linalool (5,97%), á-caryophyllene (9,61%), germacrene D (17,23%), dan benzyl benzoate (7,18%). Pengujian antioksidan minyak kenanga dengan metode DPPH scavenging assay menunjukkan aktivitas antioksidan yang lembut dari minyak kenangan (IC50: 2,29 mg/ml) jika dibandingkan dengan kontrol positif BHA (IC50: 0,03 mg/ml). Penelitian ini mengidentifikasikan bahwa minyak kenanga memiliki potensi sebagai antioksidan alami yang lembut.Kata kunci: Cananga odorata, minyak atsiri, kualitas, komposisi kimia, antioksidan.  Quality, chemical composition, and antioxidative activity of cananga (Cananga odorata) oilAbstractCananga oil in this study was obtained from fresh flowers of Cananga odorata by water-steam distillation. The result of physical properties of cananga oil were compared with the SNI 06-3949-1005 showed that cananga oil was satisfied the quality prescribed by standard. The chemical composition of cananga oil was analyzed by GC-MS. GC-MS analysis showed that 23 compounds have been identified. The main compounds of cananga oil were caryophyllene (36.44%), â-linalool (5.97%), á-caryophyllene (9.61%), germacrene D (17.23%) and benzyl benzoate (7.18%). The DPPH scavenging assay showed that cananga oil possess mild antioxidant activity (IC50: 2.29 mg/ml) if compared with positive control of BHA (IC50: 0.03 mg/ml). This study indicated that cananga oil has potency as mild natural antioxidant. 

Comparative Analysis of Essential Oil Components from Golden Pomelo Peel by Steam Distillation and Solvent Extraction

2011 ◽  
Vol 29 (1) ◽  
pp. 130-133 ◽  
Author(s):  
Yue-Lin ZHU ◽  
Zeng-Hua CHANG ◽  
Xiao-Mei ZHENG ◽  
Zhi-Ping HUANG ◽  
Kai-Wen XIAO
Keyword(s):  
Comparative Analysis ◽  
Solvent Extraction ◽  
Essential Oil ◽  
Steam Distillation ◽  
Pomelo Peel ◽  
Oil Components

Yield and Composition of Indonesian Cananga Oil Obtained by Steam Distillation and Organic Solvent Extraction

2012 ◽  
Vol 8 (3) ◽  
Author(s):  
Magdalena Kristiawan ◽  
Vaclav Sobolik ◽  
Karim Allaf
Keyword(s):  
Solvent Extraction ◽  
Organic Solvent ◽  
Steam Distillation ◽  
Volatile Oil ◽  
Oil Composition ◽  
Hexane Extraction ◽  
Oxygenated Compounds ◽  
First Order Kinetics ◽  
Organic Solvent Extraction ◽  
Cananga Odorata

Abstract Cananga oil has high economical value because of its utilisation as fragrance and food flavour. In the present work, the oil was isolated by steam distillation and organic solvent extraction from dry mature flowers of Cananga odorata Hook. fil. et Thomson, forma macrophylla. Chloroform and hexane were used as solvents with different polarities. The yield of volatile oil and its grouped compounds (LOC, sesquiterpenes hydrocarbons and HOC) was investigated as a function of time. LOC consists of oxygenated monoterpenes and other light oxygenated compounds whereas HOC comprises oxygenated sesquiterpenes and other heavy oxygenated compounds. The oil yields of 5.1, 3.8 and 2.5 % dry matter were obtained with chloroform (8 h), hexane (8 h) and steam distillation (16 h), respectively. The isolation rate was described by a first-order kinetics equation. The rate was lowest with steam distillation, intermediate with hexane extraction and best with chloroform extraction. The oil composition was analyzed by gas chromatography coupled to mass spectrometry. The steam-distilled oil and chloroform oil had a similar composition, with a high content of oxygenated compounds (61.7% and 58.3%), while hexane oil was rich in sesquiterpenes hydrocarbons (66.5%).

scholarly journals Essential Oil Variability of Azorean Cryptomeriajaponica Leaves under Different Distillation Methods, Part 1: Color, Yield and Chemical Composition Analysis

2022 ◽  
Vol 12 (1) ◽  
pp. 452
Author(s):  
Filipe Arruda ◽  
José S. Rosa ◽  
Ana Rodrigues ◽  
Luísa Oliveira ◽  
Ana Lima ◽  
...  
Keyword(s):  
Essential Oil ◽  
Steam Distillation ◽  
Plant Protection ◽  
Green Plant ◽  
Quantitative Composition ◽  
Composition Analysis ◽  
Chemical Profile ◽  
Water Steam ◽  
Azores Archipelago ◽  
Color Yield

This study mainly deals with the effect of hydrodistillation (HD) and water-steam distillation (WSD) methods on the color, yield, and chemical profile of the essential oil (EO) from Cryptomeria japonica fresh leaves from São Miguel Island (Azores Archipelago, Portugal). The yields of EO–HD (pale-yellowish) and EO–WSD (colorless) samples were 1.21% and 0.45% (v/w), respectively. The GC–FID, GC–MS, and 13C-NMR analyses of EO–HD vs. EO–WSD revealed (i) a high-content of monoterpenes (72.8% vs. 86.7%), mainly α-pinene (34.5% vs. 46.4%) and sabinene (20.2% vs. 11.6%), and oxygenated mono- and sesquiterpenes (20.2% vs. 9.6%); (ii) similar sesquiterpene (1.6% vs. 1.6%), β-myrcene (5.9% vs. 5.8%), and camphene (3.5% vs. 3.8%) contents; and (iii) significant differences in other classes/components: EO–HD is richer in oxygenated sesquiterpenes (17.1%, mainly elemol (10.4%) and α-eudesmol (3.4%)) and diterpenes (3%; mostly phyllocladene), while EO–WSD is richer in oxygenated monoterpenes (7.2%, mainly terpinen-4-ol (5.4%)), p-cymene (4.4%), and limonene (3.2%). Overall, the color, yield, and quantitative composition of the EO samples studied are strongly influenced by the distillation method. Nonetheless, this C. japonica leaf EO displayed a consistent α-pinene- and sabinene-rich composition. The same chemotype was found in a commercial Azorean C. japonica leaf EO sample, obtained by industrial steam distillation (SD), as well as in Corsica C. japonica leaf EO–HD. Furthermore, the bioactive composition of our EO samples revealed the potential to be used in green plant protection and in the medical, food, cosmetic, and household industries.

Anti-Neuropathic Pain Activity of Ageratum conyzoides L due to The Essential Oil Components

2020 ◽  
Vol 19 ◽  
Author(s):  
Yedy Purwandi Sukmawan ◽  
Kusnandar Anggadiredja ◽  
I Ketut Adnyana
Keyword(s):  
Neuropathic Pain ◽  
Essential Oil ◽  
Opioid Receptor ◽  
Steam Distillation ◽  
Chronic Constriction Injury ◽  
Thermal Hyperalgesia ◽  
Ageratum Conyzoides ◽  
Safety And Efficacy ◽  
Activity Test ◽  
Oil Components

Background: Neuropathic pain is one of the contributors to the global burdens of illness. At present many patients do not achieve satisfactory pain relief even with synthetic pain-killers. Taking this into consideration, it is necessary to search for natural product-derived alternative treatment with confirmed safety and efficacy. Ageratum conyzoides L is a plant often used as analgesic in Indonesia, however, anti-neuropathic pain activity of this plant is still unknown. Objective: To determine the anti-neuropathic pain activity of the essential oil and non-essential oil component (distillation residue) of A. conyzoides L. Methods: We conducted separation of the essential oil component from other secondary metabolites through steam distillation. Both components were tested for anti-neuropathic pain activity using chronic constriction injury animal models with thermal hyperalgesia and allodynia tests. The animals were divided into 7 test groups namely normal, sham, negative, positive (pregabalin at 0.195 mg/20 g BW of mice), essential oil component (100 mg/kg BW), and non-essential oil component (100 mg/kg BW). Naloxone was tested against the most potent anti-neuropathic pain component (essential oil or nonessential oil) to investigate the involvement of opioid receptor. Results: The GC-MS of the essential oil component indicated the presence of 60 compounds. Meanwhile, non-essential oil components contained alkaloid, flavonoid, polyphenol, quinone, steroid, and triterpenoid. This non-essential oil component contained a total flavonoid equivalent to 248.89 ppm quercetin. The anti-neuropathic pain activity test showed significantly higher activity of the essential oil component compared to the non-essential oil component and negative groups (p<0.05). Furthermore, the essential oil component showed equal activity to pregabalin (p>0.05). However, this activity was abolished by naloxone, indicating the involvement of opioid receptor in the action of the essential oil component. Conclusion: The essential oil component of A. conyzoides L is a potential novel substance for use as anti-neuropathic pain.

scholarly journals Innovation in a Continuous System of Distillation by Steam to Obtain Essential Oil from Persian Lime Juice (Citrus latifolia Tanaka)

Molecules ◽  
2021 ◽  
Vol 26 (14) ◽  
pp. 4172
Author(s):  
José Daniel Padilla-de la Rosa ◽  
Magaly Dyanira Manzano-Alfaro ◽  
Jaime Rosalío Gómez-Huerta ◽  
Enrique Arriola-Guevara ◽  
Guadalupe Guatemala-Morales ◽  
...  
Keyword(s):  
Essential Oil ◽  
Oil Recovery ◽  
Steam Distillation ◽  
Optical Rotation ◽  
Process Time ◽  
Chemical Compositions ◽  
Distillation Process ◽  
Steam Consumption ◽  
Lime Juice ◽  
Oil Fractions

The citrus industry is one of the most important economic areas within the global agricultural sector. Persian lime is commonly used to produce lime juice and essential oil, which are usually obtained by batch distillation. The aim of this work was to validate a patented continuous steam distillation process and to both physically and chemically characterize the volatile fractions of essential Persian lime oil. Prior to distillation, lime juice was obtained by pressing the lime fruit. Afterwards, the juice was subjected to a continuous steam distillation process by varying the ratio of distillate flow to feed flow (0.2, 0.4, and 0.6). The distillate oil fractions were characterized by measuring their density, optical rotation, and refractive index. Gas chromatography GC-FID was used to analyze the chemical compositions of the oil fractions. The process of continuous steam distillation presented high oil recovery efficiencies (up to 90%) and lower steam consumption compared to traditional batch process distillation since steam consumption ranged from 32 to 60% for different steam levels. Moreover, a reduction in process time was observed (from 8 to 4 h). The oil fractions obtained via continuous steam distillation differed significantly in their composition from the parent compounds and the fractions.

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