scholarly journals Innovation in a Continuous System of Distillation by Steam to Obtain Essential Oil from Persian Lime Juice (Citrus latifolia Tanaka)

Molecules ◽  
2021 ◽  
Vol 26 (14) ◽  
pp. 4172
Author(s):  
José Daniel Padilla-de la Rosa ◽  
Magaly Dyanira Manzano-Alfaro ◽  
Jaime Rosalío Gómez-Huerta ◽  
Enrique Arriola-Guevara ◽  
Guadalupe Guatemala-Morales ◽  
...  
Keyword(s):  
Essential Oil ◽  
Oil Recovery ◽  
Steam Distillation ◽  
Optical Rotation ◽  
Process Time ◽  
Chemical Compositions ◽  
Distillation Process ◽  
Steam Consumption ◽  
Lime Juice ◽  
Oil Fractions

The citrus industry is one of the most important economic areas within the global agricultural sector. Persian lime is commonly used to produce lime juice and essential oil, which are usually obtained by batch distillation. The aim of this work was to validate a patented continuous steam distillation process and to both physically and chemically characterize the volatile fractions of essential Persian lime oil. Prior to distillation, lime juice was obtained by pressing the lime fruit. Afterwards, the juice was subjected to a continuous steam distillation process by varying the ratio of distillate flow to feed flow (0.2, 0.4, and 0.6). The distillate oil fractions were characterized by measuring their density, optical rotation, and refractive index. Gas chromatography GC-FID was used to analyze the chemical compositions of the oil fractions. The process of continuous steam distillation presented high oil recovery efficiencies (up to 90%) and lower steam consumption compared to traditional batch process distillation since steam consumption ranged from 32 to 60% for different steam levels. Moreover, a reduction in process time was observed (from 8 to 4 h). The oil fractions obtained via continuous steam distillation differed significantly in their composition from the parent compounds and the fractions.

scholarly journals Physico-chemical evaluation of Rosmarinus officinalis L. essential oils

2005 ◽  
Vol 48 (6) ◽  
pp. 1035-1039 ◽  
Author(s):  
Ana Cristina Atti-Santos ◽  
Marcelo Rossato ◽  
Gabriel Fernandes Pauletti ◽  
Luciana Duarte Rota ◽  
Juarez Ciro Rech ◽  
...  
Keyword(s):  
Steam Distillation ◽  
Optical Rotation ◽  
Volatile Oil ◽  
Rosmarinus Officinalis ◽  
Chemical Compositions ◽  
Chemical Parameters ◽  
Alpha Pinene ◽  
Chemical Evaluation ◽  
Physico Chemical ◽  
Rosmarinus Officinalis L

Nineteen samples of Rosmarinus officinalis were extracted by steam distillation in a pilot plant and evaluated in terms of chemical compositions and physico-chemical characteristics. The volatile oil yields ranged from 0.37% (1999 harvest) to 0.49% (1998 harvest). Twenty components were identified in the oils. The major components were alpha-pinene (40.55 to 45.10%), 1,8-cineole (17.40 to 19.35%), camphene (4.73 to 6.06%) and verbenone (2.32 to 3.86%). The physico-chemical parameters averaged 0.8887 g/cm³ for specific gravity, 1.4689 for refractive index, and +11.82° for optical rotation, and there were no significant variations in either the chemical or physico-chemical data in the different years.

scholarly journals First Report on Yield and Chemical Composition of Essential Oil Extracted from Myrcia eximia DC (Myrtaceae) from the Brazilian Amazon

Molecules ◽  
2020 ◽  
Vol 25 (4) ◽  
pp. 783
Author(s):  
Oberdan Oliveira Ferreira ◽  
Jorddy Neves da Cruz ◽  
Celeste de Jesus Pereira Franco ◽  
Sebastião Gomes Silva ◽  
Wanessa Almeida da Costa ◽  
...  
Keyword(s):  
Gas Chromatography ◽  
Chemical Composition ◽  
Essential Oil ◽  
Steam Distillation ◽  
Brazilian Amazon ◽  
Major Constituent ◽  
Chemical Compositions ◽  
Mass Yield ◽  
New Information ◽  
The City

The essential oil (EO) of plants of the Myrtaceae family has diverse chemical composition and several applications. However, data on the oil yield, its composition, and its complete chemistry are still unavailable for some species belonging to this family, such as Myrcia eximia DC. In this study, the chemical compositions of the EOs of Myrcia eximia were evaluated by using gas chromatography (GC) alone and gas chromatography coupled with mass spectrometry (GC–MS). Samples for both evaluations were collected from the city of Magalhães Barata, State of Pará, Brazil, in 2017 and 2018. For the plant material collected in 2017, EO was obtained by hydrodistillation (HD) only, while, for the material collected in 2018, EO was obtained by hydrodistillation and steam distillation (SD), in order to evaluate the differences in chemical composition and mass yield of the EO. The yields of (E)-caryophyllene were 15.71% and 20.0% for the samples collected by HD in 2017 and 2018, respectively, while the yield was 15.0% for the sample collected by SD in 2018. Hexanal was found to be the major constituent in the EO obtained by HD, with yield of up to 26.09%. The oil yields reached 0.08% by using SD, and 0.01% and 0.36% for the samples collected in 2017 and 2018, respectively, using HD. The results of this study provide new information about the mass yield and chemical composition of Myrcia eximia DC, and they can add value and income to traditional populations, as well as facilitate the preservation of this species.

scholarly journals Chemical Composition and Antioxidant Activity of Steam-Distilled Essential Oil and Glycosidically Bound Volatiles from Maclura Tricuspidata Fruit

Foods ◽  
2019 ◽  
Vol 8 (12) ◽  
pp. 659 ◽  
Author(s):  
Gyung-Rim Yong ◽  
Yoseph Asmelash Gebru ◽  
Dae-Woon Kim ◽  
Da-Ham Kim ◽  
Hyun-Ah Han ◽  
...  
Keyword(s):  
Antioxidant Activity ◽  
Essential Oil ◽  
Steam Distillation ◽  
Antioxidant Activities ◽  
Natural Antioxidants ◽  
Gas Chromatography Mass Spectrometry ◽  
Chemical Compositions ◽  
Time Out ◽  
Good Potential ◽  
First Time

Essential oil obtained from Maclura triscuspidata fruit has been reported to have functional properties. This study aimed at determining chemical compositions and antioxidant activities of steam-distilled essential oil (SDEO) and glycosidically bound aglycone fraction (GBAF) isolated from fully ripe M. triscuspidata fruit. SDEO was isolated by simultaneous steam distillation and extraction (SDE). GBAF was prepared by Amberlite XAD-2 adsorption of methanol extract, followed by methanol elution and enzymatic hydrolysis. Both fractions were analyzed by gas chromatography–mass spectrometry (GC–MS). A total of 76 constituents were identified from both oils. Apart from fatty acids and their esters, the SDEO contained p-cresol in the highest concentration (383.5 ± 17.7), followed by δ-cadinene (147.7 ± 7.7), β-caryophyllene (145.7 ± 10.5), β-ionone (141.0 ± 4.5), n-nonanal (140.3 ± 20.5), theaspirane A (121.3 ± 4.5) and theaspirane B (99.67 ± 9.05 µg/g). Thirteen carotenoid-derived compounds identified in the SDEO are being isolated from M. triscuspidata fruit for the first time. Out of the 22 components identified in GBAF, 14 were present only in the glycosidically bound volatiles. Antioxidant activity of the GBAF was higher than that of SDEO. These results suggest that glycosidically bound volatiles of M. triscuspidata fruit have a good potential as natural antioxidants.

scholarly journals Utilization of Nutmeg (Myristica fragrans Houtt.) Seed Hydrodistillation Time to Produce Essential Oil Fractions with Varied Compositions and Pharmacological Effects

Molecules ◽  
2020 ◽  
Vol 25 (3) ◽  
pp. 565 ◽  
Author(s):  
Mohamed A. Ibrahim ◽  
Charles L. Cantrell ◽  
Ekaterina A. Jeliazkova ◽  
Tess Astatkie ◽  
Valtcho D. Zheljazkov
Keyword(s):  
Plasmodium Falciparum ◽  
Essential Oil ◽  
Seed Oil ◽  
Antimalarial Activity ◽  
Chemical Compositions ◽  
Pharmacological Effects ◽  
Substantial Variation ◽  
Myristica Fragrans ◽  
Oil Fractions ◽  
Myristica Fragrans Houtt

The intent of this study was to utilize distillation timeframes (DT) of nutmeg (Myristica fragrans) essential oil (EO) to generate fractions with differential chemical compositions and bioactivity. Ten fractions were captured at the following distillation timeframes: 0.0–0.5, 0.5–1.0, 1.0–2.5, 2.5–5.0, 5.0–10, 10–30, 30–60, 60–90, 90–120, and 120–240 min. In addition, a control EO was collected from a straight 0–240 min non-stop distillation. ANOVA and advanced regression modeling revealed that the produced EO fractions possess substantial variation in the concentration of potentially desired compounds. The concentrations (%) of α-phellandrene, 3-carene, p-cymene, limonene, α-thujene, α-pinene, camphene, sabinene, β-pinene, and myrcene decreased, while the concentrations (%) of α-terpinene, γ-terpinene, terpinolene, and myristicin increased in later DT fractions. Nutmeg EO showed some antimalarial activity against Plasmodium falciparum D6, but did not exhibit significant antifungal activity. In general, nutmeg seed oil yields increased with an increase of DT. These results may be utilized by industries using nutmeg EO.

Comparison of Biomaterials from Essential Oils in Five Parts of Magnolia sieboldii

2013 ◽  
Vol 442 ◽  
pp. 142-146 ◽  
Author(s):  
Guang Ren Sun ◽  
Feng Guo Du ◽  
Rui Jian Wang
Keyword(s):  
Essential Oil ◽  
Essential Oils ◽  
Steam Distillation ◽  
Hierarchical Cluster ◽  
Stem Bark ◽  
Chemical Components ◽  
Chemical Compositions ◽  
Root Bark ◽  
Cosmetic Products ◽  
Magnolia Sieboldii

Essential oils were extracted from biomaterials of root bark, stem bark, twigs, leaves and flowers fromMagnolia sieboldiiby the means of steam distillation. Their chemical compositions of these essential oils were analyzed by GC-MS method and their flavor properties were evaluated based on the basic media of cold creams. The results showed that the highest yield of essential oils belonged to the essential oil from root bark and the lowest belonged to that from leaves; As to flavor, the parts of leaves and flower are more suitable for exploiting cosmetic products; Twigs, flowers and leaves belonged to the same cluster by Hierarchical cluster analysis on chemical components from these essential oils. The essential oil from leaves should be further exploited due to its good flavor for cosmetic products and a kind of newable natural resources, although this essential oil had lower extraction yeilds.

scholarly journals Komposisi kimia minyak atsiri daun cengkeh dari proses penyulingan uap

2018 ◽  
Vol 10 (1) ◽  
pp. 37 ◽  
Author(s):  
J Jayanudin
Keyword(s):  
Chemical Composition ◽  
Essential Oil ◽  
Food Industry ◽  
Steam Distillation ◽  
Composition Analysis ◽  
Distillation Process ◽  
Leaf Oil ◽  
Leaf Essential Oil ◽  
Anhydrous Na2so4 ◽  
Chemical Composition Analysis

The chemical composition of clove leaf essential oil obtained from steam distillation process Essential oils are needed in various industries such as industrial perfumes, cosmetics, pharmaceuticals, food industry, and beverages. This study aims to determine the chemical composition of clove leaf essential oil from steam distillation process using GCMS. Dry clove leaves weighing 1.5 kg are included in the kettle flute and sealed properly. Steam from the boiler flows into the kettle with the pressure of 0.5 barG, 1 barG and 1.5 barG for 5, 6 and 7 hours. Mixture oil and water out of the condenser are accommodated and let stand for 24 hours to separate water and oil. Clove leaf oil was purified with 10% bentonite by weight of oil at a temperature of 50oC with stirring for 1 hour. Clove leaf oil that has separated from bentonite added anhydrous Na2SO4 and let stand for 15 minutes and then separate the water and Na2SO4 in oil. Samples with % yield of the largest in its chemical composition analysis using GCMS. Based on the results obtained the largest yield is 1.84% with content of eugenol is 65.03% and 20.94% trans-caryophyllene. Keywords : Clove leaf, Eugenol, Essential Oil, Steam distillationAbstrakMinyak atsiri sangat dibutuhkan dalam berbagai industri seperti industri parfum, kosmetik, farmasi, industri makanan, dan minuman. Penelitian ini bertujuan untuk mengetahui komposisi kimia minyak atsiri daun cengkeh dari proses penyulingan uap menggunakan analisa GCMS. Daun cengkeh kering seberat 1,5 kg yang sudah bersih dari kotoran dimasukkan dalam ketel suling dan ditutup dengan rapat. Steam dari boiler dialirkan ke ketel suling dengan tekanan 0,5 barG, 1 barG dan 1,5 barG selama 5, 6 dan 7 jam. Campuran minyak dan air yang keluar dari kondenser ditampung dan diamkan selama 24 jam untuk memisahkan air dan minyak. Minyak daun cengkeh dimurnikan dengan bentonit 10% dari berat minyak pada suhu 50oC sambil diaduk selama 1 jam. Minyak daun cengkeh yang telah terpisah dari bentonit ditambahkan Na2SO4 anhidrat dan diamkan selama 15 menit kemudian pisahkan air dan Na2SO4 dalam minyak. Sampel dengan % rendemen terbesar di analisa komposisi kimianya menggunakan GCMS. Berdasarkan hasil penelitian didapat rendemen terbesar adalah 1,84% dengan kadar yaitu eugenol 65,03% dan trans-caryophyllene 20.94%.Kata kunci : Daun cengkeh, Eugenol, Minyak atsiri, Penyulingan uap

scholarly journals RENDEMEN DAN KUALITAS MINYAK ATSIRI EUCALYPTUS PELLITA PADA BERBAGAI WAKTU PENYIMPANAN BAHAN BAKU

2018 ◽  
Vol 13 (2) ◽  
pp. 1-9
Author(s):  
Ambar Tri Ratnaningsih ◽  
Enny Insusanty ◽  
Azwin Azwin
Keyword(s):  
Refractive Index ◽  
Essential Oil ◽  
Specific Gravity ◽  
Steam Distillation ◽  
Oil Quality ◽  
Forest Harvesting ◽  
Distillation Process ◽  
Eucalyptus Pellita ◽  
Yield And Quality

 Forest harvesting waste in the form of Ecalyptus pellita leaves can be utilized to be essential oil by distillation process. The research aimed to 1) to know the effect of duration of leaf storage on yield and quality of essential oil produced, 2). Comparing the quality of E.pellita leaves essential oil with eucalyptus oil according to SNI. Methods taken by taking E. pellita leaf waste were then stored for 1,2,3,4,5 and 6 days then steam distillation and measured rendemen, specific gravity, sineol content and refractive index. The average oil yield of E.Pellita is 0.15% with the highest yield of 0.4593% in leaves stored for 3 days. The best essential oil quality comes from leaves that have been stored for 3 days with specific gravity of 0.9186, 60% sineol content, refractive index 1.4603 and 80% alcohol solubility by 1: 1.

scholarly journals Effect of Distillation Tank Density and Storage Time on the Quality and Chemical Composition of Cajuput Oil

2020 ◽  
Vol 10 (1) ◽  
pp. 18-25
Author(s):  
Satrian Nur Alam ◽  
Rini Pujiarti ◽  
Kasmudjo Kasmudjo
Keyword(s):  
Storage Time ◽  
Steam Distillation ◽  
Optical Rotation ◽  
Chemical Components ◽  
Chemical Compositions ◽  
Water Steam ◽  
Oil Storage ◽  
Melaleuca Cajuputi ◽  
Main Components ◽  
And Storage

Cajuput oil is a commodity of non-timber forest product which is needed and potential to be developed in Indonesia. Therefore, further research on the factors of production and post-production are needed to produce optimum quality. In this study, the leaves of cajuput (Melaleuca cajuputi Powell) were distillated by water-steam distillation. This study evaluated effects of distillation tank density (60%, 70%, and 80%) and oil storage time (0 month, 1 month, 2 months, and 3 months) on physicochemical properties and chemical compositions of cajuput oils. The results showed that cajuput oils had a specific gravity of 0.915~0.923; optical rotation of (-2,10°) ~ (-1,20°); refractive index of 1.463~1.464; solubility in alcohol 1 : 1; cineole contents of 61.18~76.24%; clear to yellowish clear color; distinctive smell of cajuput and in accordance with SNI 06-3954- 2006. The GC-MS analysis identified 24 of chemical components on the cajuput oils with main components were 1,8-cineole, α-pinene, and β-caryophylene. Tank density 70% to 80% with the oil storage time up to 3 months still gives the optimum quality and chemical compositions.

scholarly journals The Effect of Temperature on the Essential Oil Components of Salvia potentillifolia Obtained by Various Methods

2009 ◽  
Vol 4 (7) ◽  
pp. 1934578X0900400 ◽  
Author(s):  
Mehmet Öztürk ◽  
Gülsen Tel ◽  
Mehmet Emin Duru ◽  
Mansur Harmandar ◽  
Gülaçtı Topçu
Keyword(s):  
High Temperature ◽  
Essential Oil ◽  
Essential Oils ◽  
Volatile Compounds ◽  
Steam Distillation ◽  
Extraction Methods ◽  
Effect Of Temperature ◽  
Chemical Compositions ◽  
Percentage Concentration ◽  
Oil Components

The chemical compositions of the essential oils of Salvia potentillifolia (Lamiaceae) were analyzed by GC and GCMS. The oils were obtained by four different methods (hydrodistillation, steam distillation, and two extraction methods) to investigate the effect of temperature on the volatile compounds. In total, 121 components were detected in the various oils. The major compounds characterized were α-pinene (30.2, 31.2, 10.6, and 14.8 %) and β-pinene (15.0, 14.6, 7.6, and 11.4%), respectively. Surprisingly, the percentage concentrations of α-pinene and β-pinene in the hydrodistilled and steam distilled oils were high, even though prepared at high temperature, whereas the contents of both compounds were lower in the essential oils obtained by the extraction methods prepared without added heat. The percentage concentration of 8,13-epoxy-labda-14-en-2-one, a diterpenoid, in the extracted essential oil was 22 times higher than in the hydrodistilled and steam distilled essential oils. However, the concentrations of cis-p-menth-2-en-1-ol was four times, and β-bourbonene and β-caryophyllene two times superior than their percentage concentrations in the hydrodistilled and steam distilled essential oils.

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