DC magnetization of titania supported on reduced graphene oxide flakes

DC magnetization of a series of titania nanocomposites modified with reduced graphene oxide (rGO) has been investigated. Hysteresis loops observed at room temperature disappeared at low temperatures. At a temperature of about 100 K, a phase transition to the superferromagnetic order state was observed, probably due to the linear expansion and self-reorientation of the magnetic moments. Processes associated with magnetic moment reorientation can cause a hysteresis loop to disappear at low temperatures as well as superferromagnetic ordering. It was suggested that the isolated nanoparticle in the nanopore could be used to create a “compass” at a nanometer-sized level that would be many times more sensitive than the conventional one. Measurements of the zero-field cooling and field cooling modes do not exclude the possibility of the coexistence of a superparamagnetic state.

Magnetic Barkhausen Noise Testing for Subsurface Discontinuities under DC Magnetization

Subsurface discontinuities are inevitably formed during the long-term operations of pipelines, oil tanks, ship hulls, and the like. However, it is still a big challenge to detect deeply buried subsurface discontinuities using existing nondestructive testing methods. In this paper, based on the high sensitivity of magnetic Barkhausen noise (MBN) to the movement of the domain walls, an MBN test under direct current (DC) magnetization is proposed for subsurface discontinuity detection. Under DC magnetization, subsurface discontinuities will distort the magnetic field distribution in the near-surface layer of the specimen and then affect the movement of the domain walls in this region. Meanwhile, through alternating current (AC) excitation, MBN testing is conducted to detect the movement of the domain walls to evaluate subsurface discontinuities. To validate the proposed technique, MBN experiments under DC magnetization are conducted to quantify subsurface discontinuities with different buried depths. Experimental results indicate that the proposed technique can detect subsurface discontinuities with buried depths of up to 5 mm, and the extracted MBN energy feature has an approximately linear relationship with the buried depth.

Anomalous magnetic properties in LaFe11.5Al1.5

We report the magnetic relaxation, DC magnetization, heat capacity, and X-ray powder diffraction studies of a melt-spun LaFe11.5Al1.5 compound executed across a temperature range of 5 to 300 K.