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Kinetics of Grape Seed Oil Epoxidation in Supercritical CO2

The epoxidation of grape seed oil in supercritical CO2, to the best of our knowledge, has been only superficially described in the literature, apart from a short communication and our own previous published work on the topic. In this work, a thorough study of the performance of the supercritical epoxidation of grape seed oil is performed in a wide range of conditions, and the kinetic parameters of the supercritical epoxidation of vegetable oils are reported for the first time in the literature. The experimental work has covered a 40–60 °C temperature range at 150 bar, sampling during a period of 48 h. The nature and extent of the side reactions and secondary products obtained have been evaluated, being hydrolysis products and their oligomerization derivatives the major by-products. Reaction rate constants (10−2 h−1 order) and activation energy parameters were finally calculated from the experimental conversion and epoxy yield data to establish the effect of temperature on the kinetics of the process.

Fatty Acids and Triacylglycerols Profiles from Sicilian (Cold Pressed vs. Soxhlet) Grape Seed Oils

Among the Sicilian economic productive sectors, that of wine production has today a considerable economic value. However, with the growth of this sector, notable was the increase in the production of waste, which to date is not only an economic damage for companies, but also a threat to the environment. It is known that waste from wine production has properties (e.g., antioxidants) which have potential reuse at cosmetic, pharmaceutical and nutritional levels to obtain economically sustainable applications. A new goal is given by the recovery of added value compounds from agri-food wastes and by-products. Grape seed oil is a promising vegetable fat and cold pressing does not involve the use of chemicals, which are harmful to health. It implies that cold-pressed seed oils may contain phytochemicals, as well as natural antioxidants, more than refined oils. In this context, this works aims at studying the chemical characterization (triglycerides profile and composition in fatty acids) of grape seed oils obtained from Soxhlet and cold pressed extraction from Sicilian red grape seeds and white grape seeds. The possibility of obtaining high yields of triglycerides and fatty acids from the waste of wine production through new extraction methods would open up new perspectives for the reuse of waste in a human and animal food context. The results of this work allow the opening up of new perspectives to reuse and then reduce these wastes, helping not only to reduce the damage to the environment and costs for companies but also to create a new product that is environmentally sustainable and with an important economic value.

A Study on Performance Evaluation of Biodiesel from Grape Seed Oil and Its Blends for Diesel Vehicles

With incessant increases in fuel prices worldwide and concerns for environmental pollution, the need for alternative sources of energy is becoming urgent. In this study, the potential of grape seed oil for biodiesel as an alternative fuel was evaluated. Refined grape seed oil was bought in liquid form and then subjected to an alkali-catalyzed transesterification process for biodiesel production. The physicochemical properties of the resulting biodiesel—namely, viscosity, cetane number, and heating value—were investigated. The biodiesel was blended with a conventional diesel in various proportions and combusted in a four-cylinder, four-stroke compression ignition (diesel) engine under two loading conditions. Experimental results revealed that the blend ratio of B70 (70% GS biodiesel and 30% conventional diesel) gave the best overall engine performance in terms of maximum power, minimum emissions, and fuel consumption. Furthermore, a novel neural network technique called extreme learning machine was adopted to investigate the optimal blend ratio using the dataset obtained from the experimental results. The results also indicate that the best choice of biodiesel blend ratio is approximately B73.67 (73.67% GS biodiesel and 26.33% conventional diesel). The study shows that grape seed oil could serve as a reliable source of production of quality biodiesel fuels, which could be used as an alternative to conventional diesel fuels.