One-Step MIBK Synthesis: A New Process from 2-Propanol

2002 ◽  
Vol 208 (1) ◽  
pp. 114-123 ◽  
Author(s):  
J.I. Di Cosimo ◽  
G. Torres ◽  
C.R. Apesteguı́a
Keyword(s):  
Author(s):  
R. Irawan

Leap frog concept was created to address the loss of single joint rig agility and drive the cycle time average lower than ever. The idea is to move the preparation step into a background activity that includes moving the equipment, killing the well, dismantling the wellhead and installing the well control equipment/BOP before the rig came in. To realize the idea, a second set of equipment is provided along with the manpower. By moving the preparation step, the goal is to eliminate a 50% portion of the job from the critical path. The practice is currently performed in tubing pump wells on land operations. However, the work concept could be implemented for other type of wells, especially ESP wells. After implementation, the cycle time average went down from 18 hours to 11 hours per job, or down by ~40%. The toolpusher also reports more focused operations due to reduced scope and less crew to work with, making the leap frog operation safer and more reliable. Splitting the routine services into 2 parts not only shortened the process but it also reduces noise that usually appear in the preparation process. The team are rarely seen waiting on moving support problems that were usually seen in the conventional process. Having the new process implemented, the team had successfully not only lowered cycle time, but also eliminated several problems in one step. Other benefits from leap frog implementation is adding rig count virtually to the actual physical rig available on location, and also adding rig capacity and completing more jobs compared to the conventional rig. In other parts, leap frog faced some limitation and challenges, such as: limited equipment capability for leap frog remote team to work on stuck plunger, thus hindering its leap frog capability, and working in un-restricted/un-clustered area which disturb the moving process and operation safety.


2002 ◽  
Vol 17 (3) ◽  
pp. 542-549 ◽  
Author(s):  
Christophe Gras ◽  
Frédéric Bernard ◽  
Frédéric Charlot ◽  
Eric Gaffet ◽  
Zuhair A. Munir

A new process combining electric field activation and the imposition of pressure from mechanically activated powder mixtures is demonstrated as a means to simultaneously synthesize and densify nano-MoSi2 in one step. Nanophase reactants (Mo + 2Si) produced by mechanical activation are reacted by field activation with the simultaneous application of a uniaxial pressure. Mo + 2Si powders were comilled in a specially designed planetary mill to obtain nanometric reactants but to avoid formation of any product phases. These were then subjected to high alternating currents (1600 A) and pressures of 106 MPa. Under these conditions, a reaction is initiated and completed within a short period of time (3–6 min). The relative density of the product ranged from 82 to 93%. The crystallite size of the MoSi2 compound was determined by x-ray diffraction line-broadening analysis using the Langford method. The size ranged from 58 to 75 nm.


2020 ◽  
Vol 40 (3) ◽  
pp. 256-266
Author(s):  
Tim Deringer ◽  
Dietmar Drummer

AbstractA new process, called thermoset in-mold forming, for combining thermoset master forming and thermoset forming in one mold is in development. A pre-impregnated continuous-fiber reinforced sheet based on epoxy (prepreg) is formed in the injection molding machine, followed by instantaneous overmolding of a short-fiber reinforced epoxy compound in one step. Compared with conventional processes in which thermoset injection molding, prepreg compression molding, and hence curing of the materials are separated, the new process allows for the combination in one step and simultaneous curing of both components. The result is a hybrid component, which features a continuous-fiber reinforced part for higher mechanical performance and a short-fiber reinforced part with high design freedom for integration of additional functions. For a successful combination of both materials in one process, it is essential to investigate the bond strength between them in relation to the processing parameters and their influence on the degree of cure. This paper analyzes the influence of the mold temperature in this process on curing degree, bond strength, and the processing viscosity.


2021 ◽  
Vol 36 (5) ◽  
pp. 608-619
Author(s):  
F. Jakob ◽  
J. Pollmeier ◽  
H.-P. Heim

Abstract A new process to produce back-injected self-reinforced composites (SRCs) is presented. In contrast to other investigations on back-injection of SRCs, a process is presented which allows compacting and back injection of SRCs in one step where the SRCs are partly consolidated only via melt pressure inside the cavity. The mechanical properties of SRCs depend to a large extent on the process parameters of temperature and pressure during manufacture. These parameters are not yet known for back-injected areas. Sensors inside of the cavity measure the influences on the temperature and pressure conditions in the cavity. Initial studies on adhesion were carried out and analysed. For this purpose, shear tests of the back-injected component were carried out and a maximum shear strength of 5.81 MPa was determined for the materials used here. The investigations also show a dependence on the Distance from the Gate (DG) and the Mass temperature (TM). First microscopic examinations show good bonding between the SRC and the injection molded part, with no voids or air pockets in the boundary layer. It can also be seen that successful consolidation takes place in the area of the back injection.


2005 ◽  
Vol 488-489 ◽  
pp. 377-380 ◽  
Author(s):  
Xiao Peng Cui ◽  
Yong Bing Liu ◽  
Zhan Yi Cao ◽  
Xiao Hong Yang ◽  
Wei Liang

Thixomolding® is a new process of net shape parts for magnesium alloys in one step, and it is suited to manufacture the thin wall products, especially to the electronic component shells. In this paper, the sample of mobile phone housing is fabricated by 220Tons Thixomolding® machine made by Japan Steel Works. The effects of barrel temperature, screw rotate rate and mold temperature on microstructure were studied. The relationship between process parameters and microstructure was also discussed in this paper.


Author(s):  
R.P. Goehner ◽  
W.T. Hatfield ◽  
Prakash Rao

Computer programs are now available in various laboratories for the indexing and simulation of transmission electron diffraction patterns. Although these programs address themselves to the solution of various aspects of the indexing and simulation process, the ultimate goal is to perform real time diffraction pattern analysis directly off of the imaging screen of the transmission electron microscope. The program to be described in this paper represents one step prior to real time analysis. It involves the combination of two programs, described in an earlier paper(l), into a single program for use on an interactive basis with a minicomputer. In our case, the minicomputer is an INTERDATA 70 equipped with a Tektronix 4010-1 graphical display terminal and hard copy unit.A simplified flow diagram of the combined program, written in Fortran IV, is shown in Figure 1. It consists of two programs INDEX and TEDP which index and simulate electron diffraction patterns respectively. The user has the option of choosing either the indexing or simulating aspects of the combined program.


2006 ◽  
Vol 73 ◽  
pp. 85-96 ◽  
Author(s):  
Richard J. Reece ◽  
Laila Beynon ◽  
Stacey Holden ◽  
Amanda D. Hughes ◽  
Karine Rébora ◽  
...  

The recognition of changes in environmental conditions, and the ability to adapt to these changes, is essential for the viability of cells. There are numerous well characterized systems by which the presence or absence of an individual metabolite may be recognized by a cell. However, the recognition of a metabolite is just one step in a process that often results in changes in the expression of whole sets of genes required to respond to that metabolite. In higher eukaryotes, the signalling pathway between metabolite recognition and transcriptional control can be complex. Recent evidence from the relatively simple eukaryote yeast suggests that complex signalling pathways may be circumvented through the direct interaction between individual metabolites and regulators of RNA polymerase II-mediated transcription. Biochemical and structural analyses are beginning to unravel these elegant genetic control elements.


2010 ◽  
Vol 43 (18) ◽  
pp. 16
Author(s):  
MATTHEW R.G. TAYLOR
Keyword(s):  

2007 ◽  
Vol 0 (0) ◽  
pp. 0-0
Author(s):  
C.W. Kim ◽  
Y.H. Kim ◽  
H.G. Cha ◽  
D.K. Lee ◽  
Y.S. Kang

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