Increasing the Information Capacity of Materials Non-destructive Electrical Measurements

2021 ◽  
pp. 657-666
Author(s):  
Nikolay Pshchelko ◽  
Olga Tsareva ◽  
Vera Breskich
Author(s):  
Terence Kane

Abstract A 300mm wafer atomic force prober (AFP) has been installed into IBM’s manufacturing line to enable rapid, nondestructive electrical identification of defects. Prior to this tool many of these defects could not detected until weeks or months later. Moving failure analysis to the FAB provides a means of complementing existing FAB inspection and defect review tools as well as providing independent, non-destructive electrical measurements at an early point in the manufacturing cycle [1] Once the wafer sites are non destructively AFP characterized, the wafer is returned to its front opening unified pod (FOUP) carrier and may be reintroduced into the manufacturing line without disruption for further inspection or processing. Whole wafer atomic force probe electrical characterization has been applied to 32nm, 28nm, 20nm and 14nm node technologies. In this paper we explore the cost benefits of performing non-destructive AFP measurements on whole wafers. We have found the methodology of employing a whole wafer AFP tool complements existing in-line manufacturing monitoring tools such as brightfield/dark field optical inspection, SEM in-line inspection and in-line E-beam voltage contrast inspection (EBI).


1983 ◽  
Vol 25 ◽  
Author(s):  
M.H. Hecht ◽  
F.J. Grunthaner ◽  
J. Maserjian

ABSTRACTWe report on the first non-destructive measurement of the chemical and physical characteristics of the interface between bulk SiO2 and thick aluminum films. Both X-Ray Photoelectron Spictroscopy (XPS) and electrical measurements of unannealed, resistively evaporated Al films on thermal SiO2 indicate an atomically abrupt interface. Post metallization annealing (PMA) at 450°C induces reduction of the SiO2 by the aluminum, resulting in the layer ordering SiO2/Al2O3/Si/Al. The XPS measurement is performed from the SiO2 side after the removal of the Si substrate after etching with XeF2 gas and thinning of the SiO2 layer with HF:ETOH. This represents a powerful new approach to the study of metal-insulator and other interfaces.


2012 ◽  
Vol 26 (3) ◽  
pp. 243-247 ◽  
Author(s):  
I. Cseresnyés ◽  
G. Fekete ◽  
K. Végh ◽  
A. Székács ◽  
M. Mörtl ◽  
...  

Monitoring of herbicide effect in maize based on electrical measurements The effect of the herbicide acetochlor on root growth was studied by a non-destructive electrical impedance and capacitance method in pot experiments on maize. Acetochlor was applied both as single active ingredient and mixed with safener AD-67 in two dosages. Without safener addition, acetochlor had a permanent inhibiting effect on plant root expansion. The safener AD-67 was capable of providing protective effect against herbicide application. High correlations between root electrical impedance or capacitance and the root dry mass or surface area under our laboratory conditions were confirmed by plant harvest method. Root electrical impedance and capacitance measurements proved to be valid for monitoring the effect of the herbicide influencing root development and for distinguishing plant groups subjected to different stress conditions.


Author(s):  
Wesley Nascimento

This work presents mathematical models obtained from electrical measurements to control of milk quality and detection of adulterations, especially by ethanol, sodium chloride and sodium bicarbonate. These substances may cause changes in the electrical properties of raw milk. Electrical measurements are non-destructive and fast techniques. The proposed models correlate the addition of the mentioned substances with measurements of conductance and phase angle at a fixed frequency of 100 Hz. Linear models were proposed from the data and the independence, normality, lack of adjustment and homoscedasticity were verified. The detection limits obtained based on conductance were 0.01 %, 0.03 g/L and 2.1 g/L for samples adulterated with ethanol, sodium chloride and sodium bicarbonate, respectively. The limits for measurements based on the phase angle were 0.4%, 1.3 g/L and 16.4 g/L, respectively. The results demonstrated that the proposed models may be a powerful tool to improve milk analysis methodologies.


Energies ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 650 ◽  
Author(s):  
Simone Vincenzo Suraci ◽  
Davide Fabiani ◽  
Laura Mazzocchetti ◽  
Loris Giorgini

The usability of any material hinges upon its stability over time. One of the major concerns, focusing on polymeric materials, is the degradation they face during their service life. The degradation mechanisms are deeply influenced by the aging temperature to which the material is subjected. In this paper, low-density polyethylene (LDPE) flat specimens were thermally aged under two different temperatures (90 °C and 110 °C) and analyzed. Specimens were characterized through both the most common mechanical and chemical measurements techniques (e.g., tensile stress, thermal analyses, oxidation induction time) and electrical measurements (dielectric spectroscopy, in particular), which are examples of non-destructive techniques. As a result, a very spread characterization of the polyethylene-based materials was obtained and a very good correlation was found to exist between these different techniques, highlighting the possibility of following the aging degradation development of polymers through electrical non-destructive techniques.


1999 ◽  
Vol 591 ◽  
Author(s):  
Rosario A. Gerhardt

ABSTRACTThis paper gives a short summary of the background, theory and methodology needed to utilize electrical measurements as a non-destructive method for microstructural characterization. Examples are given for all classes of materials. Details are given for how to detect: (1) pore volume in thermal barrier coatings, (2) formation of surface layers due to moisture adsorption in a wide variety of materials, (3) orientation of fibers and whiskers in ceramic matrix and polymer matrix composites, (4) crack detection in metals and (5 ) stacking faults in semiconductors. Many other examples are mentioned. It needs to be emphasized that electrical measurements alone are not sufficient to identify the microstructural features of interest but must always be accompanied by complementary techniques. Proper data collection and data interpretation of properties of a specific set of materials can lead to in-line process monitoring, quality control monitoring, mechanical damage monitoring and environmental degradation monitoring of those materials.


2022 ◽  
Vol 12 (1) ◽  
Author(s):  
James C. Gallagher ◽  
Mona A. Ebrish ◽  
Matthew A. Porter ◽  
Alan G. Jacobs ◽  
Brendan P. Gunning ◽  
...  

AbstractTo improve the manufacturing of vertical GaN devices for power electronics applications, the effects of defects in GaN substrates need to be better understood. Many non-destructive techniques including photoluminescence, Raman spectroscopy and optical profilometry, can be used to detect defects in the substrate and epitaxial layers. Raman spectroscopy was used to identify points of high crystal stress and non-uniform conductivity in a substrate, while optical profilometry was used to identify bumps and pits in a substrate which could cause catastrophic device failures. The effect of the defects was studied using vertical P-i-N diodes with a single zone junction termination extention (JTE) edge termination and isolation, which were formed via nitrogen implantation. Diodes were fabricated on and off of sample abnormalities to study their effects. From electrical measurements, it was discovered that the devices could consistently block voltages over 1000 V (near the theoretical value of the epitaxial layer design), and the forward bias behavior could consistently produce on-resistance below 2 mΩ cm2, which is an excellent value considering DC biasing was used and no substrate thinning was performed. It was found that high crystal stress increased the probability of device failure from 6 to 20%, while an inhomogeneous carrier concentration had little effect on reverse bias behavior, and slightly (~ 3%) increased the on-resistance (Ron). Optical profilometry was able to detect regions of high surface roughness, bumps, and pits; in which, the majority of the defects detected were benign. However a large bump in the termination region of the JTE or a deep pit can induce a low voltage catastrophic failure, and increased crystal stress detected by the Raman correlated to the optical profilometry with associated surface topography.


Author(s):  
J W Steeds

There is a wide range of experimental results related to dislocations in diamond, group IV, II-VI, III-V semiconducting compounds, but few of these come from isolated, well-characterized individual dislocations. We are here concerned with only those results obtained in a transmission electron microscope so that the dislocations responsible were individually imaged. The luminescence properties of the dislocations were studied by cathodoluminescence performed at low temperatures (~30K) achieved by liquid helium cooling. Both spectra and monochromatic cathodoluminescence images have been obtained, in some cases as a function of temperature.There are two aspects of this work. One is mainly of technological significance. By understanding the luminescence properties of dislocations in epitaxial structures, future non-destructive evaluation will be enhanced. The second aim is to arrive at a good detailed understanding of the basic physics associated with carrier recombination near dislocations as revealed by local luminescence properties.


Author(s):  
R.F. Sognnaes

Sufficient experience has been gained during the past five years to suggest an extended application of microreplication and scanning electron microscopy to problems of forensic science. The author's research was originally initiated with a view to develop a non-destructive method for identification of materials that went into objects of art, notably ivory and ivories. This was followed by a very specific application to the identification and duplication of the kinds of materials from animal teeth and tusks which two centuries ago went into the fabrication of the ivory dentures of George Washington. Subsequently it became apparent that a similar method of microreplication and SEM examination offered promise for a whole series of problems pertinent to art, technology and science. Furthermore, what began primarily as an application to solid substances has turned out to be similarly applicable to soft tissue surfaces such as mucous membranes and skin, even in cases of acute, chronic and precancerous epithelial surface changes, and to post-mortem identification of specific structures pertinent to forensic science.


Author(s):  
D. C. Joy ◽  
R. D. Bunn

The information available from an SEM image is limited both by the inherent signal to noise ratio that characterizes the image and as a result of the transformations that it may undergo as it is passed through the amplifying circuits of the instrument. In applications such as Critical Dimension Metrology it is necessary to be able to quantify these limitations in order to be able to assess the likely precision of any measurement made with the microscope.The information capacity of an SEM signal, defined as the minimum number of bits needed to encode the output signal, depends on the signal to noise ratio of the image - which in turn depends on the probe size and source brightness and acquisition time per pixel - and on the efficiency of the specimen in producing the signal that is being observed. A detailed analysis of the secondary electron case shows that the information capacity C (bits/pixel) of the SEM signal channel could be written as :


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