scholarly journals A multilevel investigation supported by multivariate analysis for tomato product formulation

Author(s):  
Fatma Boukid ◽  
Elena Curti ◽  
Agoura Diantom ◽  
Eleonora Carini ◽  
Elena Vittadini

AbstractIndustrial processing of tomato includes its cutting and mincing, thermal treatments, and the addition of ingredients, which might induce changes in physicochemical properties of the final products. In this frame, the impact of texturing/thickening [xanthan gum (X) or potato fiber (F)] on the macroscopic, mesoscopic and molecular properties of tomato double concentrate (TDC) was investigated to determine if F can efficiently substitute X, in association with small solutes (sugar and salt) and thermal treatment (cold and hot). At a macroscopic level, multivariate statistics (MANOVA) underlined that color change (ΔE) was increased by X and F addition contrary to heating and the addition of salt and sugar. MANOVA revealed that texture was greatly enhanced through the use of F over X. 1H NMR molecular mobility changes were more controlled by texturing agents (F and X) than thermal treatment and small solutes. Particularly F increased the more rigid population indicating stronger interaction with water molecules resulting in shear-thinning flow. However, adding X contributed into the increase of the dynamic and mobile populations. Therefore, F can be a valid “clean label” substitute of X in modulating tomato products properties.

Clay Minerals ◽  
1980 ◽  
Vol 15 (4) ◽  
pp. 421-428 ◽  
Author(s):  
T. Mozas ◽  
S. Bruque ◽  
A. Rodriguez

AbstractHydration/dehydration behaviour and the effect of various thermal treatments on montmorillonites saturated with lanthanide ions have been investigated by X-ray diffraction, thermal analysis (DTA, TG, DTG), IR spectroscopy and sorption-desorption of water vapour techniques. Heating at 150°C under 10−5 torr did not eliminate all the interlayer water of the montmorillonite, neither did it affect the CEC. Heating above 160°C caused a reduction in CEC. At 25°C La-montmorillonite takes up a maximum of three water layers in the interlayer space, the water molecules adopting a nonacoordinated distribution around the La3+ cation.


2020 ◽  
pp. 41-53
Author(s):  
Jahid Hasan Shourove ◽  
Wahidu Zzaman ◽  
Razia Sultana Chowdhury ◽  
Md. Mozammel Hoque

Industrial processing of the fruit juice is responsible for the changes in some quality attributes. Thermal treatment is a most applicable operation for any processing and it affects the physicochemical and antioxidant properties of the juice. This study was conducted to observe the changes in some physical properties and the bioactive compounds of star fruit (Averrhoa carambola L.) juice during thermal treatment at 70°C, 80°C and 90°C for 10, 20, 30 and 40 min by a temperature-controlled water bath. During thermal treatment of the juice pH and browning index increased significantly (P≤ 0.05) with time and increasing temperature whereas the Cloud index of the juice decreased. No significant variation (P≥ 0.05) noticed in the case of total soluble solids. Color differences gradually increased in case of color parameter (0 to 7.83 ± 0.20) and negatively increased in case of (0 to -7.33± 1.00). Irregular results observed for  and maximum difference (3.01±0.08) noticed at 90°C for 40 min. The highest overall color change (∆E= 11.04±0.76) observed when the juice treated at 90°C for 40 min. In consideration of the bioactive compounds, maximum ascorbic acid estimated (24.17±0.70mg/100ml) in fresh juice and with rising temperature and time it decreased. β-carotene also decreased significantly during heat treatment. The Total Polyphenol Content (TPC) found in fresh juice as (540.08±16.64 mg GAE/100 ml) and it was not changed in a regular manner with temperature change. Flavonoid content increased significantly (P≤0.05) when the juice was heat-treated at 70°C and 80°C while no significant change observed at 90°C. Maximum DPPH scavenging activity found in fresh juice (60.19±1.39%) and decreased to (53.83±1.43%) when 90°C temperature was applied for 40 min. This study may help to find out the nutritional value of locally available star fruit and physicochemical changes of this fruit juice during thermal processing.


2017 ◽  
Vol 68 (1) ◽  
pp. 175-179
Author(s):  
Oana Roxana Chivu ◽  
Augustin Semenescu ◽  
Claudiu Babis ◽  
Catalin Amza ◽  
Gabriel Iacobescu ◽  
...  

Rainfall is a major component of the environment and the main source of the air purification becouse of many pollutants increases who have the most varied sources: various human activities including industry and agriculture, and some household duties. Air purification by means of precipitation is achieved by numerous highly complex mechanisms. The final products of degradation of the pollutant in the air, which are generally harmless, can be reacted with each other in the presence of water, giving rise to the final compounds with a high toxicity. Thus, exhaust, mobile sources of noxious almost identical to those specific activities in the industrial processing of oil, contain lead which is the ideal catalyst for converting SO2 to sulfuric acid in the presence of rainwater, with all the disadvantages that they create. This paper will present an experimental research oabout how rainfall water quality is influenced by the activity of the industrial processing of oil, in a chemical plant in Constanta County.


Nanomaterials ◽  
2019 ◽  
Vol 9 (1) ◽  
pp. 64 ◽  
Author(s):  
Qin Wang ◽  
Hui Xie ◽  
Zhiming Hu ◽  
Chao Liu

In this study, molecular dynamics simulations were carried out to study the coupling effect of electric field strength and surface wettability on the condensation process of water vapor. Our results show that an electric field can rotate water molecules upward and restrict condensation. Formed clusters are stretched to become columns above the threshold strength of the field, causing the condensation rate to drop quickly. The enhancement of surface attraction force boosts the rearrangement of water molecules adjacent to the surface and exaggerates the threshold value for shape transformation. In addition, the contact area between clusters and the surface increases with increasing amounts of surface attraction force, which raises the condensation efficiency. Thus, the condensation rate of water vapor on a surface under an electric field is determined by competition between intermolecular forces from the electric field and the surface.


Pharmaceutics ◽  
2021 ◽  
Vol 13 (7) ◽  
pp. 996
Author(s):  
Niels Lasse Martin ◽  
Ann Kathrin Schomberg ◽  
Jan Henrik Finke ◽  
Tim Gyung-min Abraham ◽  
Arno Kwade ◽  
...  

In pharmaceutical manufacturing, the utmost aim is reliably producing high quality products. Simulation approaches allow virtual experiments of processes in the planning phase and the implementation of digital twins in operation. The industrial processing of active pharmaceutical ingredients (APIs) into tablets requires the combination of discrete and continuous sub-processes with complex interdependencies regarding the material structures and characteristics. The API and excipients are mixed, granulated if required, and subsequently tableted. Thereby, the structure as well as the properties of the intermediate and final product are influenced by the raw materials, the parametrized processes and environmental conditions, which are subject to certain fluctuations. In this study, for the first time, an agent-based simulation model is presented, which enables the prediction, tracking, and tracing of resulting structures and properties of the intermediates of an industrial tableting process. Therefore, the methodology for the identification and development of product and process agents in an agent-based simulation is shown. Implemented physical models describe the impact of process parameters on material structures. The tablet production with a pilot scale rotary press is experimentally characterized to provide calibration and validation data. Finally, the simulation results, predicting the final structures, are compared to the experimental data.


Geosciences ◽  
2021 ◽  
Vol 11 (4) ◽  
pp. 167
Author(s):  
Unai Cortada ◽  
María Carmen Hidalgo ◽  
Julián Martínez ◽  
María José de la Torre

The abandoned mining district of Linares (South Spain) is marked with waste from the mining and the processing of metal ores that pose an environmental hazard to watercourses. A combined analysis of waste, sediments and water was carried out to analyse the impact of a smelter on Baños Creek. The composition of the facility waste was determined using X-ray diffractometry and scanning electron microscopy. The total contents of the metal(loid)s in the waters and sediments of the watercourse were analysed, and sequential metal(loid) extraction of solid samples was carried out. The facility wastes consisted mainly of secondary minerals, such as natropharmacosiderite and spertiniite, as well as rare metal salts, such as mopungite and NaPb2(CO3)2(OH). The leachates generated by these wastes were highly alkaline, with a pH of 10 and a total dissolved solids concentration of approximately 9 g L−1. This Na-bicarbonate-type water had an As concentration above 200 mg L−1 and elevated levels of Pb, Sb and Zn (5029 µg L−1, 841 µg L−1 and 525 µg L−1, respectively). This highly contaminated lixiviate had a significant effect on the chemical quality of the waters and the bioavailability of metal(loid)s in the creek sediments, especially in the headwaters. In this zone, the As, Pb, Sb and Zn concentrations in the most mobile fraction of the sediments reached 1035 mg kg−1, 261 mg kg−1, 45 mg kg−1 and 30 mg kg−1, respectively. By comparison, smelter slag and mining waste have a much lower impact on the waters and the mobile fraction of the sediments, while significantly increasing the total concentration of these potentially toxic elements in creek sediments.


2020 ◽  
Vol 20 (5) ◽  
pp. 2840-2846
Author(s):  
Hyorim Kim ◽  
Ramalingam Manivannan ◽  
Young-A Son

A new chromone moiety fused with phenyl hydrazine carboxamide as a binding site for metal ion was designed and synthesized as a colorimetric/fluorimetric probe for selective sensing of Al3+ ion. The absorption and fluorescence spectral results showed selective and sensitive recognition of Al3+ with no significant interference from other competitive metal ions. The addition of Al3+ to R brought a prompt color change from colorless to yellow and the turn-on fluorescence response with Al3+ among different cations was studied. The visible color change and turn-on fluorescence Al3+ ion with R was attributed to the intra molecular charge transfer transition. The plausible binding nature of the receptor with Al3+ has also been anticipated by the results of 1H NMR and mass spectral analysis. For the practical effectiveness, test strip prepared using probe R was successfully applied to monitor the presence of Al3+ ion in aqueous medium.


Author(s):  
Андрей Киричек ◽  
Andrey Kirichek ◽  
Дмитрий Соловьев ◽  
Dmitriy Solovyev ◽  
Александр Хандожко ◽  
...  

The problems of analyzing metallographic images and the method of their solution using modern software for the analysis of metallographic images are described. There is given an analysis of microstructure images as the main indicator of the surface layer quality by the example of studying the research results of strain wave hardening combinations and chemical-thermal treatment, in particular the influence of previous strain wave hardening and subsequent thermal and chemical- thermal treatment on the alloy steel microstructure or previous thermal and chemical- thermal treatment and subsequent strain wave hardening. On the basis of the analysis the effectiveness of strain wave hardening and chemical and thermal treatment is established.


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