Complete and Incomplete Wetting of Ferrite Grain Boundaries by Austenite in the Low-Alloyed Ferritic Steel

2012 ◽  
Vol 21 (5) ◽  
pp. 667-670 ◽  
Author(s):  
B. B. Straumal ◽  
Y. O. Kucheev ◽  
L. I. Efron ◽  
A. L. Petelin ◽  
J. Dutta Majumdar ◽  
...  
Keyword(s):  
Grain Boundaries ◽  
Ferritic Steel ◽  
Incomplete Wetting

The Effect of Nano-precipitates on Strength in a Micro-alloyed Ferritic Steel

2011 ◽  
Vol 1296 ◽  
Author(s):  
H.A. Askari ◽  
Y.F. Shen ◽  
C.M. Wang ◽  
X. Sun ◽  
H.M. Zbib
Keyword(s):  
Shear Stress ◽  
Grain Boundaries ◽  
Ferritic Steel ◽  
Mechanistic Model ◽  
Particle Interaction ◽  
High Strength ◽  
Average Diameter ◽  
Ferrite Matrix ◽  
Dislocation Dynamics ◽  
Rolled Sheet

ABSTRACTA high strength ferritic steel with finely dispersive precipitates was investigated to reveal the fundamental strengthening mechanisms in this alloy. Using energy dispersive X-ray spectroscopy (EDXS) and transmission electron microscope (TEM), fine carbides with an average diameter of 10 nm were observed in the ferrite matrix of the 0.08%Ti steel, and some cubic M23C6 precipitates were also observed at the grain boundaries and the interior of grains. The dual precipitate structure of finely dispersive TiC precipitates in the matrix and coarse M23C6 at grain boundaries provides combined matrix and grain boundary strengthening. The resulting yield stress is two or three times higher than that of conventional Ti-bearing high strength hot-rolled sheet steels. The effect of the particle size, particle distribution and intrinsic particle strength have been investigated through dislocation dynamics (DD) simulations and the relationship for resolved shear stress for single crystal under this condition has been presented using simulation data. The results show that the finely dispersive precipitates can strengthen the material by pinning the dislocations up to a certain shear stress and retarding the recovery as well as annihilation of dislocations. The DD results also show that strengthening is not only a function of the density of the nano-scale precipitates but also of their size. This size effect is explained using a mechanistic model developed based on dislocation-particle interaction.

Development of High Chromium Steel for SFR in Japan and Creep-Fatigue Assessment of the Welded Joint

2008 ◽  
Author(s):  
Takashi Wakai ◽  
Nobuhiro Isobe ◽  
Shingo Date ◽  
Tai Asayama ◽  
Shigenobu Kubo
Keyword(s):  
Fatigue Strength ◽  
Grain Boundaries ◽  
Welded Joints ◽  
Ferritic Steel ◽  
Welded Joint ◽  
Assessment Procedure ◽  
Test Results ◽  
Strength Assessment ◽  
High Chromium ◽  
Creep Fatigue

This paper describes the provisional material specifications of the high chromium (Cr) ferritic steel for the Sodium cooled Fast Reactor (SFR) and development of creep-fatigue assessment procedure for the welded joint made of the steel. Based on the test results, it was revealed that tungsten (W) should be diminished to achieve better creep-fatigue strength and toughness after long term aging at elevated temperature. Metallurgical examinations using a scanning electron microscope showed that W precipitated on the grain boundaries as “Laves phase” during aging process. The toughness of the steel which contained much W might be degraded by such coarse precipitations on the grain boundaries. As a result, provisional specifications of the high Cr ferritic steel for SFR pipes and tubes were proposed. Creep-fatigue strength assessment procedure for the welded joints made of the steels was also investigated. An assessment procedure using 2-element model was proposed and verified by comparing with some creep-fatigue test results. The creep-fatigue lives observed in the experiments were well predicted by the proposed assessment procedure, but the failure of the welded joints really occurred in the heat affected zone (HAZ) in some creep-fatigue tests. Since the HAZ was not taken into account in the procedure, there were obviously some rooms for improvement. Creep-fatigue failure mechanisms of the welded joint must be investigated and the characteristics of the HAZ must be formulated for more precise creep-fatigue strength assessment.

Morphology, Distribution and Identification of Micro-Constituents Along Grain Boundaries in Nickel-Base Alloys

1973 ◽  
Vol 31 ◽  
pp. 176-177
Author(s):  
D. E. Fornwalt ◽  
A. R. Geary ◽  
B. H. Kear
Keyword(s):  
Electron Microscope ◽  
Grain Boundaries ◽  
Volume Fraction ◽  
Rupture Life ◽  
Stress Rupture ◽  
High Volume ◽  
Precipitate Morphology ◽  
Stress Rupture Life ◽  
Nickel Base ◽  
Scanning Electron

A systematic study has been made of the effects of various heat treatments on the microstructures of several experimental high volume fraction γ’ precipitation hardened nickel-base alloys, after doping with ∼2 w/o Hf so as to improve the stress rupture life and ductility. The most significant microstructural chan§e brought about by prolonged aging at temperatures in the range 1600°-1900°F was the decoration of grain boundaries with precipitate particles.Precipitation along the grain boundaries was first detected by optical microscopy, but it was necessary to use the scanning electron microscope to reveal the details of the precipitate morphology. Figure 1(a) shows the grain boundary precipitates in relief, after partial dissolution of the surrounding γ + γ’ matrix.

Measurement of the Displacement Across a Coincidence Grain Boundary

1977 ◽  
Vol 35 ◽  
pp. 124-125
Author(s):  
J. W. Matthews ◽  
W. M. Stobbs
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Stacking Fault ◽  
The Other ◽  
Measuring Technique ◽  
High Angle ◽  
Twin Boundaries ◽  
Rigid Displacement ◽  
Cubic Crystals ◽  
Lattice Displacement

Many high-angle grain boundaries in cubic crystals are thought to be either coincidence boundaries (1) or coincidence boundaries to which grain boundary dislocations have been added (1,2). Calculations of the arrangement of atoms inside coincidence boundaries suggest that the coincidence lattice will usually not be continuous across a coincidence boundary (3). There will usually be a rigid displacement of the lattice on one side of the boundary relative to that on the other. This displacement gives rise to a stacking fault in the coincidence lattice.Recently, Pond (4) and Smith (5) have measured the lattice displacement at coincidence boundaries in aluminum. We have developed (6) an alternative to the measuring technique used by them, and have used it to find two of the three components of the displacement at {112} lateral twin boundaries in gold. This paper describes our method and presents a brief account of the results we have obtained.

Lattice Imaging of Grain Boundaries in Ceramics

1977 ◽  
Vol 35 ◽  
pp. 114-115
Author(s):  
D. R. Clarke ◽  
G. Thomas
Keyword(s):  
Mechanical Properties ◽  
High Temperature ◽  
Silicon Nitride ◽  
Grain Boundaries ◽  
High Temperature Strength ◽  
Current Interest ◽  
Lattice Imaging ◽  
Special Significance ◽  
Structural Applications ◽  
Refractory Ceramics

Grain boundaries have long held a special significance to ceramicists. In part, this has been because it has been impossible until now to actually observe the boundaries themselves. Just as important, however, is the fact that the grain boundaries and their environs have a determing influence on both the mechanisms by which powder compaction occurs during fabrication, and on the overall mechanical properties of the material. One area where the grain boundary plays a particularly important role is in the high temperature strength of hot-pressed ceramics. This is a subject of current interest as extensive efforts are being made to develop ceramics, such as silicon nitride alloys, for high temperature structural applications. In this presentation we describe how the techniques of lattice fringe imaging have made it possible to study the grain boundaries in a number of refractory ceramics, and illustrate some of the findings.

The Effect of Specimen Thickness and Probe Size on Aem Analysis of Cr-Depletion Profiles in Sensitized Stainless Steel

1982 ◽  
Vol 40 ◽  
pp. 518-519
Author(s):  
E. L. Hall
Keyword(s):  
Grain Boundaries ◽  
Boundary Region ◽  
Chromium Concentration ◽  
Foil Thickness ◽  
Specimen Thickness ◽  
Probe Size ◽  
Analytical Electron ◽  
Analytical Electron Microscope ◽  
Sensitization Process ◽  
Compositional Gradients

Sensitization in stainless steels is caused by the formation of chromium-rich M23C6 carbides at grain boundaries, which depletes the adjacent matrix and boundary region of chromium, and hence leads to rapid intergranular attack. To fully understand the sensitization process, and to test the accuracy of theories proposed to model this process, it is necessary to obtain very accurate measurements of the chromium concentration at grain boundaries in sensitized specimens. Quantitative X-ray spectroscopy in the analytical electron microscope (AEM) enables the chromium concentration profile across these boundaries to be studied directly; however, it has been shown that a strong effect of foil thickness and electron probe size may be present in the analysis of rapidly-changing compositional gradients. The goal of this work is to examine these effects.

Electrolytic Isolation of Twin-Type Shock Deformation Structures

1967 ◽  
Vol 25 ◽  
pp. 318-319
Author(s):  
F. I. Grace ◽  
L. E. Murr
Keyword(s):  
Grain Boundaries ◽  
Thin Foil ◽  
Electrolyte Composition ◽  
Experimental Conditions ◽  
Average Current Density ◽  
Electron Transmission ◽  
Deformation Structures ◽  
The Matrix ◽  
Average Current ◽  
Specimen Edge

During the course of electron transmission investigations of the deformation structures associated with shock-loaded thin foil specimens of 70/30 brass, it was observed that in a number of instances preferential etching occurred along grain boundaries; and that the degree of etching appeared to depend upon the various experimental conditions prevailing during electropolishing. These included the electrolyte composition, the average current density, and the temperature in the vicinity of the specimen. In the specific case of 70/30 brass shock-loaded at pressures in the range 200-400 kilobars, the predominant mode of deformation was observed to be twin-type faults which in several cases exhibited preferential etching similar to that observed along grain boundaries. A novel feature of this particular phenomenon was that in certain cases, especially for twins located in the vicinity of the specimen edge, the etching or preferential electropolishing literally isolated these structures from the matrix.

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