scholarly journals Assessment of wear micromechanisms on a laser textured cemented carbide tool during abrasive-like machining by FIB/FESEM

Friction ◽  
2020 ◽  
Author(s):  
Shiqi Fang ◽  
Dirk Bähre ◽  
Luis Llanes
Keyword(s):  
Focused Ion Beam ◽  
Ion Beam ◽  
Local Level ◽  
Surface Texturing ◽  
Laser Surface ◽  
Laser Surface Texturing ◽  
Near Surface ◽  
Dual Beam ◽  
Cemented Carbide Tool ◽  
Microstructural Integrity

Abstract The combined use of focused ion beam (FIB) milling and field-emission scanning electron microscopy inspection (FESEM) is a unique and successful approach for assessment of near-surface phenomena at specific and selected locations. In this study, a FIB/FESEM dual-beam platform was implemented to docment and analyze the wear micromechanisms on a laser-surface textured (LST) hardmetal (HM) tool. In particular, changes in surface and microstructural integrity of the laser-sculptured pyramids (effective cutting microfeatures) were characterized after testing the LST-HM tool against a steel workpiece in a workbench designed to simulate an external honing process. It was demonstrated that: (1) laser-surface texturing does not degrade the intrinsic surface integrity and tool effectiveness of HM pyramids; and (2) there exists a correlation between the wear and loading of shaped pyramids at the local level. Hence, the enhanced performance of the laser-textured tool should consider the pyramid geometry aspects rather than the microstructure assemblage of the HM grade used, at least for attempted abrasive applications.

Effects of Laser Surface Texturing on the Microstructure and Frictional Characteristics of Zirconia Surfaces Under Liquid and Solid Lubrication

2005 ◽  
Author(s):  
Peter J. Blau ◽  
Jun Qu ◽  
Laura Riester
Keyword(s):  
Electron Microscopy ◽  
Surface Texturing ◽  
Microstructural Characterization ◽  
Laser Surface ◽  
Acoustic Microscopy ◽  
Laser Surface Texturing ◽  
Grain Structure ◽  
Solid Lubrication ◽  
Near Surface ◽  
Frictional Behavior

The production of dimple patterns in surfaces by laser surface texturing (LST) has received considerable interest. The current research characterized the effects of LST on the near-surface microstructures in transformation-toughened zirconia (TTZ) and investigated how dimpling can affect reciprocating frictional behavior under both liquid and solid lubrication. Microstructural characterization included scanning electron microscopy (SEM), transmission electron microscopy (TEM), scanning acoustic microscopy (SAcM), and nanoindentation testing. Fine-scale micro-cracks were observed in both the rims and bottoms of dimple craters. Most of the laser-affected zone is composed of very fine grains with diameters 125∼150 nm, but no grain structure was observed nearest the rim edges. The distribution of residual stresses around the dimples, induced by LST, was revealed by SAcM. Nanoindentation tests of TTZ indicated no significant differences in hardness or elastic modulus between the material near the dimples and in the bulk. Counterface materials in the flat-on-flat reciprocating sliding tests included silicon nitride and a galling-resistant stainless steel. Friction tests were conducted under both liquid (mineral oil) and solid (fine graphite powder) lubrication. Dimpling did not show measurable improvement on frictional behavior under the applied test conditions, although they were supposed to function as lubricant reservoirs and debris traps.

Direct Plan View FIB Liftout for Near-Surface Defect Analysis in TEM

2013 ◽  
Author(s):  
Max L. Lifson ◽  
Carla M. Chapman ◽  
D. Philip Pokrinchak ◽  
Phyllis J. Campbell ◽  
Greg S. Chrisman ◽  
...  
Keyword(s):  
Failure Analysis ◽  
Silicon Germanium ◽  
Focused Ion Beam ◽  
Surface Defects ◽  
Ion Beam ◽  
Misfit Dislocations ◽  
Tem Analysis ◽  
Plan View ◽  
Near Surface ◽  
Straightforward Method

Abstract Plan view TEM imaging is a powerful technique for failure analysis and semiconductor process characterization. Sample preparation for near-surface defects requires additional care, as the surface of the sample needs to be protected to avoid unintentionally induced damage. This paper demonstrates a straightforward method to create plan view samples in a dual beam focused ion beam (FIB) for TEM studies of near-surface defects, such as misfit dislocations in heteroepitaxial growths. Results show that misfit dislocations are easily imaged in bright-field TEM and STEM for silicon-germanium epitaxial growth. Since FIB tools are ubiquitous in semiconductor failure analysis labs today, the plan view method presented provides a quick to implement, fast, consistent, and straightforward method of generating samples for TEM analysis. While this technique has been optimized for near-surface defects, it can be used with any application requiring plan view TEM analysis.

To Eliminate Curtain Effect of FIB TEM Samples by a Combination of Sample Dicing and Backside Milling

2014 ◽  
Author(s):  
Jian-Shing Luo ◽  
Hsiu Ting Lee
Keyword(s):  
Sample Preparation ◽  
Focused Ion Beam ◽  
Preparation Method ◽  
Low Cost ◽  
Ion Beam ◽  
Sample Preparation Method ◽  
Site Specific ◽  
Dual Beam ◽  
Transmission Electron

Abstract Several methods are used to invert samples 180 deg in a dual beam focused ion beam (FIB) system for backside milling by a specific in-situ lift out system or stages. However, most of those methods occupied too much time on FIB systems or requires a specific in-situ lift out system. This paper provides a novel transmission electron microscopy (TEM) sample preparation method to eliminate the curtain effect completely by a combination of backside milling and sample dicing with low cost and less FIB time. The procedures of the TEM pre-thinned sample preparation method using a combination of sample dicing and backside milling are described step by step. From the analysis results, the method has applied successfully to eliminate the curtain effect of dual beam FIB TEM samples for both random and site specific addresses.

Manufacturing In-Line Whole Wafer Focused Ion Beam (FIB) Memory Address Descramble Verification

2008 ◽  
Author(s):  
Steven B. Herschbein ◽  
Hyoung H. Kang ◽  
Scott L. Jansen ◽  
Andrew S. Dalton
Keyword(s):  
Flip Chip ◽  
Focused Ion Beam ◽  
Ion Beam ◽  
Random Access ◽  
Cell Counting ◽  
Test Results ◽  
Laboratory Procedure ◽  
Memory Array ◽  
Dual Beam ◽  
Process Level

Abstract Test engineers and failure analyst familiar with random access memory arrays have probably encountered the frustration of dealing with address descrambling. The resulting nonsequential internal bit cell counting scheme often means that the location of the failing cell under investigation is nowhere near where it is expected to be. A logical to physical algorithm for decoding the standard library block might have been provided with the design, but is it still correct now that the array has been halved and inverted to fit the available space in a new processor chip? Off-line labs have traditionally been tasked with array layout verification. In the past, hard and soft failures could be induced on the frontside of finished product, then bitmapped to see if the sites were in agreement. As density tightened, flip-chip FIB techniques to induce a pattern of hard fails on packaged devices came into practice. While the backside FIB edit method is effective, it is complex and expensive. The installation of an in-line Dual Beam FIB created new opportunities to move FA tasks out of the lab and into the FAB. Using a new edit procedure, selected wafers have an extensive pattern of defects 'written' directly into the memory array at an early process level. Bitmapping of the RAM blocks upon wafer completion is then used to verify correlation between the physical damaged cells and the logical sites called out in the test results. This early feedback in-line methodology has worked so well that it has almost entirely displaced the complex laboratory procedure of backside FIB memory array descramble verification.

Ion Beam Imaging Methodology of Invisible Metal under Insulator Using High Energy Electron Beam Charging

2007 ◽  
Author(s):  
C.H. Wang ◽  
S.P. Chang ◽  
C.F. Chang ◽  
J.Y. Chiou
Keyword(s):  
Metal Ion ◽  
Focused Ion Beam ◽  
Ion Beam ◽  
Electrical Measurement ◽  
High Energy ◽  
Advanced Technology ◽  
High Energy Electron ◽  
Common Assumption ◽  
Dual Beam ◽  
Imaging Methodology

Abstract Focused ion beam (FIB) is a popular tool for physical failure analysis (FA), especially for circuit repair. FIB is especially useful on advanced technology where the FIB is used to modify the circuit for new layout verification or electrical measurement. The samples are prepared till inter-metal dielectric (IMD), then a hole is dug or a metal is deposited or oxide is deposited by FIB. A common assumption is made that metal under oxide can not be seen by FIB. But a metal ion image is desired for further action. Dual beam, FIB and Scanning Electron Microscope (SEM), tools have a special advantage. When switching back and forth from SEM to FIB the observation has been made that the metal lines can be imaged. The details of this technique will be discussed below.

scholarly journals Does laser surface texturing really have a negative impact on the fatigue lifetime of mechanical components?

Friction ◽  
2021 ◽  
Author(s):  
Chia-Jui Hsu ◽  
Andreas Stratmann ◽  
Simon Medina ◽  
Georg Jacobs ◽  
Frank Mücklich ◽  
...  
Keyword(s):  
Boundary Lubrication ◽  
Surface Texturing ◽  
Contact Stresses ◽  
Laser Surface ◽  
Laser Surface Texturing ◽  
Wear Loss ◽  
Textured Surface ◽  
Periodic Patterns ◽  
Rolling Bearings ◽  
Fatigue Lifetime

AbstractLaser surface texturing (LST) has been proven to improve the tribological performance of machine elements. The micro-scale patterns manufactured by LST may act as lubricant reservoirs, thus supplying oil when encountering insufficient lubrication. However, not many studies have investigated the use of LST in the boundary lubrication regime, likely due to concerns of higher contact stresses that can occur with the increasing surface roughness. This study aims to examine the influence of LST on the fatigue lifetime of thrust rolling bearings under boundary lubrication. A series of periodic patterns were produced on the thrust rolling bearings, using two geometrically different designs, namely cross and dimple patterns. Base oil ISO VG 100 mixed with 0.05 wt% P of zinc dialkyldithiophosphate (ZDDP) was supplied. The bearings with cross patterns reduce the wear loss by two orders of magnitude. The patterns not only retain lubricant in the textured pockets but also enhance the formation of an anti-wear tribofilm. The tribofilm generation may be improved by the higher contact stresses that occur when using the textured surface. Therefore, in contrast to the negative concerns, the ball bearings with cross patterns were instead found to increase the fatigue life by a factor of three.

Tribological effects of laser surface texturing and residual stress

2018 ◽  
Vol 70 (1) ◽  
pp. 126-132 ◽  
Author(s):  
Shuwen Wang ◽  
Feiyan Yan ◽  
Ao Chen
Keyword(s):  
Residual Stress ◽  
Wear Resistance ◽  
Friction And Wear ◽  
Surface Texturing ◽  
Laser Surface ◽  
Friction Reduction ◽  
Laser Surface Texturing ◽  
Wear Testing ◽  
Content Type ◽  
Surface Textures

Purpose The purpose of this paper is to investigate the tribological effects of laser surface texturing (LST) and residual stress on functional surfaces. Design/methodology/approach Three different surface textures (circular dimple, elliptical dimple and groove) with two different textured area ratios (10 and 20 per cent) are designed and fabricated by a Picosecond Nd YAG Laser machine. The friction and wear performance of textured specimens is tested using a UMT-2 friction and wear testing machine in mixed lubrication. Findings Test results show that elliptical dimples exhibit the best performance in wear resistance, circular dimples in friction reduction and grooves in stabilization of friction. The surfaces with larger textured area density exhibit better performance in both friction reduction and wear resistance. The improved performance of LST is the coupled effect of surface texture and residual stress. Originality/value The findings of this study may provide guidance for optimal design of functional surface textures in reciprocating sliding contacts under mixed or hydrodynamic lubrication, which can be used in automotive and other industrial applications.

Effect of Micro-Manufacturing Processes on Surface Behavior

2007 ◽  
Author(s):  
Tiffany Davis ◽  
Jian Cao ◽  
Wei Chen ◽  
Q. Jane Wang ◽  
Cedric Xia ◽  
...  
Keyword(s):  
Surface Texture ◽  
Surface Texturing ◽  
Steel Sample ◽  
Laser Surface ◽  
Laser Surface Texturing ◽  
Copper Sheet ◽  
Property Variation ◽  
Nano Indentation ◽  
Interface Surface ◽  
Significant Difference

Surface texturing has become a valuable technique for reducing friction and wear in contacting parts; laser surface texturing is one such method used to create micro-dimples on the interface surface. This work investigates the surface material property variation caused by laser surface texturing. The hardness and modulus of elasticity of a steel laser surface texture sample were evaluated near the dimples and away from the dimpled zone through nano-indentation. Resulting data shows that no significant difference exists between the material properties from the two positions. An alternate technique for surface texture generation was also explored, involving the use of micro-punches to create surface features in a metal sample. Computational simulations were performed using a second material underneath a thin copper sheet. The second material was present to serve as a support and to allow extensive deformation of the top material. The choice of the support material and ratio of material thicknesses was optimized to minimize pile up. Trials were conducted for three base supporting materials: PTFE, PMMA, and aluminum. Results show that PMMA performed better than the other materials. Positive deflection was minimized when the PMMA thickness was at least fifteen times that of the copper sheet. Physical experiments were completed with a thin copper sheet to verify the results. An array of micro-indentations was also created in a bulk steel sample. In order to assess the effect of dimpling via micro-forming, nano-indentation was performed near and far from the deformed material of the dimples. Similar to the laser textured sample, no significant differences were found between the two locations.

Effectiveness of multi-shape laser surface texturing in the reduction of friction under lubrication regime

2016 ◽  
Vol 68 (1) ◽  
pp. 116-124 ◽  
Author(s):  
Dawit Zenebe Segu ◽  
Pyung Hwang
Keyword(s):  
Hydrodynamic Lubrication ◽  
Surface Texturing ◽  
Laser Surface ◽  
Laser Surface Texturing ◽  
Textured Surface ◽  
Content Type ◽  
Laser Ablation Process ◽  
Specific Formula ◽  
Steel Surfaces ◽  
Lubrication Conditions

Purpose – The purpose of this paper is to investigate and discuss the effect of multi-shape laser surface texturing (LST) steel surfaces on tribological performance. Design/methodology/approach – The textured surface with some specific formula arrays was fabricated by laser ablation process by combining patterns of circles and triangles, circles and squares and circles and ellipses. The tribological test was performed by a flat-on-flat tribometer under dry and lubrication conditions, and results were compared with that of untextured surface. Findings – The results showed that the textured surface had better friction coefficient performance than the untextured surface due to hydrodynamic lubrication effect. Through an increase in sliding speed, the beneficial effect of LST performance was achieved under dry and lubrication conditions. Originality/value – This paper develops multi-shape LST steel surfaces for improving the friction and wear performance under dry and lubrication conditions.

Laser surface texturing inhibits Bioflim formation

2021 ◽  
pp. 124909
Author(s):  
Venkata Sai Prabhu Suraj Nanduru ◽  
Nagalla Siva Ramakrishna ◽  
Ramineni Surendra Babu ◽  
P. Dinesh Babu ◽  
P. Marimuthu ◽  
...  
Keyword(s):  
Surface Texturing ◽  
Laser Surface ◽  
Laser Surface Texturing
Sign in / Sign up

Export Citation Format

Share Document