The effect of TiO2 and SiO2 nanoparticles on flexural strength of poly (methyl methacrylate) acrylic resins

2013 ◽  
Vol 57 (1) ◽  
pp. 15-19 ◽  
Author(s):  
Ahmad Sodagar ◽  
Abbas Bahador ◽  
Safia Khalil ◽  
Atefe Saffar Shahroudi ◽  
Mohammad Zaman Kassaee
Materials ◽  
2019 ◽  
Vol 12 (24) ◽  
pp. 4146 ◽  
Author(s):  
Grzegorz Chladek ◽  
Katarzyna Pakieła ◽  
Wojciech Pakieła ◽  
Jarosław Żmudzki ◽  
Marcin Adamiak ◽  
...  

Colonization of polymeric dental prosthetic materials by yeast-like fungi and the association of these microorganisms with complications occurring during prosthetic treatment are important clinical problems. In previously presented research, submicron inorganic particles of silver sodium hydrogen zirconium phosphate (S–P) were introduced into poly(methyl methacrylate) (PMMA) denture base material which allowed for obtaining the antimicrobial effect during a 90 day experiment. The aim of the present study was to investigate the flexural strength, impact strength, hardness, wear resistance, sorption, and solubility during three months of storage in distilled water. With increasing S–P concentration after 2 days of conditioning in distilled water, reduced values of flexural strength (107–72 MPa), impact strength (18.4–5.5 MPa) as well as enhanced solubility (0.95–1.49 µg/mm3) were registered, but they were at acceptable levels, and the sorption was stable. Favorable changes included increased hardness (198–238 MPa), flexural modulus (2.9–3.3 GPa), and decreased volume loss during wear test (2.9–0.2 mm3). The percentage changes of the analyzed properties during the 90 days of storage in distilled water were similar for all materials.


Materials ◽  
2020 ◽  
Vol 13 (2) ◽  
pp. 371 ◽  
Author(s):  
Myung-Jin Lee ◽  
Min-Ji Kim ◽  
Sang-Hwan Oh ◽  
Jae-Sung Kwon

Despite the many advantages of poly (methyl methacrylate) (PMMA) as a dental polymer, its antifungal and antibacterial effects remain limited. Here, phytoncide was incorporated into PMMA to inhibit fungal and biofilm accumulation without impairing the basic and biological properties of PMMA. A variable amount of phytoncide (0 wt % to 5 wt %) was incorporated into PMMA, and the basic material properties of microhardness, flexural strength and gloss were evaluated. In addition, cell viability was confirmed by MTT assay. This MTT assay measures cell viability via metabolic activity, and the color intensity of the formazan correlates viable cells. The fungal adhesion and viability on the PMMA surfaces were evaluated using Candida albicans (a pathogenic yeast). Finally, the thickness of saliva-derived biofilm was estimated. The flexural strength of PMMA decreased with increasing phytoncide contents, whereas there were no significant differences in the microhardness and gloss (p > 0.05) and the cell viability (p > 0.05) between the control and the phytoncide-incorporated PMMA samples. The amounts of adherent Candida albicans colony-forming unit (CFU) counts, and saliva-derived biofilm thickness were significantly lower in the phytoncide-incorporated PMMA compared to the control (p < 0.05). Hence, it was concluded that the incorporation of appropriate amounts of phytoncide in PMMA demonstrated antifungal effects while maintaining the properties, which could be a possible use in dentistry application such as denture base resin.


2014 ◽  
Vol 2014 ◽  
pp. 1-8 ◽  
Author(s):  
L. S. Acosta-Torres ◽  
M. C. Arenas ◽  
R. E. Nuñez­-Anita ◽  
F. H. Barceló-Santana ◽  
C. A. Álvarez-Gayosso ◽  
...  

The highlight of this study was the synthesis of nanopigmented poly(methyl methacrylate) nanoparticles that were further processed using a water bath and/or microwave energy for dentures. The experimental acrylic resins were physicochemically characterized, and the adherence ofCandida albicansand biocompatibility were assessed. A nanopigmented acrylic resin cured by a water bath or by microwave energy was obtained. The acrylic specimens possess similar properties to commercial acrylic resins, but the transverse strength and porosity were slightly improved. The acrylic resins cured with microwave energy exhibited reducedC. albicansadherence. These results demonstrate an improved noncytotoxic material for the manufacturing of denture bases in dentistry.


Materials ◽  
2019 ◽  
Vol 12 (20) ◽  
pp. 3438 ◽  
Author(s):  
Utkarsh Mangal ◽  
Ji-Yeong Kim ◽  
Ji-Young Seo ◽  
Jae-Sung Kwon ◽  
Sung-Hwan Choi

Herein we evaluate the effect of nanodiamond (ND) incorporation on the mechanical properties of poly(methyl methacrylate) (PMMA) nanocomposite. Three quantities of ND (0.1, 0.3, and 0.5 wt.%) were tested against the control and zirconium oxide nanoparticles (ZrO). Flexural strength and elastic modulus were measured using a three-point bending test, surface hardness was evaluated using the Vickers hardness test, and surface roughness was evaluated using atomic force microscopy (AFM), while fungal adhesion and viability were studied using Candida albicans. Samples were also analyzed for biofilm thickness and biomass in a saliva-derived biofilm model. All groups of ND-PMMA nanocomposites had significantly greater mean flexural strengths and statistically improved elastic modulus, compared to the control and ZrO groups (P < 0.001). The Vickers hardness values significantly increased compared to the control group (P < 0.001) with 0.3% and 0.5% ND. ND addition also gave significant reduction in fungal adhesion and viability (P < 0.001) compared to the control group. Finally, salivary biofilm formation was markedly reduced compared to the ZrO group. Hence, the incorporation of 0.1–0.5 wt.% ND with auto- polymerized PMMA resin significantly improved the flexural strength, elastic modulus, and surface hardness, and provided considerable fungal resistance.


2008 ◽  
Vol 19 (3) ◽  
pp. 190-196 ◽  
Author(s):  
Wander José da Silva ◽  
Rodrigo Nunes Rached ◽  
Pedro Luis Rosalen ◽  
Altair Antoninha Del Bel Cury

The prevalence of candidosis in denture wearers is as well established as its treatment with antifungal agents (AAs). However, little research has been done regarding the effects of AAs on denture base surfaces. Therefore, the aim of this study was to evaluate the effects of fluconazole (FLU), nystatin (NYS) and propolis orabase gel (PRO) on poly (methyl-methacrylate) (PMMA) surfaces. Deionized water and orabase gel without any active component were used as control groups. Conventional heat-polymerized (Clássico) and microwave-polymerized (Onda Cryl) acrylic resins were used. After polymerization, the specimens were polished and had their surfaces evaluated for roughness, free energy and Knoop hardness. Subsequently, specimens were immersed in AAs and controls for 14 days at 35±2 °C and all variables were measured again. Data were analyzed statistically by 2-way ANOVA followed by Tukey's test ( α=0.05). Roughness results showed similar behavior for both PMMA resins, with PRO reaching the highest values and differing significantly from the other AAs (p<0.05). No statistically significant differences (p>0.05) were found between the two PMMA resins or between NYS and FLU as regards surface free energy. In conclusion, PRO was able to induce changes in PMMA surface properties, such as roughness, which could be related to microbial adhesion.


2018 ◽  
Vol 54 (1A) ◽  
pp. 285
Author(s):  
Long Giang Bach

This article describes the fabrication of SiO2 nanoparticles grafted with poly(methyl methacrylate) (PMMA) via a fascinating reversible addition-fragmentation chain transfer (RAFT) polymerization by adopting “grafting from” approach. The silane coupling agent, S-benzyl S’-trimethoxysilylpropyltrithiocarbonate, was anchored onto SiO2 nanoparticles in a simple procedure using a ligand exchange reaction. RAFT agents-anchored SiO2 nanoparticles were then used for the surface-initiated RAFT polymerization of MMA to fabricate structurally well-defined, core-shell SiO2-g-PMMA nanocomposites. The structure and properties of the as-synthesized nanocomposites were investigated by Fourier Transformed Infrared Spectrophotometry (FT-IR), X-ray Photoelectron Spectroscopy (XPS), Thermogravimetric analysis (TGA), Field Emission Scanning Electron Microscopy (FE-SEM).


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