scholarly journals Overview of the soybean process in the crushing industry

OCL ◽  
2020 ◽  
Vol 27 ◽  
pp. 60
Author(s):  
Anibal Demarco ◽  
Véronique Gibon
Keyword(s):  
Solvent Extraction ◽  
Coming Out ◽  
Oil Content ◽  
Production Capacity ◽  
Extraction Process ◽  
Plant Production ◽  
Residual Oil ◽  
Lower Efficiency ◽  
Residual Solvent ◽  
Air Stream

A minimal residual oil content in the meal coming out of the hexane extractor is a clear benefit for a crushing plant; the more oil yield the better revenue for the crusher. In a modern and efficient extraction plant, a residual oil content ≤ 0.5% for soybean meal is expected. The first step for an efficient solvent extraction is a good preparation process; its optimization makes it possible to shape the seeds for effective leaching and washing of the oil. Preparation also goes through an optimized dehulling (warm or hot dehulling) allowing, in an economical way, to maximize the protein content. The seed flaking can optionally be complemented by expanding which permits rupture of a more efficient portion of the cell walls. Solvent extraction consists in washing the prepared material in a countercurrent multistage process to enable a reasonable quantity of solvent to extract a maximal amount of oil. Major progresses in solvent extraction relate to plant production capacity increases which propelled technological improvements. Following extraction, the solvent is distilled from the miscella and recovered. A mineral oil system absorbs the residual solvent out of the effluent air stream. A single integrated unit also called desolventizer/toaster/dryer/cooler removes the solvent, toasts the meal in order to control the anti-nutritional factors and reduces moisture and temperature to levels appropriate for storage and transport. Although today the industry is mostly based on the solvent extraction process, certain strict constraints in the environmental aspects suggest alternative processes to minimize hexane emissions and even the return to mechanical operations (for example full press) allowing to completely eliminate the use of solvent at the expense of lower efficiency.

scholarly journals Solid Concentration Effect for Solvent Extraction Process of Oily Contaminated Soil

REAKTOR ◽  
2019 ◽  
Vol 19 (2) ◽  
pp. 84-88
Author(s):  
Lely Fitriyani ◽  
Edwan Karadena ◽  
Sukandar Sukandar
Keyword(s):  
Solvent Extraction ◽  
Contaminated Soil ◽  
Petroleum Hydrocarbon ◽  
Oil Content ◽  
Soil Washing ◽  
Extraction Process ◽  
Total Petroleum Hydrocarbon ◽  
The Other ◽  
Solvent Ratio ◽  
Solid Concentration

Solvent extraction has been used as a method to wash oil content of oily contaminated soil in industry for years. Some solvents and temperature ranges has been chosen to increase the oil recovery rate of extraction process, however only few studies reported that it has been able to reach remaining Total Petroleum Hydrocarbon (TPH) less than 0.5% in less than 30 minutes. During the experiments, acetone and toluene chosen to extract oil content from contaminated soil by using solvent extraction process. Temperature selected were between 24°C up to 70°C. Mixing apparatus which has been utilized was centrifugation machine with 1000 rpm (1570 g) operational speed. Duration of treatment process was 10 minutes with some variations of solid to solvent ratio. During the experiments, it was observed that by using toluene and acetone as solvents, the optimum Total Petroleum Hydrocarbon (TPH) removal obtained at temperature 50°C. In the other hand, optimum solid to solvent ratio toluene ratio was 1:6. As a solvent acetone observed capable to reduce TPH content until below 0.5% as threshold limit for TPH of contaminated soil regulated by environmental regulation in Indonesia. During the experiments it was also observed the dependency of solid concentration (Cs) with dissociation coefficient (KD). In the other hand, heavy metal at the remaining extracted soil after soil washing was observed available in safe concentration to be discharged to the environment base on regulation in Indonesia. Keywords: solvent extraction, soil washing, contaminated soil, TPH, centrifugation, oil sludge, acetone, toluene, solid treatment.

scholarly journals Proses Ekstraksi Minyak Alga Chlorella.sp menggunakan Metode Sokhletasi

2020 ◽  
Vol 5 (1) ◽  
pp. 12
Author(s):  
Yustia Wulandari Mirzayanti ◽  
Dian Yanuarita Purwaningsih ◽  
Siti Nur Faida ◽  
Nurza Istifara
Keyword(s):  
Fatty Acids ◽  
Linoleic Acid ◽  
Solvent Extraction ◽  
Oil Content ◽  
Extraction Process ◽  
Oil Extraction ◽  
Reproductive Rate ◽  
Acid Number ◽  
Extraction Time ◽  
Algae Oil

 Chlorella.sp is a type of green algae and has no flagella. One of the advantages of algae Chlorella.sp is that it has a high reproductive rate. Chlorella.sp algae is one of the algae that has oil content from its body mass. This study aims to determine the effect of the amount of solvent, extraction time on the Chlorella.sp algae oil extraction process using methanol solvent through the sokhletation method. Also, knowing the composition of fatty acids and acid numbers from algae oil Chlorella.sp. The ratio of Chlorella.sp algae: the amount of methanol solvent used are 1: 6; 1: 9 and 1:12 gr/ml. Then for the extraction time variation are 4; 4,5; 5; 5.5 and 6 hours. Chlorella.sp algae oil extraction process using sokhletation method is carried out at 70oC. The best results through the% yield and number parameters obtained by 17.98% Chlorella.sp algae oil yield ratio of 1:12 and the extraction time for 5.5 hours. Chlorella.sp algae oil has an acid number of 3.14 mg NaOH/g. Based on the results of the GC-MS test it is known that Chlorella.sp algae are dominated by linoleic acid by 55.01%area. ABSTRAKChlorella.sp merupakan jenis alga berwarna hijau dan tidak memiliki flagella. Salah satu kelebihan dari alga Chlorella.sp yaitu memiliki tingkat reproduksi yang tinggi. Alga Chlorella.sp merupakan salah satu alga yang memiliki kandungan minyak dari massa tubuhnya. Penelitian ini bertujuan untuk mengetahui pengaruh jumlah pelarut, waktu ekstraksi pada proses ekstraksi minyak alga Chlorella.sp menggunakan pelarut methanol melalui metode sokhletasi. Selain itu, mengetahui komposisi asam lemak dan bilangan asam dari minyak alga Chlorella.sp. Variasi rasio perbandingan antara alga Chlorella.sp : jumlah pelarut metanol yang digunakan yaitu 1:6; 1:9 dan 1:12 gr/ml. kemudian untuk variasi waktu ekstraksi adalah 4; 4,5; 5; 5,5 dan 6 jam. Proses ekstraksi minyak alga Chlorella.sp menggunakan metode sokhletasi dilakukan pada temperatur 70oC. Hasil terbaik melalui parameter %yield dan bilangan diperoleh sebesar 17,98% yield minyak alga Chlorella.sp dengan ratio perbandingan 1:12 dan waktu ekatraksi selama 5,5 jam. Minyak alga Chlorella.sp memiliki bilangan asam sebesar 3,14 mgNaOH/g. Berdasarkan hasil uji GC-MS diketahui bahwa untuk alga jenis Chlorella.sp didominasi oleh asam linoleat sebesar 55,01%area.

scholarly journals A Technical Analysis of Solid Recovered Fuel from Torrefied Jatropha Seed Residue via a Two-Stage Mechanical Screw Press and Solvent Extraction Process

Energies ◽  
2021 ◽  
Vol 14 (23) ◽  
pp. 7876
Author(s):  
Min-Hao Yuan ◽  
Chia-Chi Chang ◽  
Tsung-Chi Hsu ◽  
Je-Lueng Shie ◽  
Yi-Hung Chen ◽  
...  
Keyword(s):  
Solvent Extraction ◽  
Enhanced Recovery ◽  
Extraction Process ◽  
Thermal Reaction ◽  
Net Energy ◽  
Residual Oil ◽  
Two Stage ◽  
Screw Pressing ◽  
Tar Oil ◽  
Jatropha Seed

This study investigated the torrefaction of de-oiled Jatropha seed residue after a two-stage sequential process consisting of mechanical screw pressing and solvent extraction using n-hexane (denoted as JMS). The optimal torrefaction temperature (Tr) and torrefaction time (tr) were determined in the ranges of 260–300 °C and 10–60 min, respectively, so to achieve a better heating value and satisfactory energy densification (ED) with acceptable mass loss. Thermogravimetric analysis was employed to elucidate the thermal decomposition behaviors of JMS. By comparison with the torrefaction of Jatropha seed residue after mechanical oil extraction by screw pressing only (namely, JMET), the results indicated that the ED of the torrefaction of JMS yielding the torrefied product JMST (two-stage product) was higher than that of the torrefaction of JME giving the torrefied product JMET (single-stage product). Further, it was found that JMET contained some tar, which was attributed to a thermal reaction in the residual oil in JME during torrefaction. The tar/oil content of JMET was about 1.0–1.8 wt.% in the determined optimal conditions. Thus, the enhanced recovery of the residual oil is advantageous not only because it allows obtaining more oil from Jatropha seed residue with a positive net energy gain but also because it prevents the formation of tar in torrefied biomass products.

scholarly journals Effect of Oil Content in Tea-seed Pancake on the Determination of Tea Saponin

2021 ◽  
Vol 290 ◽  
pp. 01018
Author(s):  
Longfa Jiang ◽  
Lingyun Bai ◽  
Shumin Zhang ◽  
Heng zhang ◽  
Xuming Tu
Keyword(s):  
Oil Content ◽  
Extraction Process ◽  
National Standard ◽  
Residual Oil ◽  
Tea Saponin ◽  
Saponin Content ◽  
Ether Extraction ◽  
Alkali Hydrolysis ◽  
Subsequent Acid

According to the national standard for the determination of tea saponin content in tea-seed pancake (GB/T 35131-2017), tea saponin was obtained by extracting oil with ethanol and removing solvent. The actual samples of tea-seed pancake did not completely remove the oil, and some of the residual oil content was as high as 9%. Due to the long period of national standard determination, people often use ethanol to extract tea saponin directly, instead of subsequent acid hydrolysis or alkali hydrolysis steps, so as to realize the rapid evaluation of tea-seed pancake quality. In this case, the residual oil has a greater impact on the results. If it was still tested according to the national standard method, the result will be much higher than the actual result. In this work, petroleum ether extraction process was selected before ethanol extraction to remove the residual oil. Experimental results showed that, the accuracy of the determination was effectively improved.

scholarly journals Study on the Effect and Mechanism of Impurity Aluminum on the Solvent Extraction of Rare Earth Elements (Nd, Pr, La) by P204-P350 in Chloride Solution

Minerals ◽  
2021 ◽  
Vol 11 (1) ◽  
pp. 61
Author(s):  
Wenjie Zhang ◽  
Xian Xie ◽  
Xiong Tong ◽  
Yunpeng Du ◽  
Qiang Song ◽  
...  
Keyword(s):  
Rare Earth ◽  
Solvent Extraction ◽  
Rare Earth Elements ◽  
Organic Phase ◽  
Extraction Process ◽  
Industrial Applications ◽  
Separation And Purification ◽  
Aluminum Ion ◽  
Hydrochloric Acid Medium ◽  
Impurity Ion

Solvent extraction is the most widely used method for separation and purification of rare earth elements, and organic extractants such as di(2-ethylhexyl) phosphoric acid (P204) and di(1-methyl-heptyl) methyl phosphonate (P350) are most commonly used for industrial applications. However, the presence of impurity ions in the feed liquid during extraction can easily emulsify the extractant and affect the quality of rare earth products. Aluminum ion is the most common impurity ion in the feed liquid, and it is an important cause of emulsification of the extractant. In this study, the influence of aluminum ion was investigated on the extraction of light rare earth elements by the P204-P350 system in hydrochloric acid medium. The results show that Al3+ competes with light rare earths in the extraction process, reducing the overall extraction rate. In addition, the Al3+ stripping rate is low and there is continuous accumulation of Al3+ in the organic phase during the stripping process, affecting the extraction efficiency and even causing emulsification. The slope method and infrared detection were utilized to explore the formation of an extraction compound of Al3+ and the extractant P204-P350 that entered the organic phase as AlCl[(HA)2]2P350(o).

scholarly journals Separation of Sn, Sb, Bi, and Cu from Tin Anode Slime by Solvent Extraction and Chemical Precipitation

Metals ◽  
2021 ◽  
Vol 11 (3) ◽  
pp. 515
Author(s):  
Wei-Sheng Chen ◽  
Shota Mesaki ◽  
Cheng-Han Lee
Keyword(s):  
Solvent Extraction ◽  
Liquid Phase ◽  
Ph Value ◽  
Chemical Precipitation ◽  
Extraction Process ◽  
Refining Process ◽  
Anode Slime ◽  
Electrolytic Refining ◽  
Precipitation Procedure ◽  
Tin Anode

Tin anode slime is a by-product of the tin electrolytic refining process. This study investigated a route to separate Sn, Sb, Bi, and Cu from tin anode slime after leaching with hydrochloric acid. In the solvent extraction process with tributyl phosphate, Sb and Sn were extracted into the organic phase. Bi and Cu were unextracted and remained in the liquid phase. In the stripping experiment, Sb and Sn were stripped and separated with HCl and HNO3. Bi and Cu in the aqueous phase were also separated with chemical precipitation procedure by controlling pH value. The purities of Sn, Sb, Cu solution and the Bi-containing solid were 96.25%, 83.65%, 97.51%, and 92.1%. The recovery rates of Sn, Sb, Cu, and Bi were 76.2%, 67.1%, and 96.2% and 92.4%.

Residual solvent extraction via chemical displacement for efficient and stable perovskite solar cells

2021 ◽  
Vol 61 ◽  
pp. 8-14
Author(s):  
Min Fang ◽  
Lei Tao ◽  
Wen Wu ◽  
Qi Wei ◽  
Yingdong Xia ◽  
...  
Keyword(s):  
Solar Cells ◽  
Solvent Extraction ◽  
Perovskite Solar Cells ◽  
Residual Solvent

Facile fractionation of bamboo hydrolysate and characterization of isolated lignin and lignin-carbohydrate complexes

Holzforschung ◽  
2020 ◽  
Vol 0 (0) ◽  
Author(s):  
Xiaodi Wang ◽  
Yongchao Zhang ◽  
Luyao Wang ◽  
Xiaoju Wang ◽  
Qingxi Hou ◽  
...  
Keyword(s):  
Solvent Extraction ◽  
Organic Solvent ◽  
Extraction Process ◽  
Water Soluble ◽  
Organic Solvent Extraction ◽  
Glycoside Linkage ◽  
Potential Applications ◽  
Tremendous Amount ◽  
Main Components ◽  
Hemicellulosic Sugars

AbstractAn efficient separation technology for hydrolysates towards a full valorization of bamboo is still a tough challenge, especially regarding the lignin and lignin-carbohydrate complexes (LCCs). The present study aimed to develop a facile approach using organic solvent extraction for efficiently fractionating the main components of bamboo hydrolysates. The high-purity lignin with only a trace of carbohydrates was first obtained by precipitation of the bamboo hydrolysate. The water-soluble lignin (WSL) fraction was extracted in organic solvent through a three-stage organic solvent extraction process, and the hemicellulosic sugars with increased purity were also collected. Furthermore, a thorough characterization including various NMR techniques (31P, 13C, and 2D-HSQC), GPC, and GC-MS was conducted to the obtained lignin-rich-fractions. It was found that the WSL fraction contained abundant functional groups and tremendous amount of LCC structures. As compared to native LCC of bamboo, the WSL fraction exhibited more typical LCC linkages, i.e. phenyl glycoside linkage, which is the main type of chemical linkage between lignin and carbohydrate in both LCC samples. The results demonstrate that organic phase extraction is a highly efficient protocol for the fractionation of hydrolysate and the isolation of LCC-rich streams possessing great potential applications.

Modelling tyramine extraction from wastewater using a non-dispersive solvent extraction process

2020 ◽  
Vol 27 (31) ◽  
pp. 39068-39076 ◽  
Author(s):  
Mahdi Ghadiri ◽  
Alireza Hemmati ◽  
Ali Taghvaie Nakhjiri ◽  
Saeed Shirazian
Keyword(s):  
Solvent Extraction ◽  
Extraction Process
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