Fabrication and Testing of Planar Stent Mesh Designs Using Carbon-Infiltrated Carbon Nanotubes

Author(s):  
Kristopher Jones ◽  
Brian D. Jensen ◽  
Anton Bowden

This paper explores and demonstrates the potential of using pyrolytic carbon as a material for coronary stents. Stents are commonly fabricated from metal, which has worse biocompatibilty than many polymers and ceramics. Pyrolytic carbon, a ceramic, is currently used in medical implant devices due to its preferable biocompatibility properties. Micropatterned pyrolytic carbon implants can be created by growing carbon nanotubes (CNTs), and then filling the space between with amorphous carbon via chemical vapor deposition (CVD). We prepared multiple samples of two different stent-like flexible mesh designs and smaller cubic structures out of carbon-infiltrated carbon nanotubes (CI-CNT). Tension loads were applied to expand the mesh samples and we recorded the forces at brittle failure. The cubic structures were used for separate compression tests. These data were then used in conjunction with a nonlinear finite element analysis (FEA) model of the stent geometry to determine Young's modulus and maximum fracture strain in tension and compression for each sample. Additionally, images were recorded of the mesh samples before, during, and at failure. These images were used to measure an overall percent elongation for each sample. The highest fracture strain observed was 1.4% and Young's modulus values confirmed that the material was similar to that used in previous carbon-infiltrated carbon nanotube work. The average percent elongation was 86% with a maximum of 145%. This exceeds a typical target of 66%. The material properties found from compression testing show less stiffness than the mesh samples; however, specimen evaluation reveals poorly infiltrated samples.

Author(s):  
Kristopher Jones ◽  
Brian D. Jensen ◽  
Anton Bowden

This paper explores and demonstrates the potential of using pyrolitic carbon as a material for coronary stents. Stents are commonly fabricated from metal, which has worse biocompatibilty than many polymers and ceramics. Pyrolitic carbon, a ceramic, is currently used in medical implant devices due to its preferrable biocompatibility properties. It can be created by growing carbon nanotubes, and then filling the space between with amorpheous carbon via chemical vapor deposition. We prepared multiple samples of two different stent-like flexible geometry designs out of carbon infiltrated carbon nanotubes. Tension loads were applied to expand the samples and we recorded the forces at brittle failure. These data were then used in conjunction with a nonlinear FEA model of the stent geometry to determine Youngs modulus and maximum fracture strain for each sample. Additionally, images were recorded of the samples before, during, and at failure. These images were used to measure an overall percent elongation for each sample. The highest fracture strain observed was 1.4% and Youngs modulus values confirmed the the material was the similar to that used in previous carbon infiltrated carbon nanotube work. The average percent elongation was 86% and reached as high as 145%. This exceeds a typical target of 66%.


2014 ◽  
Vol 23 (1-2) ◽  
pp. 15-19 ◽  
Author(s):  
Khaled A. Alnefaie

AbstractCarbon nanotubes (CNTs) were fabricated using low-pressure chemical vapor deposition and then embedded in epoxy polymer at several weight ratios, 0, 0.75, 1.5, and 3 wt%, for tensile testing and Young’s modulus determination using an Instron machine. The tensile strength and Young’s modulus of the epoxy resin were increased with the addition of CNTs to a certain extent, and then decreased with the increase in the weight fraction of CNTs. The best properties occurred at 1.5 wt% of CNTs. Scanning electron microscopy was used to reveal the dispersion status of CNTs in the nanocomposites.


Author(s):  
Jonathan B. Hopkins ◽  
Lucas A. Shaw ◽  
Todd H. Weisgraber ◽  
George R. Farquar ◽  
Christopher D. Harvey ◽  
...  

The aim of this paper is to introduce an approach for optimally organizing a variety of different unit cell designs within a large lattice such that the bulk behavior of the lattice exhibits a desired Young’s modulus with a graded change in thermal expansion over its geometry. This lattice, called a graded microarchitectured material, can be sandwiched between two other materials with different thermal expansion coefficients to accommodate their different expansions or contractions caused by changing temperature while achieving a desired uniform stiffness. First, this paper provides the theory necessary to calculate the thermal expansion and Young’s modulus of large multi-material lattices that consist of periodic (i.e., repeating) unit cells of the same design. Then it introduces the theory for calculating the graded thermal expansions of a large multimaterial lattice that consists of non-periodic unit cells of different designs. An approach is then provided for optimally designing and organizing different unit cells within a lattice such that both of its ends achieve the same thermal expansion as the two materials between which the lattice is sandwiched. A MATLAB tool is used to generate images of the undeformed and deformed lattices to verify their behavior and various examples are provided as case studies. The theory provided is also verified and validated using finite element analysis and experimentation.


1999 ◽  
Vol 594 ◽  
Author(s):  
T. Y. Zhang ◽  
Y. J. Su ◽  
C. F. Qian ◽  
M. H. Zhao ◽  
L. Q. Chen

AbstractThe present work proposes a novel microbridge testing method to simultaneously evaluate the Young's modulus, residual stress of thin films under small deformation. Theoretic analysis and finite element calculation are conducted on microbridge deformation to provide a closed formula of deflection versus load, considering both substrate deformation and residual stress in the film. Silicon nitride films fabricated by low pressure chemical vapor deposition on silicon substrates are tested to demonstrate the proposed method. The results show that the Young's modulus and residual stress for the annealed silicon nitride film are respectively 202 GPa and 334.9 MPa.


Author(s):  
Alexander E. Stott ◽  
Constantinos Charalambous ◽  
Tristram J. Warren ◽  
William T. Pike ◽  
Robert Myhill ◽  
...  

ABSTRACT The National Aeronautics and Space Administration InSight mission has deployed the seismic experiment, SEIS, on the surface of Mars, and has recorded a variety of signals including marsquakes and dust devils. This work presents results on the tilt and local noise sources, which provide context to aid interpretation of the observed signals and allow an examination of the near-surface properties. Our analysis uses data recorded by the short-period sensors on the deck, throughout deployment and in the final configuration. We use thermal decorrelation to provide an estimate of the sol-to-sol tilt. This tilt is examined across deployment and over a Martian year. After each modification to the site, the tilt is seen to stabilize over 3–20 sols depending on the action, and the total change in tilt is <0.035°. Long-term tilt over a Martian year is limited to <0.007°. We also investigate the attenuation of lander-induced vibrations between the lander and SEIS. Robotic arm motions provide a known lander source in the 5–9 Hz bandwidth, yielding an amplitude attenuation of lander signals between 100 and 1000 times. The attenuation of wind sensitivity from the deck to ground presents a similar value in the 1.5–9 Hz range, thus favoring a noise dominated by lander vibrations induced by the wind. Wind sensitivities outside this bandwidth exhibit different sensitivity changes, indicating a change in the coupling. The results are interpreted through a finite-element analysis of the regolith with a depth-dependent Young’s modulus. We argue that discrepancies between this model and the observations are due to local compaction beneath the lander legs and/or anelasticity. An estimate for the effective Young’s modulus is obtained as 62–81 MPa, corroborating previous estimates for the top layer duricrust.


2013 ◽  
Vol 761 ◽  
pp. 83-86
Author(s):  
Hideaki Sano ◽  
Junichi Morisaki ◽  
Guo Bin Zheng ◽  
Yasuo Uchiyama

Effects of carbon nanotubes (CNT) addition on mechanical properties, electric conductivity and oxidation resistance of CNT/Al2O3-TiC composite were investigated. It was found that flexural strength, Young’s modulus and fracture toughness of the composites were improved by addition of more than 2 vol%-CNT. In the composites with more than 3 vol%-CNT, the oxidation resistance of the composite was degraded. In comparison with Al2O3-26vol%TiC sample as TiC particle-percolated sample, the Al2O3-12vol%TiC-3vol%CNT sample, which is not TiC particle-percolated sample, shows almost the same mechanical properties and electric conductivity, and also shows thinner oxidized region after oxidation at 1200°C due to less TiC in the composite.


2015 ◽  
Vol 83 ◽  
pp. 276-283 ◽  
Author(s):  
L. Pérez ◽  
S. Lascano ◽  
C. Aguilar ◽  
D. Domancic ◽  
I. Alfonso

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