Zamak 2 Alloy Produced by Mechanical Alloying and Consolidated by Sintering and Hot Pressing

Author(s):  
Flávia Costa da Silva ◽  
Kamila Kazmierczak ◽  
César Edil da Costa ◽  
Júlio César Giubilei Milan ◽  
José Manuel Torralba

The Zamak 2 alloy has the best mechanical properties of the Zamak alloys with respect to the tensile strength, creep resistance, and hardness. Zamak 2 is a commercial material widely used for the manufacturing of mechanical components. The presence of Cu in this alloy (3 wt. %) improves the mechanical properties through the formation of E (CuZn4) precipitates. The powder metallurgy (P/M) has an important direct advantage in the fabricated parts with respect to the finished dimensions or near net shaping due to the additional phase stabilization without heat treatment. However, there are few studies into the production of this zinc alloy via mechanical alloying and the effect of the consolidation technique in terms of the material properties; these research deficiencies led to the development of this work. The powder was analyzed during milling until achieving a steady-state, which occurred after 30 h of milling in a planetary ball mill at 400 rpm. The high-energy milling produces a Zamak 2 alloy powder with a T′ stable phase and with a greater melting point. When consolidated using hot pressing, the hardness increases compared to sintering and casting alloy.

2011 ◽  
Vol 43 (3) ◽  
pp. 289-294 ◽  
Author(s):  
J. Zhu ◽  
L. Ye ◽  
F. Wang

A Ti3AlC2/Al2O3 nanocomposite was synthesized using Ti, Al, C and TiO2 as raw materials by a novel combination of high-energy milling and hot pressing. The reaction path of the 3Ti-8C-16Al-9TiO2 mixture of powders was investigated, and the results show that the transitional phases TiC, TixAly and Al2O3 are formed in high-energy milling first, and then TixAly is transformed to the TiAl phase during the hot pressing. Finally, a reaction between TiC and TiAl occurs to produce Ti3AlC2 and the nanosized Ti3AlC2/Al2O3 composite is synthesized. The Ti3AlC2/Al2O3 composite possessed a good combination of mechanical properties with a hardness of 6.0 GPa, a flexural strength of 600 MPa, and a fracture toughness (K1C) of 5.8 MPa?m1/2. The strengthening and toughening mechanisms were also discussed.


2015 ◽  
Vol 60 (2) ◽  
pp. 1523-1527 ◽  
Author(s):  
M. Suśniak ◽  
J. Karwan-Baczewska ◽  
J. Dutkiewicz ◽  
M. Actis Grande ◽  
M. Rosso

Abstract The present work investigates the possibility of using powder metallurgy processing for producing a metal matrix composite. Materials were prepared from AlSi5Cu2 chips with reinforcement of 10, 15, 20 wt. % silicon carbide. Aluminum alloy chips were milled with SiC powder in a high-energy ball mill by 40 hours. Mechanical alloying process lead to obtain an uniform distribution of hard SiC particles in the metallic matrix and refine the grain size. The consolidation of composite powders was performed by vacuum hot pressing at 450°C, under pressure of 600 MPa by 10 min. The results shows that the addition of SiC particles has a substantial influence on the microstructure and mechanical properties of composite powder as well as consolidated material. Hot pressing is an effective consolidation method which leads to obtain dense AlSi5Cu2/SiC composite with homogeneous structure and advanced mechanical properties.


2014 ◽  
Vol 217-218 ◽  
pp. 347-354 ◽  
Author(s):  
Jokin Lozares ◽  
Zigor Azpilgain ◽  
Iñaki Hurtado ◽  
Iñigo Loizaga

Due to the current trend in prices of raw material and their sources, near net shaping of mechanical components will become a key factor for the companies to get the desired competitiveness. Semisolid metal (SSM) forming is one of those near net shape forming techniques revealing a high potential to reduce material as well as energy consumption compared to conventional process technologies. Thus, the aim of this research work is to demonstrate the above by manufacturing a steel commercial automotive spindle by thixo-lateral forming from three different steel grades. The starting material, the microstructure and mechanical properties are analysed along the article. Material savings of 20% have been reported together with a substantial decrease of the forming forces. In addition, great mechanical properties have been achieved which brings the process closer to the desired final industrial application.


2012 ◽  
Vol 1456 ◽  
Author(s):  
Tsung-ta E. Chan ◽  
Rama Venkatasubramanian ◽  
James M. LeBeau ◽  
Peter Thomas ◽  
Judy Stuart ◽  
...  

ABSTRACTNanocomposite Bi2Te3 based alloys are attractive for their potentially high thermoelectric figure-of-merit (ZT) around room temperature. The nano-scale structural features embedded in the matrix provide more scattering of phonons and can thus reduce the lattice thermal conductivity. To further take advantage of such nanocomposite structures, we focus on the development of nanocrystalline Bi(Sb)Te(Se) powders by high energy cryogenic mechanical alloying followed by an optimized hot pressing process. This approach is shown to successfully produce Bi(Sb)Te(Se) alloy powders with grain size averaging about 9 nm for n-type BiTe(Se) and about 16 nm for p-type Bi(Sb)Te respectively. This cryogenic process offers much less milling time and prevents thermally activated contamination or imperfections from being introduced during the milling process. The nanocrystalline powders are then compacted at optimized pressures and temperatures to achieve full density compactions and preserve the grain sizes effectively. The resulting nano-bulk materials have optimal Seebeck coefficients and are expected to have improved ZT. Thermoelectric properties and microstructure studies by X-ray diffraction and transmission electron microscopy will also be presented and discussed.


Metals ◽  
2020 ◽  
Vol 10 (9) ◽  
pp. 1144
Author(s):  
Dora Janovszky

High-density Al-based composites reinforced with ten-wt.% recycled nanocrystalline CuZrAgAl particles have been fabricated by mechanical milling, cold- and hot-pressing. The microstructures, phase transformations, and mechanical properties of the mixed powder and sintered samples were investigated. After milling in a ball mill for 30 h, the microhardness of the mixed powder increases to 301 ± 31 HV0.01 and 222 ± 10 HV0.01 without and with ethanol milling, respectively. On account of the interdiffusion, the melting temperature of mixed powder reduces to 574 ± 5.0 °C and 627.5 ± 6.5 °C after 30 h milling. The study showed that the reinforcing particles are homogeneously distributed in the sintered nanocrystalline Al-based composites. During the hot-pressing, a shell zone forms at the interface of reinforcing particles during hot pressing after high energy milling with a minimum of ten hours milling time. This shell zone consists of Al3Zr (D023) phase. The coarsening resistant core-shell structure and grain refinement greatly improve mechanical properties. The compression strength at room temperature varies between 650 and 800 MPa at room temperature and is 380 MPa at 400 °C for the composite containing ten-wt.% of the Cu-Zr-based amorphous-nanocrystalline phases. The Brinell hardness of the sintered composite is 329 HB.


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