Electron Backscatter Diffraction-Enabled Anisotropic Thermo-Elastic Analysis of Additively Manufactured Single Tracks

Author(s):  
Andrew J. Birnbaum ◽  
John G. Michopoulos ◽  
John C. Steuben ◽  
Athanasios P. Iliopoulos

Abstract Despite extensive efforts directed toward elucidating the connections between process, microstructure and performance of additively manufactured structures and components, a significant number of meaningful questions remain unanswered. Specifically, a large body of work has demonstrated that microstructural/sub-structural features in selectively laser melted (SLM) components give rise to a significant enhancement in strength. Furthermore, the change in associated ductility is comparable to that seen in post-processed, wrought annealed material. However, the origin and mechanism by which these features arise have remained elusive. This work is an initial step in leveraging computational capabilities for validating experiment-based theories that explain the basis for the above-mentioned phenomena. The present work describes a computational approach for utilizing spatially resolved crystal-lographic descriptions obtained via electron backscatter diffraction (EBSD) to define the domain geometry and material properties of an anisotropic thermo-elastic simulation. The resulting solution is used to ascertain the elastic strain energy state, and slip-system resolved shear stresses on a per-grain basis. This analysis is performed, in part, as a means for validating a hypothesis linking these characteristics with the development of sub-structural features, which are in turn, correlated with improvements in material performance. The results suggest that both strain energy density and grain boundary character play an important role in the formation of substructure in additively manufactured 316L stainless steels.

2019 ◽  
Vol 9 (1) ◽  
Author(s):  
Fabian Pöhl

Abstract This study analyzes the elastic-to-plastic transition during nanoindentation of polycrystalline iron. We conduct nanoindentation (Berkovich indenter) experiments and electron backscatter diffraction analysis to investigate the initiation of plasticity by the appearance of the pop-in phenomenon in the loading curves. Numerous load–displacement curves are statistically analyzed to identify the occurrence of pop-ins. A first pop-in can result from plasticity initiation caused by homogeneous dislocation nucleation and requires shear stresses in the range of the theoretical strength of a defect-free iron crystal. The results also show that plasticity initiation in volumes with preexisting dislocations is significantly affected by small amounts of interstitially dissolved atoms (such as carbon) that are segregated into the stress fields of dislocations, impeding their mobility. Another strong influence on the pop-in behavior is grain boundaries, which can lead to large pop-ins at relatively high indentation loads. The pop-in behavior appears to be a statistical process affected by interstitial atoms, dislocation density, grain boundaries, and surface roughness. No effect of the crystallographic orientation on the pop-in behavior can be observed.


2004 ◽  
Vol 467-470 ◽  
pp. 1243-1250 ◽  
Author(s):  
John Wheeler ◽  
Zhenting Jiang ◽  
David J. Prior ◽  
Jan Tullis

It is generally agreed that the driving force (plastic strain energy) is much too small to allow "classical" nucleation during static and dynamic recrystallisation, and that rotation/growth of subgrains is an alternative. The latter explanation predicts that new grains should begin at low angles to old grains. We have used electron backscatter diffraction on an experimentally deformed quartz polycrystal that has deformed by dislocation creep and partially recrystallised. In a region shortened by about 30% new grains are at high angles (much greater than 15º) to adjacent parent grains. A histogram of misorientation versus number of boundaries shows a gap at 15-20º. In its simple form we expect the subgrain rotation model to predict a spectrum of misorientations but with most of them being low angle. Instead, the histogram suggests that new boundaries began life as high-angle structures, so current models for deformation-induced nucleation require refinement.


Author(s):  
Frank Altmann ◽  
Jens Beyersdorfer ◽  
Jan Schischka ◽  
Michael Krause ◽  
German Franz ◽  
...  

Abstract In this paper the new Vion™ Plasma-FIB system, developed by FEI, is evaluated for cross sectioning of Cu filled Through Silicon Via (TSV) interconnects. The aim of the study presented in this paper is to evaluate and optimise different Plasma-FIB (P-FIB) milling strategies in terms of performance and cross section surface quality. The sufficient preservation of microstructures within cross sections is crucial for subsequent Electron Backscatter Diffraction (EBSD) grain structure analyses and a high resolution interface characterisation by TEM.


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