Mechanical Property Characterization of Additive Manufactured ABS Material Using Design of Experiment Approach

Author(s):  
Adugna D. Akessa ◽  
Hirpa G. Lemu ◽  
Aboma W. Gebisa

Additive manufacturing technology is a process of joining materials to make objects from 3D model data, usually layer upon layer, contrary to conventional manufacturing technologies, which mostly use subtractive process. The technology has developed from the earlier days of rapid prototyping to sophisticated rapid manufacturing in the last 20 years and can create parts directly from CAD model without the use of tooling. This technology is predicted to revolutionize many sectors of manufacturing by reducing component lead-time, material waste, energy usage, etc. Though there is significant progress in the field, there are still a number of challenges including characterization of mechanical properties. This paper presents a study conducted to characterize the mechanical properties of ABS-M30 materials whose specimens are fabricated using different printing parameters. To understand the mechanical properties, it is vital to study the effects of the printing parameters on 3D printed parts. For this purpose, Design of Experiment (DOE) is used. The printing parameters of the machine (Fortus 450mc Fused Deposition Modeling (FDM) machine) such as raster orientation, air gap, and raster width, were examined to test Tensile strengths and 3-point bend strength of the tested specimens. The study shows that, raster orientation and air gap has more effect on mechanical properties of ABS-M30 products where raster width has less effect.

2020 ◽  
Author(s):  
Muhammad Salman Mustafa ◽  
Muhammad Qasim Zafar ◽  
Muhammad Arslan Muneer ◽  
Muhammad Arif ◽  
Farrukh Arsalan Siddiqui ◽  
...  

Abstract Fused Deposition Modeling (FDM) is a widely adopted additive manufacturing process to produce complex 3D structures and it is typically used in the fabrication of biodegradable materials e.g. PLA/PHA for biomedical applications. However, FDM as a fabrication process for such material needs to be optimized to enhance mechanical properties. In this study, dogbone and notched samples are printed with the FDM process to determine optimum values of printing parameters for superior mechanical properties. The effect of layer thickness, infill density, and print bed temperature on mechanical properties is investigated by applying response surface methodology (RSM). Optimum printing parameters are identified for tensile and impact strength and an empirical relation has been formulated with response surface methodology (RSM). Furthermore, the analysis of variance (ANOVA) was performed on the experimental results to determine the influence of the process parameters and their interactions. ANOVA results demonstrate that 44.7% infill density, 0.44 mm layer thickness, and 20C° printing temperatures are the optimum values of printing parameters owing to improved tensile and impact strength respectively. The experimental results were found in strong agreement with the predicted theoretical results.


2019 ◽  
Vol 16 (2) ◽  
pp. 25-31 ◽  
Author(s):  
Jessica Zuleima Parrado-Agudelo ◽  
Carlos Narváez-Tovar

This study aims to determine the mechanical properties of parts manufactured by Fused Deposition Modeling (FDM) using three biocompatible polymer materials: Polylactic Acid (PLA), Polycaprolactone (PCL) and Lay-Fomm 40. Also, it was analyzed the influence of different printing parameters, material selection, infill percentage, and raster angle, over the mechanical properties. The samples were subjected to tension and compression tests using a universal testing machine, and elastic modulus, yield stress, and ultimate stress were obtained from the stress-strain curves. PLA samples have the highest elastic modulus, yield stress and ultimate stress for both compression and tension tests, for example, the ultimate tensile stress with infill percentage of 30 % and raster angle of 0-90° has an average value of 41.20 MPa, while PCL samples had an ultimate tensile stress average value of 9.68 MPa. On the other hand, Lay-Fomm40 samples had the highest elongations, with percentage values between 300 and 600 %. Finally, ANOVA analysis showed that the choice of the material is the leading printing parameter that contributes to the mechanical properties, with percentages of 84.20% to elastic modulus, 93.30% to yield stress, and 82.44% to ultimate stress. The second important factor is the raster angle, with higher strengths for the 0-90° when compared to 45-135°. On the other hand, the contribution of the infill percentage to the mechanical properties was no statistically significant. The obtained results could be useful for material selection and 3D printing parameters definition for additive manufacturing of scaffolds, implants, and other structures for biomedical and tissue engineering applications.


Materials ◽  
2018 ◽  
Vol 11 (12) ◽  
pp. 2540 ◽  
Author(s):  
José Linares-Alvelais ◽  
J. Figueroa-Cavazos ◽  
C. Chuck-Hernandez ◽  
Hector Siller ◽  
Ciro Rodríguez ◽  
...  

In this work, we assess the effects of sterilization in materials manufactured using additive manufacturing by employing a sterilization technique used in the food industry. To estimate the feasibility of the hydrostatic high-pressure (HHP) sterilization of biomedical devices, we have evaluated the mechanical properties of specimens produced by commercial 3D printers. Evaluations of the potential advantages and drawbacks of Fused Deposition Modeling (FDM), Digital Light Processing (DLP) technology, and Stereolithography (SLA) were considered for this study due to their widespread availability. Changes in mechanical properties due to the proposed sterilization technique were compared to values derived from the standardized autoclaving methodology. Enhancement of the mechanical properties of samples treated with Hydrostatic high-pressure processing enhanced mechanical properties, with a 30.30% increase in the tensile modulus and a 26.36% increase in the ultimate tensile strength. While traditional autoclaving was shown to systematically reduce the mechanical properties of the materials employed and damages and deformation on the surfaces were observed, HHP offered an alternative for sterilization without employing heat. These results suggest that while forgoing high-temperature for sanitization, HHP processing can be employed to take advantage of the flexibility of additive manufacturing technologies for manufacturing implants, instruments, and other devices.


Polymers ◽  
2021 ◽  
Vol 13 (11) ◽  
pp. 1758
Author(s):  
Ming-Hsien Hsueh ◽  
Chao-Jung Lai ◽  
Shi-Hao Wang ◽  
Yu-Shan Zeng ◽  
Chia-Hsin Hsieh ◽  
...  

Fused Deposition Modeling (FDM) can be used to manufacture any complex geometry and internal structures, and it has been widely applied in many industries, such as the biomedical, manufacturing, aerospace, automobile, industrial, and building industries. The purpose of this research is to characterize the polylactic acid (PLA) and polyethylene terephthalate glycol (PETG) materials of FDM under four loading conditions (tension, compression, bending, and thermal deformation), in order to obtain data regarding different printing temperatures and speeds. The results indicated that PLA and PETG materials exhibit an obvious tensile and compression asymmetry. It was observed that the mechanical properties (tension, compression, and bending) of PLA and PETG are increased at higher printing temperatures, and that the effect of speed on PLA and PETG shows different results. In addition, the mechanical properties of PLA are greater than those of PETG, but the thermal deformation is the opposite. The above results will be a great help for researchers who are working with polymers and FDM technology to achieve sustainability.


Author(s):  
M Corsi ◽  
S Bagassi ◽  
MC Moruzzi ◽  
L Seccia

Fused Deposition Modeling (FDM), is one of the most popular and widely used Additive Manufacturing filament based technology employing materials such as Acrylonitrile Butadiene Styrene (ABS), Polycarbonate (PC), Thermoplastic Polyurethane (TPU) and Polylactic Acid (PLA). In this technique, the part is built up layer-by-layer, affecting, both the resolution along the z-axis, and the mechanical properties dependent on the mesostructure, controlled by a large amount of production parameters such as layer thickness, raster orientation, number of contour and air gap. When dealing with functional and structural printed parts, a deep understanding of these tunable building parameters and their influence on the mechanical properties is of the utmost importance and over the years many experimental studies have been carried to investigate this need. This study is intended to explore specimens realized through FDM technique with different combinations of printing parameters to analyse their effect on the mechanical properties of ABS Plus p430. To this aim, tensile and compression specimens, had been designed and tested. Sixteen different types of tensile specimen had been realized by varying four different parameters, namely, layer thickness, part interior style, infill orientation and number of contours. Whereas, the number of compression specimens had been limited to four considering the variation of two parameters: layer thickness and part interior style. Three samples for each specimen had been produced in ABS Plus p430 using a Stratasys Fortus 250mc FDM printer and tested with a universal testing machine through tension and compression tests to analyse the correlation between printing parameters and material properties. Test results had led to important conclusions on the consistency and homogeneity of the mechanical properties and on the variation of the material’s performances in accordance with the different combinations of production parameters.


Author(s):  
Abigail Chaffins ◽  
Mohan Yu ◽  
Pier Paolo Claudio ◽  
James B. Day ◽  
Roozbeh (Ross) Salary

Abstract Fused deposition modeling (FDM), is a direct-write material extrusion additive manufacturing process, which has emerged as a method of choice for the fabrication of a wide range of biological tissues and structures. FDM allows for non-contact, multi-material deposition of a broad spectrum of functional materials for tissue engineering applications. However, the FDM process is intrinsically complex, consisting of a multitude of parameters as well as material-machine interactions, which may adversely influence the mechanical properties, the surface morphology, and ultimately the functional integrity of fabricated bone scaffolds. Hence, process optimization in addition to physics-based characterization of the FDM process would be inevitably a need. The overarching goal of this research work is to fabricate biocompatible, porous bone scaffolds, incorporating autologous human bone marrow mesenchymal stem cells (hBMSCs), for the treatment of osseous fractures, defects, and eventually diseases. The objective of this work is to investigate the mechanical properties of several triply periodic minimal surface (TPMS) bone scaffolds, fabricated using fused deposition modeling (FDM) additive manufacturing process. In this study, biocompatible TPMS bone scaffolds were FDM-deposited, based on a medical-grade polymer composite, composed of polyamide, polyolefin, and cellulose fibers (named PAPC-II). In addition, the experimental characterization of the TPMS bone scaffolds was on the basis of a single factor experiment. The compression properties of the fabricated bone scaffolds were measured using a compression testing machine. Furthermore, a digital image processing program was developed in the MATLAB environment to characterize the morphological properties of the fabricated bone scaffolds.


2020 ◽  
Vol 22 (4) ◽  
pp. 895-908
Author(s):  
M. Ouhsti ◽  
B. El Haddadi ◽  
S. Belhouideg

Abstract3D polymer-based printers have become easily accessible to the public. Usually, the technology used by these 3D printers is Fused Deposition Modelling (FDM). The majority of these 3D printers mainly use acrylonitrile butadiene styrene (ABS) and polylactic acid (PLA) to fabricate 3D objects. In order for the printed parts to be useful for specific applications, the mechanical properties of the printed parts must be known. The aim of this study is to determine the tensile strength and elastic modulus of printed materials in polylactic acid (PLA) according to three important printing parameters such as deposition angle, extruder temperature and printing speed. The central composite design (CCD) was used to reduce the number of tensile test experiments. The obtained results show that the mechanical properties of printed parts depend on printing parameters. Empirical models relating response and process parameters are developed. The analysis of variance (ANOVA) was used to test the validity of models relating response and printing parameters. The optimal printing parameters are determined for the desired mechanical properties.


2016 ◽  
Vol 22 (2) ◽  
pp. 387-404 ◽  
Author(s):  
Jonathan Torres ◽  
Matthew Cole ◽  
Allen Owji ◽  
Zachary DeMastry ◽  
Ali P. Gordon

Purpose This paper aims to present the influences of several production variables on the mechanical properties of specimens manufactured using fused deposition modeling (FDM) with polylactic acid (PLA) as a media and relate the practical and experimental implications of these as related to stiffness, strength, ductility and generalized loading. Design/methodology/approach A two-factor-level Taguchi test matrix was defined to allow streamlined mechanical testing of several different fabrication settings using a reduced array of experiments. Specimens were manufactured and tested according to ASTM E8/D638 and E399/D5045 standards for tensile and fracture testing. After initial analysis of mechanical properties derived from mechanical tests, analysis of variance was used to infer optimized production variables for general use and for application/load-specific instances. Findings Production variables are determined to yield optimized mechanical properties under tensile and fracture-type loading as related to orientation of loading and fabrication. Practical implications The relation of production variables and their interactions and the manner in which they influence mechanical properties provide insight to the feasibility of using FDM for rapid manufacturing of components for experimental, commercial or consumer-level use. Originality/value This paper is the first report of research on the characterization of the mechanical properties of PLA coupons manufactured using FDM by the Taguchi method. The investigation is relevant both in commercial and consumer-level aspects, given both the currently increasing utilization of 3D printers for component production and the viability of PLA as a renewable, biocompatible material for use in structural applications.


2019 ◽  
Vol 25 (7) ◽  
pp. 1145-1154 ◽  
Author(s):  
Xia Gao ◽  
Daijun Zhang ◽  
Xiangning Wen ◽  
Shunxin Qi ◽  
Yunlan Su ◽  
...  

Purpose This work aims to develop a new kind of semicrystalline polymer filament and optimize its printing parameters in the fused deposition modeling process. The purpose of this work also includes producing FDM parts with good ductility. Design/methodology/approach A new kind of semicrystalline filaments composed of long-chain polyamide (PA)1012 was prepared by controlling screw speed and pulling speed carefully. The optimal printing parameters for PA1012 filaments were explored through investigating dimensional accuracy and bonding strength of FDM parts. Furthermore, the mechanical properties of PA1012 specimens were also evaluated by varying nozzle temperatures and raster angles. Findings It is found that PA1012 filaments can accommodate for FDM process under suitable printing parameters. The print quality and mechanical properties of FDM parts highly depend on nozzle temperature and bed temperature. Even though higher temperatures facilitate stronger interlayer bonding, FDM parts with excellent tensile strength were obtained at a moderate nozzle temperature. Moreover, a bed temperature well above the glass transition temperature of PA1012 can eliminate shrinkage and distortion of FDM parts. As expected, FDM parts prepared with PA1012 filaments exhibit good ductility. Originality/value Results in this work demonstrate that the PA1012 filament allows the production of FDM parts with desired mechanical performance. This indicates the potential for overcoming the dependence on amorphous thermoplastics as a feedstock in the FDM technique. This work also provides insight into the effect of materials properties on the mechanical performance of FDM-printed parts.


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