STRUCTURE, KINEMATICS, AND STRAIN PARTITIONING OF AN EXHUMED HIGH PRESSURE TERRAIN: THE ROAN WINDOW, NORWAY

2019 ◽  
Author(s):  
Christine E. Newville ◽  
◽  
Christian Teyssier ◽  
Donna L. Whitney ◽  
Hannah J. Blatchford
Solid Earth ◽  
2017 ◽  
Vol 8 (4) ◽  
pp. 751-765 ◽  
Author(s):  
Alejandra Quintanilla-Terminel ◽  
Mark E. Zimmerman ◽  
Brian Evans ◽  
David L. Kohlstedt

Abstract. Usually several deformation mechanisms interact to accommodate plastic deformation. Quantifying the contribution of each to the total strain is necessary to bridge the gaps from observations of microstructures, to geomechanical descriptions, to extrapolating from laboratory data to field observations. Here, we describe the experimental and computational techniques involved in microscale strain mapping (MSSM), which allows strain produced during high-pressure, high-temperature deformation experiments to be tracked with high resolution. MSSM relies on the analysis of the relative displacement of initially regularly spaced markers after deformation. We present two lithography techniques used to pattern rock substrates at different scales: photolithography and electron-beam lithography. Further, we discuss the challenges of applying the MSSM technique to samples used in high-temperature and high-pressure experiments. We applied the MSSM technique to a study of strain partitioning during creep of Carrara marble and grain boundary sliding in San Carlos olivine, synthetic forsterite, and Solnhofen limestone at a confining pressure, Pc, of 300 MPa and homologous temperatures, T∕Tm, of 0.3 to 0.6. The MSSM technique works very well up to temperatures of 700 °C. The experimental developments described here show promising results for higher-temperature applications.


2020 ◽  
Author(s):  
Francesco Giuntoli ◽  
Giulio Viola

<p>Exhumation of subducted high-pressure units is favoured by relatively narrow, high-strain shear zones, where most metamorphic and deformational processes occur. Unfortunately, these are commonly overprinted and/or partly or fully obliterated along the exhumation path by younger fabrics or by metamorphic re-equilibration. Their identification and characterization are, therefore, of primary importance when aiming at reconstructing the deepest (and thus earliest) tectonometamorphic history of high-pressure crustal units.</p><p>The Northern Apennines (Italy) offer the opportunity to study a unique setting where continental units (Tuscan Metamorphic Units) were subducted to high-pressure conditions and then exhumed and juxtaposed against non-metamorphic units (Tuscan Nappe). We have studied a well exposed section in the Monticiano-Roccastrada Unit of the Mid Tuscan Ridge (MTR), where a mesoscopic (~20 m length and 5 m high) compressional duplex deforms the Palaeozoic-Triassic quartz-rich metasandstones, metaconglomerates and minor metapelites of the Monte Quoio - Montagnola Senese Unit with a top-to-the-NE sense of shear (Arenarie di Poggio al Carpino Formation; Casini et al., 2007).</p><p>Our approach is based on detailed fieldwork, microstructural and petrological investigations. Field observations reveal severe strain partitioning within the duplex between metapelite levels, corresponding to 10-50 cm thick high-strain zones, and metasandstone levels, which form relatively strain-free metric horses. Early generations of quartz veins are highly transposed (sheath folds occur) parallel to the metapelitic high-strain shear zones. Veins are composed of iso-oriented quartz, forming up to several centimetre long single-grain ribbons, Mg-carpholite (XMg~ 0.65) needles and K-white mica marking the stretching lineation. Carpholite in the transposed veins invariably defines the stretching direction of shear zones. These high-P veins coexist with a later generation of less deformed, oblique quartz veins. The mylonitic foliation in the metapelites is defined by quartz, chloritoid, pyrophyllite and K-white mica forming a stretching lineation coherent with the one visible in the veins. Geometrical, cross-cutting and petrographic relations suggest that there has occurred cyclic deformation between brittle and viscous conditions, with the veins forming broadly syn-mylonitic shearing. Thermodynamic modeling results suggest >0.8 GPa and ~350°C for the formation of both the high-pressure veins and the mylonitic foliation.</p><p>Shear zones were subsequently folded about the NNW-SSE axis of the regional antiform associated with the MTR. Later brittle overprinting is represented by quart-filled tension gashes and localized C’ planes, mostly within the more competent metasandstone levels, indicating top-to-the-SW reactivation. In summary, our results suggest a cyclic brittle-ductile behaviour occurring at high pressure conditions. This could potentially reflect the repeated alternation between aseismic creep (viscous) and coseismic slip (brittle) during the first stages of the exhumation history of this portion of the northern Apennines, from lower to middle crustal levels in a compressional top-to-the-NE setting. Dating of K-white mica is ongoing to constrain the geodynamic scenario of such shear zone.</p><p> </p><p>Casini, G., Decandia, F.A., Tavarnelli, E., 2007. Analysis of a mesoscopic duplex in SW Tuscany, Italy: implications for thrust system development during positive tectonic inversion. Geol. Soc. London, Spec. Publ. 272, 437–446.</p><p> </p>


Minerals ◽  
2019 ◽  
Vol 9 (11) ◽  
pp. 679 ◽  
Author(s):  
Lin ◽  
Giannetta ◽  
Jugle ◽  
Couper ◽  
Dunleavy ◽  
...  

Keywords: multiphase deformation; high pressure; texture; plasticity modeling


Author(s):  
Marek Malecki ◽  
James Pawley ◽  
Hans Ris

The ultrastructure of cells suspended in physiological fluids or cell culture media can only be studied if the living processes are stopped while the cells remain in suspension. Attachment of living cells to carrier surfaces to facilitate further processing for electron microscopy produces a rapid reorganization of cell structure eradicating most traces of the structures present when the cells were in suspension. The structure of cells in suspension can be immobilized by either chemical fixation or, much faster, by rapid freezing (cryo-immobilization). The fixation speed is particularly important in studies of cell surface reorganization over time. High pressure freezing provides conditions where specimens up to 500μm thick can be frozen in milliseconds without ice crystal damage. This volume is sufficient for cells to remain in suspension until frozen. However, special procedures are needed to assure that the unattached cells are not lost during subsequent processing for LVSEM or HVEM using freeze-substitution or freeze drying. We recently developed such a procedure.


Author(s):  
Robert Corbett ◽  
Delbert E. Philpott ◽  
Sam Black

Observation of subtle or early signs of change in spaceflight induced alterations on living systems require precise methods of sampling. In-flight analysis would be preferable but constraints of time, equipment, personnel and cost dictate the necessity for prolonged storage before retrieval. Because of this, various tissues have been stored in fixatives and combinations of fixatives and observed at various time intervals. High pressure and the effect of buffer alone have also been tried.Of the various tissues embedded, muscle, cartilage and liver, liver has been the most extensively studied because it contains large numbers of organelles common to all tissues (Fig. 1).


Author(s):  
R.E. Crang ◽  
M. Mueller ◽  
K. Zierold

Obtaining frozen-hydrated sections of plant tissues for electron microscopy and microanalysis has been considered difficult, if not impossible, due primarily to the considerable depth of effective freezing in the tissues which would be required. The greatest depth of vitreous freezing is generally considered to be only 15-20 μm in animal specimens. Plant cells are often much larger in diameter and, if several cells are required to be intact, ice crystal damage can be expected to be so severe as to prevent successful cryoultramicrotomy. The very nature of cell walls, intercellular air spaces, irregular topography, and large vacuoles often make it impractical to use immersion, metal-mirror, or jet freezing techniques for botanical material.However, it has been proposed that high-pressure freezing (HPF) may offer an alternative to the more conventional freezing techniques, inasmuch as non-cryoprotected specimens may be frozen in a vitreous, or near-vitreous state, to a radial depth of at least 0.5 mm.


Author(s):  
William P. Sharp ◽  
Robert W. Roberson

The aim of ultrastructural investigation is to analyze cell architecture and relate a functional role(s) to cell components. It is known that aqueous chemical fixation requires seconds to minutes to penetrate and stabilize cell structure which may result in structural artifacts. The use of ultralow temperatures to fix and prepare specimens, however, leads to a much improved preservation of the cell’s living state. A critical limitation of conventional cryofixation methods (i.e., propane-jet freezing, cold-metal slamming, plunge-freezing) is that only a 10 to 40 μm thick surface layer of cells can be frozen without distorting ice crystal formation. This problem can be allayed by freezing samples under about 2100 bar of hydrostatic pressure which suppresses the formation of ice nuclei and their rate of growth. Thus, 0.6 mm thick samples with a total volume of 1 mm3 can be frozen without ice crystal damage. The purpose of this study is to describe the cellular details and identify potential artifacts in root tissue of barley (Hordeum vulgari L.) and leaf tissue of brome grass (Bromus mollis L.) fixed and prepared by high-pressure freezing (HPF) and freeze substitution (FS) techniques.


Author(s):  
E. F. Koch

Because of the extremely rigid lattice structure of diamond, generating new dislocations or moving existing dislocations in diamond by applying mechanical stress at ambient temperature is very difficult. Analysis of portions of diamonds deformed under bending stress at elevated temperature has shown that diamond deforms plastically under suitable conditions and that its primary slip systems are on the ﹛111﹜ planes. Plastic deformation in diamond is more commonly observed during the high temperature - high pressure sintering process used to make diamond compacts. The pressure and temperature conditions in the sintering presses are sufficiently high that many diamond grains in the sintered compact show deformed microtructures.In this report commercially available polycrystalline diamond discs for rock cutting applications were analyzed to study the deformation substructures in the diamond grains using transmission electron microscopy. An individual diamond particle can be plastically deformed in a high pressure apparatus at high temperature, but it is nearly impossible to prepare such a particle for TEM observation, since any medium in which the diamond is mounted wears away faster than the diamond during ion milling and the diamond is lost.


Author(s):  
Peter Pegler ◽  
N. David Theodore ◽  
Ming Pan

High-pressure oxidation of silicon (HIPOX) is one of various techniques used for electrical-isolation of semiconductor-devices on silicon substrates. Other techniques have included local-oxidation of silicon (LOCOS), poly-buffered LOCOS, deep-trench isolation and separation of silicon by implanted oxygen (SIMOX). Reliable use of HIPOX for device-isolation requires an understanding of the behavior of the materials and structures being used and their interactions under different processing conditions. The effect of HIPOX-related stresses in the structures is of interest because structuraldefects, if formed, could electrically degrade devices.This investigation was performed to study the origin and behavior of defects in recessed HIPOX (RHIPOX) structures. The structures were exposed to a boron implant. Samples consisted of (i) RHlPOX'ed strip exposed to a boron implant, (ii) recessed strip prior to HIPOX, but exposed to a boron implant, (iii) test-pad prior to HIPOX, (iv) HIPOX'ed region away from R-HIPOX edge. Cross-section TEM specimens were prepared in the <110> substrate-geometry.


Author(s):  
Robert W. Roberson

The use of cryo-techniques for the preparation of biological specimens in electron microscopy has led to superior preservation of ultrastructural detail. Although these techniques have obvious advantages, a critical limitation is that only 10-40 μm thick cells and tissue layers can be frozen without the formation of distorting ice crystals. However, thicker samples (600 μm) may be frozen well by rapid freezing under high-pressure (2,100 bar). To date, most work using cryo-techniques on fungi have been confined to examining small, thin-walled structures. High-pressure freezing and freeze substitution are used here to analysis pre-germination stages of specialized, sexual spores (teliospores) of the plant pathogenic fungus Gymnosporangium clavipes C & P.Dormant teliospores were incubated in drops of water at room temperature (25°C) to break dormancy and stimulate germination. Spores were collected at approximately 30 min intervals after hydration so that early cytological changes associated with spore germination could be monitored. Prior to high-pressure freezing, the samples were incubated for 5-10 min in a 20% dextran solution for added cryoprotection during freezing. Forty to 50 spores were placed in specimen cups and holders and immediately frozen at high pressure using the Balzers HPM 010 apparatus.


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