Expansion of Nanosized MgSiO3/Chitosan Nanocomposite Structural and Spectroscopic for Loading Velosef by Nanomaterial Intervention

2021 ◽  
Author(s):  
amal aboelnaga ◽  
talaat Meaz ◽  
amany M elnahrawy
Keyword(s):  
Antimicrobial Activity ◽  
High Performance ◽  
Sol Gel ◽  
Polymerization Process ◽  
Absorption Bands ◽  
Structural Morphology ◽  
Crystallinity Degree ◽  
Chitosan Matrix ◽  
Antimicrobial Studies ◽  
Sol Gel Process

Abstract The aim of this study is to investigate the effect of different doses of Velosef in magnesium silica/chitosan nanocomposite in terms of structural, morphology, optical properties, and bioactivity. Loading Velosef in fine-sized magnesium silica/chitosan is an efficient engineering approach for drug delivery. The sol-gel process was used to prepare magnesium silica fine-sized before being blended into chitosan matrix, which acts as a potential morphogenetic biomaterial. The Velosef/magnesium silica/chitosan nanocomposites were characterized by XRD, TEM, SEM, FTIR, UV-absorption, and antimicrobial studies. The XRD was characteristic of the crystallinity degree of the MgO-SiO2/chitosan/Velosef nanocomposites with three maximum peaks at 26.37°, 33.34o, 36.9°. FTIR results indicated the structural change occurred with the Velosef sol-gel polymerization process. UV-absorbance reveals that the MgO-SiO2/chitosan nanocomposite appeared a high performance for loading Velosef at two absorption bands at 253 and 347 nm. The MgO-SiO2/Chitosan/Velosef nanocomposites showed considerable antimicrobial activity in opposition to the tested representative microorganisms. The maximum antimicrobial activity was obtained with MgO-SiO2/Chitosan against both Escherichia coli and Candida albicans (37 mm), while the minimum antimicrobial activity (30 mm) was recorded against B. mycoides and E. coli with control.

scholarly journals Synthesis of ZnO and CuO nanoparticles via Sol gel method and Its Characterization by using XRD and FT-IR Analysis

2022 ◽  
Author(s):  
Monika Patel ◽  
Sunita Mishra ◽  
Ruchi Verma ◽  
Deep Shikha
Keyword(s):  
Particle Size ◽  
Zno Nanoparticles ◽  
Sol Gel ◽  
Broad Band ◽  
Zinc Nitrate ◽  
Zno Nanoparticle ◽  
Absorption Bands ◽  
Characteristic Absorption ◽  
Sol Gel Process ◽  
Ft Ir

Abstract Nanotechnology is a completely unique branch of technology that offers with substances in a very small size between (1-100 nm) with various crystal shapes which include spherical nanoparticles, flower shaped, Nano rods, Nano ribbons, and Nano platelets. Metals have ability to produce large number of oxides. These metal oxides play an major role in many areas of chemistry, physics, material science and food science. In this research, Zinc Oxide (ZnO) and Copper (II) oxide nanoparticles were synthesized via sol-gel process using zinc nitrate and copper (II) nitrate as precursor respectively. The characterization of CuO and ZnO nanoparticles was done by using various techniques. X-ray Diffraction (XRD) indicates the crystallinity and crystal size of CuO and ZnO nanoparticle. Fourier transform infrared spectroscopy (FT-IR) was used to get the infrared spectrum of the sample indicating composition of the sample which contains various functional groups. XRD result shows the particle size of CuO at highest peak 29.40140 was 61.25 nm and the particle size of ZnO at highest peak 36.24760 was 21.82 nm. FT-IR spectra peak at 594.56 cm-1 indicated characteristic absorption bands of ZnO nanoparticles and the broad band peak at 3506.9 cm-1 can be attributed to the characteristic absorption of O-H group. The analysis of FT-IR spectrum of CuO shows peaks at 602.09, 678.39, and 730.19cm−1 which refer to the formation of CuO. A broad absorption peak noticed at 3308.2 cm−1 attributed to O–H stretching of the moisture content.

Preparation of LiTaO3 Nano-Crystalline Films by Sol-Gel Process

2012 ◽  
Vol 531-532 ◽  
pp. 446-449 ◽  
Author(s):  
Jun Gou ◽  
Jun Wang ◽  
Ze Hua Huang ◽  
Ya Dong Jiang
Keyword(s):  
Thin Films ◽  
High Performance ◽  
Detection System ◽  
Sol Gel ◽  
Precursor Solution ◽  
Film Material ◽  
Nano Crystalline ◽  
Sol Gel Process ◽  
Crystalline Films ◽  
P Type

Lithium tantalite (LiTaO3) thin film material shows good feasibility and potential for the application of high-performance detection system. In this paper, sol-gel process of LiTaO3 thin films on p-type (111) silicon substrates was described. Stable precursor solution with a desired viscosity was obtained using lithium acetate (LiAc) and tantalum ethoxide (Ta(OC2H5)5) as starting materials. Heat treatment process was optimized to fabricate LiTaO3 films of high crystallinity. Higher crystalline quality films were obtained when each spin-coating process was followed by an annealing operation. Microstructures and crystallization properties of LiTaO3 thin films were further studied. Nano-crystalline films were obtained after annealing at 700 °C for 5 min. The experimental results indicated that the crystallinity and mean grain size of LiTaO3 thin films were proportional to the film thickness.

High-performance Li3V2(PO4)3/C cathode material with a mixed morphology prepared by solvothermal assisted sol–gel process

Ionics ◽  
2018 ◽  
Vol 25 (5) ◽  
pp. 2057-2067 ◽  
Author(s):  
Xiao-Kai Ding ◽  
Jing Liu ◽  
Lu-Lu Zhang ◽  
Xue-Lin Yang
Keyword(s):  
Cathode Material ◽  
High Performance ◽  
Sol Gel ◽  
Sol Gel Process

scholarly journals Morphologically and compositionally tuned lithium silicate nanorods as high-performance carbon dioxide sorbents

2016 ◽  
Vol 4 (43) ◽  
pp. 16928-16935 ◽  
Author(s):  
P. V. Subha ◽  
Balagopal N. Nair ◽  
A. Peer Mohamed ◽  
G. M. Anilkumar ◽  
K. G. K. Warrier ◽  
...  
Keyword(s):  
Carbon Dioxide ◽  
High Performance ◽  
Sol Gel ◽  
Lithium Silicate ◽  
Sol Gel Process

The lithium silicate nanorods derived by a microwave sol gel process display extremely fast CO2 absorption rates as well as remarkable durability for prolonged application.

Production and Shaping of High Performance Phosphors for Lighting by Using Sol-Gel Process.

ChemInform ◽  
2005 ◽  
Vol 36 (35) ◽  
Author(s):  
G. Bertrand-Chadeyron ◽  
D. Boyer ◽  
P. Boutinaud ◽  
A. C. Franville ◽  
J. M. Nedelec ◽  
...  
Keyword(s):  
High Performance ◽  
Sol Gel ◽  
Sol Gel Process

scholarly journals Heterogeneous Hybrid Nanocomposite Based on Chitosan/Magnesia Hybrid Films: Ecofriendly and Recyclable Solid Catalysts for Organic Reactions

Polymers ◽  
2021 ◽  
Vol 13 (20) ◽  
pp. 3583
Author(s):  
Metwally Madkour ◽  
Khaled D. Khalil ◽  
Fakhreia A. Al-Sagheer
Keyword(s):  
Heterogeneous Catalysts ◽  
Sol Gel ◽  
Analytical Techniques ◽  
Hybrid Films ◽  
One Pot ◽  
Solid Catalysts ◽  
Force Microscopy ◽  
Chitosan Matrix ◽  
Atomic Force ◽  
Sol Gel Process

Chitosan/magnesia hybrid films (CS-Mg) have been prepared via sol-gel process and employed as heterogeneous catalysts. An in situ generation of a magnesia network in the chitosan matrix was performed through hydrolysis/condensation reactions of magnesium ethoxide. The synthesized hybrid films were characterized using various analytical techniques, such as X-ray photo-electron spectroscopy (XPS), field emission scanning electron microscopy (FESEM) and atomic force microscopy (AFM). The hybrid films display excellent catalytic activities in Michael and Knoevenagel reactions via one pot or solvent-free approaches under microwave irradiation conditions. Chitosan/magnesia hybrid films, catalysed pyrimidine, benzochromene, coumarin and arylidene-malononitriles derivatives formation reactions occurred with highly efficient yields of 97%, 92%, 86% and 95% respectively. Due to the fact that the films are durable and insoluble in common organic solvents, they were easily separated and can be recycled up to five times without a considerable loss of their catalytic activity.

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