scholarly journals A detailed microstructural and corrosion analysis of an additively manufactured magnesium alloy produced by selective laser melting

Author(s):  
Mohsen Esmaily ◽  
Zhuoran Zeng ◽  
Nooshin Mortazavi ◽  
Alessio Gullino ◽  
Sanjay Choudhary ◽  
...  

Magnesium (Mg) alloys have promising potentials for lightweight and biomedical applications. Although there has been a recent interest in producing Mg alloys (including AZ, ZK and WE series) using additive manufacturing (AM), the process-structure-corrosion properties relationships in AM Mg alloys are yet to be understood. Herein, the production of Mg alloy WE43 was achieved by selective laser melting (SLM). The alloy was investigated after SLM, hot isostatic pressing (HIP) as well as an additional solutionising heat treatment. Specimens were carefully characterised, whilst assessed and contrast relative to the conventionally cast alloy counterpart. Characterisation included detailed microstructural analysis employing analytical transmission electron microscopy, X-ray mapping, and electron backscatter diffraction, which revealed the SLM prepared specimens possess a unique microstructure comprising fine grains growing with a strong [0001] texture along the building direction. The SLM prepared specimens also revealed a low fraction of process-induced and metallurgical defects, reaching < 0.1% after optimising the SLM parameters and HIP treatment. The SLM prepared WE43 was found to be cathodically more active relative to the cast WE43 because of a fine distribution of zirconium-, yttrium- and oxygen-rich particles as well as the alterations in the chemical composition of the solid-solution matrix originating from the high cooling rates of SLM. It was revealed that the oxide particles were mainly sourced by powder and thus it is hypothesised that the corrosion of SLM prepared Mg alloys could be greatly improved once the influence of powder characteristics is further understood and controlled.

2021 ◽  
Vol 1016 ◽  
pp. 399-406
Author(s):  
Christoph Egger ◽  
Florian Grünbart ◽  
Zahra Silvayeh ◽  
Olga Šulcová ◽  
Christoph Seper ◽  
...  

Fabrication of aluminum alloy components by traditional high-pressure die casting (HPDC) requires cost- and time-consuming tooling of steel dies, which makes HPDC uneconomic for producing low-volume components or prototypes. In comparison, powder bed-based additive manufacturing, e.g. selective laser melting (SLM), enables rapid prototyping and production of even complex-shaped components directly from computer-aided design models without needing expensive tools. However, SLM prototype components must have almost identical mechanical properties to HPDC serial components in order to emulate their functionality under different load conditions. In this work uniaxial tensile properties of cast alloy AlSi10MnMg (EN AC-43500) in condition T7, i.e. with 120-170 MPa yield stress, 200-240 MPa tensile strength and 9-12 % strain at fracture, shall be attained using selective laser melting of powder alloy AlSi10Mg (EN AC-43000). These properties were achieved by tailored heat treatment. Furthermore, the effect of hot isostatic pressing (HIP) was investigated. The results of the tensile tests confirmed the basic feasibility of substituting HPDC components with SLM components for prototyping. In particular, similar tensile strength and uniform strain were achieved for SLM samples in condition O, i.e. for SLM samples which were only annealed.


Materials ◽  
2021 ◽  
Vol 14 (5) ◽  
pp. 1215
Author(s):  
Mirza Atif Abbas ◽  
Yan Anru ◽  
Zhi Yong Wang

Additively manufactured tungsten and its alloys have been widely used for plasma facing components (PFCs) in future nuclear fusion reactors. Under the fusion process, PFCs experience a high-temperature exposure, which will ultimately affect the microstructural features, keeping in mind the importance of microstructures. In this study, microhardness and electron backscatter diffraction (EBSD) techniques were used to study the specimens. Vickers hardness method was used to study tungsten under different parameters. EBSD technique was used to study the microstructure and Kikuchi pattern of samples under different orientations. We mainly focused on selective laser melting (SLM) parameters and the effects of these parameters on the results of different techniques used to study the behavior of samples.


2019 ◽  
Vol 25 ◽  
pp. 412-420 ◽  
Author(s):  
Tadashi Fujieda ◽  
Meichuan Chen ◽  
Hiroshi Shiratori ◽  
Kosuke Kuwabara ◽  
Kenta Yamanaka ◽  
...  

Metals ◽  
2020 ◽  
Vol 10 (6) ◽  
pp. 814 ◽  
Author(s):  
Carlo Alberto Biffi ◽  
Paola Bassani ◽  
Jacopo Fiocchi ◽  
Ausonio Tuissi

Nowadays, additive manufacturing (AM) permits to realize complex metallic structural parts, and the use of NiTi alloy, known as Nitinol, allows the integration of specific functions to the AM products. One of the most promising designs for AM is concerning the use of lattice structures that show lightweight, higher than bulk material deformability, improved damping properties, high exchange surface. Moreover, lattice structures can be realized with struts, having dimensions below 1 mm—this is very attractive for the realization of Nitinol components for biomedical devices. In this light, the present work regarded the experimental characterization of lattice structures, produced by selective laser melting (SLM), by using Ni-rich NiTi alloy. Differential scanning calorimetry (DSC), electron backscatter diffraction (EBSD), and compression testing were carried out for analyzing microstructure, martensitic transformation (MT) evolution, and superelasticity response of the SLMed lattice samples. The lattice microstructures were compared with those of the SLMed bulk material for highlighting differences. Localized martensite was detected in the nodes zones, where the rapid solidification tends to accumulate solidification stresses. An increase of martensitic transformation temperatures was also observed in lattice NiTi.


2019 ◽  
Vol 5 ◽  
pp. 23 ◽  
Author(s):  
Anne-Helene Puichaud ◽  
Camille Flament ◽  
Aziz Chniouel ◽  
Fernando Lomello ◽  
Elodie Rouesne ◽  
...  

Additive manufacturing (AM) is rapidly expanding in many industrial applications because of the versatile possibilities of fast and complex fabrication of added value products. This manufacturing process would significantly reduce manufacturing time and development cost for nuclear components. However, the process leads to materials with complex microstructures, and their structural stability for nuclear application is still uncertain. This study focuses on 316L stainless steel fabricated by selective laser melting (SLM) in the context of nuclear application, and compares with a cold-rolled solution annealed 316L sample. The effect of heat treatment (HT) and hot isostatic pressing (HIP) on the microstructure and mechanical properties is discussed. It was found that after HT, the material microstructure remains mostly unchanged, while the HIP treatment removes the materials porosity, and partially re-crystallises the microstructure. Finally, the tensile tests showed excellent results, satisfying RCC-MR code requirements for all AM materials.


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