Production and characterization of Al6061/zirconium carbide surface composites

2020 ◽  
Vol 111 (8) ◽  
pp. 639-644
Author(s):  
Shalini Sundarrajan ◽  
Thandlam Satish Kumar ◽  
Ganesan Suganya Priyadharshini
Keyword(s):  
Volume Fraction ◽  
Zirconium Carbide ◽  
X Ray Diffraction ◽  
Scanning Electron Microscopy Micrographs ◽  
X Ray ◽  
Friction Stir ◽  
Surface Composites ◽  
Carbide Particles ◽  
Microstructural Studies

Abstract In the present study, Al6061/zirconium carbide surface composites have been developed using the friction stir processing method. The volume fraction of the zirconium carbide particles was varied as 3%, 6% and 9%. The developed composites were characterized using optical microscopy, X-ray diffraction and scanning electron microscopy. Micrographs revealed uniform distribution of zirconium carbide particles, and addition of zirconium carbide particles was found to improve hardness and tensile properties of Al6061 alloy. Corresponding strengthening mechanisms have been discussed and associated with the microstructural studies. Fractographic analysis was found to show a reduction in ductility with increase in addition of zirconium carbide particles.

scholarly journals Double Reinforcement of Al–Fe Intermetallic Composites Fabricated by Friction Stir Processing

Metals ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 1002
Author(s):  
Chunping Huang ◽  
Yang Xia ◽  
Chun Xia ◽  
Fencheng Liu
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Friction Stir Processing ◽  
Volume Fraction ◽  
X Ray Diffraction ◽  
X Ray ◽  
Friction Stir ◽  
Metallurgical Bond ◽  
Aluminum Alloy Surface ◽  
Scanning Electron

A double reinforced layer on an aluminum alloy surface was produced using friction stir processing (FSP) by adding 34CrNiMo6 powder into Al (AA2024) substrate for better wear resistance and gradient transitions. The microstructures of the composites were analyzed using scanning electron microscopy (SEM) and energy dispersive spectroscopy (EDS). The phase composition was examined by X-ray diffraction (XRD). The results show that the double reinforced layer of the Al13Fe4 intermetallic compound could be successfully fabricated via FSP. The volume fraction of Al13Fe4 in the double reinforced layer was higher than in the single reinforced layer due to adding 34CrNiMo6 powder and reinforced twice, and the Al13Fe4 particles were dispersed more homogeneously in the double reinforced layer. The interfaces between the double and single reinforced layer had a good metallurgical bond. The microhardness of the double reinforcement layer was significantly increased. Compared with the AA2024 substrate, the microhardness of the double and single reinforced layers increased five- (576 HV) and two-fold (254 HV), respectively.

Sol-gel derived Ba(Mg1/3Ta2/3)O3 thin films: Preparation and structure

1997 ◽  
Vol 12 (3) ◽  
pp. 596-599 ◽  
Author(s):  
Ji Zhou ◽  
Qing-Xin Su ◽  
K. M. Moulding ◽  
D. J. Barber
Keyword(s):  
Thin Films ◽  
Annealing Temperature ◽  
Volume Fraction ◽  
Sol Gel ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Sol Gel Process ◽  
Small Grains

Ba(Mg1/3Ta2/3)O3 thin films were prepared by a sol-gel process involving the reaction of barium isopropoxide, tantalum ethoxide, and magnesium acetate in 2-methoxyethanol and subsequently hydrolysis, spin-coating, and heat treatment. Transmission electron microscopy, x-ray diffraction, and Raman spectroscopy were used for the characterization of the thin films. It was shown that the thin films tend to crystallize with small grains sized below 100 nm. Crystalline phase with cubic (disordered) perovskite structure was formed in the samples annealed at a very low temperature (below 500 °C), and well-crystallized thin films were obtained at 700 °C. Although disordered perovskite is dominant in the thin films annealed below 1000 °C, a low volume fraction of 1 : 2 ordering domains was found in the samples and grows with an increase of annealing temperature.

scholarly journals Characterization Of Microstructure And Selected Properties of SnSbCu Alloy After FSP

2021 ◽  
Author(s):  
Joanna Hrabia-Wiśnios ◽  
Beata Leszczyńska-Madej ◽  
Marcin Madej ◽  
Aleksandra Węglowska
Keyword(s):  
Flexural Strength ◽  
Diffraction Method ◽  
Compression Tests ◽  
X Ray Diffraction ◽  
Linear Speed ◽  
X Ray ◽  
Friction Stir ◽  
Before And After ◽  
Bearing Alloy

Abstract The paper presents the results of research on the microstructure and selected mechanical properties of the SnSbCu bearing alloy after friction stir processing (FSP). The Whorl tool was used for modification; the process was carried out using two rotational speeds of the tool: 280 and 450 RPM and a constant linear speed of 355 mm/min. Microstructure studies were performed employing the techniques of light microscopy and scanning electron microscopy along with analysis of the chemical composition of micro-areas. Additionally, the phase composition was investigated by means of the X-ray diffraction method and statistical analysis of the precipitates present in the investigated alloy. In addition, hardness, flexural strength and uniaxial compression tests were performed before and after FSP modification. It was proved that using FSP to modify the SnSbCu alloy promotes refinement and homogenization of the microstructure, as well as improvement of the flexural strength, whereas no changes in the hardness level were found.

scholarly journals Wear Characterization of Al/ B4C surface composite produced by TIG arc process

2018 ◽  
Vol 3 (2) ◽  
pp. 01-05
Author(s):  
N. Yuvaraj ◽  
Keyword(s):  
Optical Microscope ◽  
X Ray Diffraction ◽  
Wear Properties ◽  
Composite Surface ◽  
X Ray ◽  
Surface Composite ◽  
Surface Composites ◽  
Scanning Electron ◽  
Wear Characterization

Aluminum-based surface composites were fabricated by the TIG arc process. B4C micro and nanoparticles were filled separately on the grooves of the Aluminum substrate and modified the surfaces with different TIG arc speeds. The modified composite surface was characterized by optical microscope, Scanning Electron microscope, and X-ray diffraction. The microhardness and wear properties of the composite surface were evaluated. The results of this study revealed that the newly formed nanocomposite surface enhances the hardness and wear characteristics. The wear worn-out surfaces of the composite surface were analyzed through SEM studies in order to understand the wear mechanisms

scholarly journals Effect of Silver (Ag) Addition on the Forming Of Y-247 Superconductors (Y2Ba4Cu7O15-?) using Wet Mixing Method

2019 ◽  
Vol 20 (1) ◽  
pp. 11
Author(s):  
A.A. Made Wisnu Wijaya Putra ◽  
W. G. Suharta ◽  
P. Suardana
Keyword(s):  
Volume Fraction ◽  
Lattice Parameter ◽  
Synthesis Process ◽  
X Ray Diffraction ◽  
Ag Addition ◽  
X Ray ◽  
Mixing Method ◽  
Parameter Values ◽  
Scanning Electron

Superconductor Y-247 (Y2Ba4Cu7O15-?) with adding silver (Ag) by using the wet-mixing method has been done. The synthesis process was carried out by calcination at 600o C for 3 hours and sintered at 925o C for 10 hours. Variations in the increase in the addition of Ag used were Ag0.05, Ag0.1, Ag0.15 and Ag0.2. Characterization of X-Ray Diffraction (XRD), showed an increase in the addition of Ag resulting in a decrease in the volume fraction, where the volume fractions obtained consecutive were 55.0%, 51.3%, 50.9% and 46.3%. Increasing the addition of Ag results in an increase in the lattice parameter values in the direction of the a axis which is 3.8247 Å, 3.8291 Å, 3.8292 Å, 3.8293 Å, decreasing the lattice parameter values in the b axis direction which is 3.8426 Å, 3.8415 Å, 3.8409 Å, 3.8383 Å and decreasing the lattice parameter values in the direction of the c axis are 49.2174 Å, 49.2022 Å, 49.1881 Å, 49.1761 Å. Analysis of the results of the characterization of Scanning Electron Microscopy (SEM), the particle size obtained was 225.47 nm, 202.88 nm, 190.68 nm and 172.22 nm.

Synthesis and Characterization of Magnesium Diboride Additions of Bi-2223 on the Microstructure and Superconducting Transition

2019 ◽  
Vol 290 ◽  
pp. 233-238 ◽  
Author(s):  
Arlina Binti Ali ◽  
Abdul Halim Shaari ◽  
Soo Kien Chen ◽  
Julie Juliewatty Mohamed ◽  
Nurul’ain Mohd Kamal ◽  
...  
Keyword(s):  
Volume Fraction ◽  
Magnesium Diboride ◽  
Superconducting Transition ◽  
X Ray Diffraction ◽  
Solid State Method ◽  
Metallic Behavior ◽  
Volume Percentage ◽  
X Ray ◽  
State Method

In this paper, solid state method was using to synthesize the of magnesium diboride (MgB2) added in Bi 1.6Pb 0.4Sr2Ca2Cu3Oδ(Bi-2223) superconductor from 0.00 to 0.10 wt.%. The effect on additions were investigated through X-ray Diffraction (XRD), resistance-temperature (R-T) measurement and Scanning Electron Microscope (SEM). From the XRD result, volume fraction of Bi-2223 showed the highest volume percentage was 76 % correspond to addition with MgB2=0.02 wt.% and slightly decreased the percentage while increased the additions. From the R-T measurement, all samples showed the metallic behavior in the normal state. Morphology images showed that the grains were flaky plates and the size slightly increased. These results revealed that, additions of magnesium diboride change the microstructure and decrease the superconducting transition.

scholarly journals The Characterization Of Cast Fe-Cr-C Alloy

2015 ◽  
Vol 60 (2) ◽  
pp. 779-782 ◽  
Author(s):  
K. Wieczerzak ◽  
P. Bała ◽  
M. Stępień ◽  
G. Cios ◽  
T. Kozieł
Keyword(s):  
Volume Fraction ◽  
Microstructural Characterization ◽  
High Volume ◽  
Phase Identification ◽  
Arc Furnace ◽  
X Ray Diffraction ◽  
Cast State ◽  
X Ray ◽  
Average Hardness

AbstractThe paper presents the results of the characterization of alloy from Fe-Cr-C (carbon content 0.79 wt.%) system including the microstructure, phase analysis, morphology and hardness in as cast state. The chemical composition was designed to create chromium-rich ferritic matrix with high volume fraction of carbides in form of interdendritic eutectics. The research was carried out on the cross section of the ingot, synthesized in an arc furnace under high purity argon atmosphere and crystallized on water-cooled copper mould. Microstructural characterization was carried out by light microscopy and scanning electron microscopy (SEM). Phase identification was performed by X-Ray diffraction (XRD). The microstructure of the investigated alloy is composed of primary and secondary dendrites Fe-Cr solid solution and complex M23C6and M7C3carbides in interdendritic areas. Segregation of Cr and C during crystallization causes precipitation of M7C3carbides. The average hardness of the alloy is 205±12 HV10.

scholarly journals Characterization of microstructure and selected properties of SnSbCu alloy after FSP

2021 ◽  
Author(s):  
Joanna Hrabia-Wiśnios ◽  
Beata Leszczyńska-Madej ◽  
Marcin Madej ◽  
Aleksandra Węglowska
Keyword(s):  
Flexural Strength ◽  
Diffraction Method ◽  
Compression Tests ◽  
X Ray Diffraction ◽  
Linear Speed ◽  
X Ray ◽  
Friction Stir ◽  
Before And After ◽  
Bearing Alloy

AbstractThe paper presents the results of research on the microstructure and selected mechanical properties of the SnSbCu-bearing alloy after friction stir processing (FSP). The Whorl tool was used for modification; the process was carried out using two rotational speeds of the tool: 280 and 450 RPM and a constant linear speed of 355 mm/min. Microstructure studies were performed employing the techniques of light microscopy and scanning electron microscopy along with analysis of the chemical composition of micro-areas. Additionally, the phase composition was investigated by means of the X-ray diffraction method and statistical analysis of the precipitates present in the investigated alloy. In addition, hardness, flexural strength, and uniaxial compression tests were performed before and after FSP modification. It was proved that using FSP to modify the SnSbCu alloy promotes refinement and homogenization of the microstructure, as well as improvement of the flexural strength, whereas no changes in the hardness level were found.

Structural Characterization of Mullite-Based Ceramic Material from Al2O3 and Silica Xerogel Converted from Sago Waste Ash

2013 ◽  
Vol 789 ◽  
pp. 262-268
Author(s):  
Haji Aripin ◽  
Seitaro Mitsudo ◽  
Endangsusilowati S. Prima ◽  
Inyoman Nyoman Sudiana ◽  
Hikamitsu Kikuchi ◽  
...  
Keyword(s):  
Volume Fraction ◽  
Silica Xerogel ◽  
Dsc Analysis ◽  
X Ray Diffraction ◽  
Xrd Pattern ◽  
X Ray ◽  
Sago Waste ◽  
Scanning Electron ◽  
Mullite Ceramics

In this investigation, mullite ceramics were produced by mixing Al2O3and amorphous silica xerogel (SX) extracted from sago waste ash. The composition was prepared by adding an amount from 0 to 80 mol% of Al2O3into SX. The samples were dry pressed and sintered in the temperature range between 900°C and 1200°C. Their properties have been characterized on the basis of the experimental data obtained using thermal analysis (DSC/TGA, X-ray diffraction and scanning electron microscopy (SEM). The results show that two major differences become obvious when comparing the samples loaded by the smaller and larger amount of Al2O3. First, cristobalite formation is retarded in the sample loaded by the larger amount of Al2O3. Second, at 1200°C, the observed volume fraction of mullite is higher in the sample loaded by the larger amount of Al2O3. The DSC analysis indicates that the mullite crystallization takes place at 1200°C for 60 mol% Al2O3loaded SX sample as confirmed by the XRD pattern. It was found that there was not a complete reaction of mulitization for sample sintered up to 1200°C.

Synthesis and Characterization of Ti-TiB Composites Processed through Vacuum Sintering

2014 ◽  
Vol 592-594 ◽  
pp. 765-769
Author(s):  
M. Selva Kumar ◽  
P. Chandrasekar ◽  
Balasubramanian Ravisankar ◽  
M. Mohanraj
Keyword(s):  
Volume Fraction ◽  
Titanium Boride ◽  
Electron Probe Micro Analysis ◽  
X Ray Diffraction ◽  
Vacuum Sintering ◽  
Microstructural Characteristics ◽  
X Ray ◽  
Increase With Increase ◽  
Micro Analysis

In the present work, an attempt has been made to explore the general microstructural characteristics and mechanical properties of titanium-titanium boride (Ti-TiB) composites (20 and 40 vol.% TiB reinforcement in Ti matrix) processed by Vacuum Sintering. The microstructures of the composites were investigated using electron probe micro analysis, scanning electron microscopy and X-ray diffraction. Obviously, the elastic modulus, shear modulus and hardness are found to increase with increase in volume fraction of titanium boride. The effects of titanium boride reinforcements on elastic properties and microhardness are discussed.

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