Synthesis and characterization of Co–B–Fe–Ti nanosized alloyed powders

2021 ◽  
Vol 112 (1) ◽  
pp. 35-41
Author(s):  
Hasan Eskalen ◽  
Mikail Aslan ◽  
Hakan Yaykaşlı ◽  
Musa Gögebakan
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Solid Solution ◽  
Analytical Techniques ◽  
High Energy ◽  
Nanocrystalline Phase ◽  
Micro Hardness ◽  
X Ray Diffraction ◽  
X Ray ◽  
Ball Milling Technique

Abstract In this study, novel Co60Fe18Ti18B4 alloy powders have been synthesized with high compositional homogeneity using a high-energy ball milling technique. The structural, morphological and mechanical properties of the nanosized alloyed powders were examined using different analytical techniques, including scanning electron microscopy, transmission electron microscopy, energy-dispersive X-ray spectrometry and X-ray diffraction. According to the X-ray diffraction analysis for both Co powder and Co60Fe18Ti18B4 alloy powders, with increasing milling time, the content of Co-based (hcp) solid solution decreased and Co-based (fcc) solid solution increased. The mechanical properties of the material were also investigated by Vickers micro-hardness testing. The micro-hardness value of the Co60Fe18Ti18B4 alloy was found as 120.08 HV. After sintering (1 h– 1000 °C), the hardness improved remarkably (536.32 HV). Furthermore, results indicate that the synthesized Co-based alloy powder has both glassy and nanocrystalline phase forms.

scholarly journals Analytical study of Buddha sculptures in Jingyin temple of Taiyuan, China

2021 ◽  
Vol 9 (1) ◽  
Author(s):  
Xiaojian Bai ◽  
Chen Jia ◽  
Zhigen Chen ◽  
Yuxuan Gong ◽  
Huwei Cheng ◽  
...  
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Analytical Study ◽  
Energy Dispersive Spectrometry ◽  
Analytical Techniques ◽  
X Ray Diffraction ◽  
Ancient China ◽  
X Ray ◽  
Unique Style ◽  
Scanning Electron

AbstractWith exquisite design and unique style, the painted sculptures of Tutang Buddha and two attendants Buddha in Jingyin Temple are precious cultural heritages of China. The sculpture of Tutang Buddha, which was carved from a mound and painted by ancient craftsmen, was rarely found in ancient China. However, due to natural and human factors, the sculptures were severely damaged. Obviously, they require urgent and appropriate protection and restoration. In this study, samples taken from the sculptures were analysed through multiple analytical techniques, including scanning electron microscopy with energy dispersive spectrometry (SEM–EDS), Raman spectroscopy, X-ray diffraction (XRD), optical microscopy (OM) and granulometry. The analysis results enable us to infer the techniques used by the craftsmen in making the sculptures and provide a reliable evidence for the conservation and future protection of these and similar sculptures.

scholarly journals Synthesis of Ce1−xPdxO2−δ Solid Solution in Molten Nitrate

Catalysts ◽  
2020 ◽  
Vol 10 (6) ◽  
pp. 640
Author(s):  
Hideaki Sasaki ◽  
Keisuke Sakamoto ◽  
Masami Mori ◽  
Tatsuaki Sakamoto
Keyword(s):  
Electron Microscopy ◽  
Solid Solution ◽  
Solid Solutions ◽  
Photoelectron Spectroscopy ◽  
Synthesis Method ◽  
X Ray Diffraction ◽  
X Ray ◽  
Transmission Electron ◽  
Co Precipitation ◽  
Ionic States

CeO2-based solid solutions in which Pd partially substitutes for Ce attract considerable attention, owing to their high catalytic performances. In this study, the solid solution (Ce1−xPdxO2−δ) with a high Pd content (x ~ 0.2) was synthesized through co-precipitation under oxidative conditions using molten nitrate, and its structure and thermal decomposition were examined. The characteristics of the solid solution, such as the change in a lattice constant, inhibition of sintering, and ionic states, were examined using X-ray diffraction (XRD), scanning electron microscopy–energy-dispersive X-ray spectroscopy (SEM−EDS), transmission electron microscopy (TEM)−EDS, and X-ray photoelectron spectroscopy (XPS). The synthesis method proposed in this study appears suitable for the easy preparation of CeO2 solid solutions with a high Pd content.

scholarly journals Features of the hydration process of the modified blended cement for fiber cement panels

2018 ◽  
Vol 170 ◽  
pp. 03030 ◽  
Author(s):  
Rustem Mukhametrakhimov ◽  
Liliya Lukmanova
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Blended Cement ◽  
Physical And Mechanical Properties ◽  
Hydration Process ◽  
Cement Matrix ◽  
X Ray Diffraction ◽  
Structure Form ◽  
Silicate Phase ◽  
X Ray

The paper studies features of the hydration process of the modified blended cement for fiber cement panels (FCP) using differential thermal analysis, X-ray diffraction analysis, electron microscopy and infrared spectroscopy. It is found that deeper hydration process in silicate phase, denser and finer crystalline structure form in fiber cement matrix based on the modified blended cement. Generalization of this result to the case of fiber cement panels makes it possible to achieve formation of a denser and homogeneous structure with increased physical and mechanical properties.

Effect of Sintering Temperature on Microstructure and Mechanical Properties of Al2O3-TiC-ZrO2 Ceramic Composites

2012 ◽  
Vol 476-478 ◽  
pp. 1031-1035
Author(s):  
Wei Min Liu ◽  
Xing Ai ◽  
Jun Zhao ◽  
Yong Hui Zhou
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Fracture Toughness ◽  
Flexural Strength ◽  
Relative Density ◽  
Sintering Temperature ◽  
Ceramic Composites ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

Al2O3-TiC-ZrO2ceramic composites (ATZ) were fabricated by hot-pressed sintering. The phases and microstructure of the composites were studied by X-ray diffraction (XRD) and scanning electron microscopy (SEM). The relative density and mechanical properties (flexural strength, fracture toughness and Vicker’s hardness) of the composites were tested. The results show that the microstructure of the composites was the gray core-white rim. With the increase of sintering temperature, the relative density and mechanical properties of the composites increased first and then decreased. The composite sintered at 1705°C has the highest synthetical properties, and its relative density, flexural strength, fracture toughness and Vickers hardness are 98.3%,970MPa,6.0 MPa•m1/2and 20.5GPa, respectively.

Research on compatibility and surface of high impact bio-based polyamide

2021 ◽  
pp. 095400832110055
Author(s):  
Yang Wang ◽  
Yuhui Zhang ◽  
Yuhan Xu ◽  
Xiucai Liu ◽  
Weihong Guo
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Differential Scanning Calorimetry ◽  
Crystallization Behavior ◽  
High Impact ◽  
X Ray Diffraction ◽  
Scanning Calorimetry ◽  
X Ray ◽  
Scanning Electron

The super-tough bio-based nylon was prepared by melt extrusion. In order to improve the compatibility between bio-based nylon and elastomer, the elastomer POE was grafted with maleic anhydride. Scanning Electron Microscopy (SEM) and Thermogravimetric Analysis (TGA) were used to study the compatibility and micro-distribution between super-tough bio-based nylon and toughened elastomers. The results of mechanical strength experiments show that the 20% content of POE-g-MAH has the best toughening effect. After toughening, the toughness of the super-tough nylon was significantly improved. The notched impact strength was 88 kJ/m2 increasing by 1700%, which was in line with the industrial super-tough nylon. X-ray Diffraction (XRD) and Differential Scanning Calorimetry (DSC) were used to study the crystallization behavior of bio-based PA56, and the effect of bio-based PA56 with high crystallinity on mechanical properties was analyzed from the microstructure.

scholarly journals Synthesis and characterization of apatite silicated powders with wet precipitation method

2021 ◽  
Vol 234 ◽  
pp. 00106
Author(s):  
Houda Labjar ◽  
Hassan Chaair
Keyword(s):  
Electron Microscopy ◽  
Heat Treatment ◽  
Analytical Techniques ◽  
Precipitation Method ◽  
Synthesis And Characterization ◽  
X Ray Diffraction ◽  
X Ray ◽  
Wet Precipitation ◽  
Scanning Electron

The synthesis of apatite silicated Ca10(PO4)6-x(SiO4)x(OH)2-x (SiHA) with 0≤x≤2 was investigated using a wet precipitation method followed by heat treatment using calcium carbonate CaCO3 and phosphoric acid H3PO4 and silicon tetraacetate SiC8H20O4 (TEOS) in medium of water ethanol, with three different silicate concentrations. After drying, the samples are ground and then characterized by different analytical techniques like X-ray Diffraction (XRD), Fourier Transform Infrared Spectroscopy (FTIR) and Scanning electron Microscopy (SEM) and chemical analysis.

Influence of Aging Treatments on the Structural and Mechanical Properties of AGS Alloy Wire Cold Drawn

2018 ◽  
Vol 18 ◽  
pp. 73-78
Author(s):  
Mokhtar Bayarassou ◽  
Mosbah Zidani ◽  
Hichem Farh
Keyword(s):  
Mechanical Properties ◽  
Plastic Deformation ◽  
Electron Microscope ◽  
Artificial Ageing ◽  
Micro Hardness ◽  
X Ray Diffraction ◽  
Alloy Wire ◽  
X Ray ◽  
Plastic Deformation Rate ◽  
Scanning Electron

The scope of this work is to study of microstructural changes and mechanical properties during natural and artificial ageing treatment of AGS Alloy wire cold drawn with different deformation at ENICAB in Biskra. And as well to know the phase formation during different deformation of aluminum alloys wires. as well as the combined influence of the plastic deformation rate and the aging temperature. Wire section reduction shows a change in microstructure and texture. The methods of characterization used in this work are: scanning electron microscope and X-ray diffraction, micro hardness (Hv).

UTILIZATION OF FLY ASH AND CONCRETE RESIDUE IN THE PRODUCTION OF GEOPOLYMER BRICKS

2017 ◽  
Vol 12 (1) ◽  
pp. 63-77 ◽  
Author(s):  
Siriporn Sirikingkaew ◽  
Nuta Supakata
Keyword(s):  
Electron Microscopy ◽  
Mechanical Properties ◽  
Scanning Electron Microscopy ◽  
Compressive Strength ◽  
Phase Composition ◽  
Fly Ash ◽  
Industrial Waste ◽  
X Ray Diffraction ◽  
X Ray ◽  
Scanning Electron

This study presents the development of geopolymer bricks synthetized from industrial waste, including fly ash mixed with concrete residue containing aluminosilicate compound. The above two ingredients are mixed according to five ratios: 100:0, 95:5, 90:10, 85:15, and 80:20. The mixture's physico-mechanical properties, in terms of water absorption and the compressive strength of the geopolymer bricks, are investigated according to the TIS 168-2546 standard. Scanning electron microscopy (SEM) and X-ray diffraction (XRD) analyses are used to investigate the microstructure and the elemental and phase composition of the brick specimens. The results indicate that the combination of fly ash and concrete residue represents a suitable approach to brick production, as required by the TIS 168–2546 standard.

scholarly journals Characterising the Microstructure of an Additively Built Al-Cu-Li Alloy

Materials ◽  
2020 ◽  
Vol 13 (22) ◽  
pp. 5188
Author(s):  
Iris Raffeis ◽  
Frank Adjei-Kyeremeh ◽  
Uwe Vroomen ◽  
Silvia Richter ◽  
Andreas Bührig-Polaczek
Keyword(s):  
Volume Fraction ◽  
Analytical Techniques ◽  
High Strength ◽  
High Energy ◽  
Phase System ◽  
X Ray Diffraction ◽  
Powder Bed ◽  
X Ray ◽  
Conventional View ◽  
Multi Phase

Al-Cu-Li alloys are famous for their high strength, ductility and weight-saving properties, and have for many years been the aerospace alloy of choice. Depending on the alloy composition, this multi-phase system may give rise to several phases, including the major strengthening T1 (Al2CuLi) phase. Microstructure investigations have extensively been reported for conventionally processed alloys with little focus on their Additive Manufacturing (AM) characterised microstructures. In this work, the Laser Powder Bed Fusion (LPBF) built microstructures of an AA2099 Al-Cu-Li alloy are characterised in the as-built (no preheating) and preheat-treated (320 °C, 500 °C) conditions using various analytical techniques, including Synchrotron High-Energy X-ray Diffraction (S-HEXRD). The observed dislocations in the AM as-built condition with no detected T1 precipitates confirm the conventional view of the difficulty of T1 to nucleate on dislocations without appropriate heat treatments. Two main phases, T1 (Al2CuLi) and TB (Al7.5Cu4Li), were detected using S-HEXRD at both preheat-treated temperatures. Higher volume fraction of T1 measured in the 500 °C (75.2 HV0.1) sample resulted in a higher microhardness compared to the 320 °C (58.7 HV0.1) sample. Higher TB volume fraction measured in the 320 °C sample had a minimal strength effect.

Mechanochemical Synthesis of Intermetallic Compounds in the Gallium–Iridium System

2019 ◽  
Vol 18 (03n04) ◽  
pp. 1940067
Author(s):  
P. Vitiaz ◽  
N. Lyakhov ◽  
T. Grigoreva ◽  
E. Pavlov
Keyword(s):  
Electron Microscopy ◽  
Scanning Electron Microscopy ◽  
Mechanical Activation ◽  
Intermetallic Compounds ◽  
High Energy ◽  
Planetary Mill ◽  
X Ray Diffraction ◽  
X Ray ◽  
Active Liquid ◽  
Scanning Electron

The interaction between a solid inert metal Ir and an active liquid metal Ga during mechanical activation in a high-energy planetary mill is studied by X-ray diffraction and scanning electron microscopy with high-resolution energy dispersive X-ray microanalysis. The effect of mechanical activation on the formation of GaxIry intermetallic compounds and GaxIry/Ir composites and their solubility in acids was investigated. The subsequent extraction of Ga from intermetallic compounds and composites in the mixture of concentrated acids [Formula: see text] makes it possible to produce nanoscale Ir.

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