scholarly journals Alkali-treated wheat gluten cross-linked with sodium alginate as a bio-based wood adhesive for interior grade particleboard

BioResources ◽  
2021 ◽  
Vol 16 (4) ◽  
pp. 7916-7934
Author(s):  
Ajith K. A. Gedara ◽  
Iva Chianella ◽  
Debabrata Bhattacharyya ◽  
Jose L. Endrino ◽  
Qi Zhang
Keyword(s):  
Sodium Alginate ◽  
Bending Strength ◽  
Wheat Gluten ◽  
Single Layer ◽  
Wood Adhesive ◽  
Bending Tests ◽  
Wood Particles ◽  
Ft Ir ◽  
Industrial Standards ◽  
Adhesive Formulation

A bio-based wood adhesive formulation free of formaldehyde and made from alkali-treated wheat gluten (WG) and sodium alginate (SA) was developed. Its formulation was optimised, and it was characterised by Fourier Transform Infrared (FT-IR) spectroscopy. The bio-adhesive was utilized to make particleboards both with virgin wood particles and recycled wood particles. A dry bio-adhesive content of 35% (w/w) was used to make samples with both type of particles. Single-layer samples of 10 mm thickness were obtained using wood particles of 1 mm (both virgin and recycled). These samples then were subjected to 3-point bending tests. Whereas the bending strength of samples made with recycled wood particles was 18.09 N/m2 and therefore satisfied Type 18 of the Japanese industrial standards (JIS A 5908:2015), the bending strength of the samples made with virgin wood particles was 8.08 N/m2 and satisfied ‘Type 8 Base particleboard Decorative particleboard’ of the Japanese standards. The density of particleboard samples made from recycled wood particles was 916 kg/m3, while that of samples made from virgin wood particles was 732 kg/m3. The alkali-treated WG and SA bio-adhesive has the potential to be used to re-manufacture particleboards, which can then be recycled and not disposed in landfills.

Characterization and Screening of a Novel Multiparticulate Pulsatile Delivery of Aceclofenac

2016 ◽  
Vol 9 (5) ◽  
pp. 3494-3501
Author(s):  
Bipul Nath ◽  
Santimoni Saikia
Keyword(s):  
Drug Release ◽  
Sodium Alginate ◽  
Alginate Beads ◽  
In Vitro Drug Release ◽  
Dsc Studies ◽  
Ft Ir ◽  
Lag Period ◽  
Pulsatile Delivery ◽  
Ca Alginate

In the present investigation, sodium alginate based multiparticulate system overcoated with time and pH dependent polymer was studied in the form of oral pulsatile system to achieve pulsatile with sustained release of aceclofenac for chronotherapy of rheumatoid arthritis seven batches of micro beads with varying concentration of sodium alginate (2-5 %) were prepared by ionotropic-gelation method using CaCl2 as cross-linking agent. The prepared Ca-alginate beads were coated with 5% Eudragit L100 and filled into pulsatile capsule with varying proportion of plugging materials. Drug loaded microbeads were investigated for physicochemical properties and drug release characteristics. The mean particle sizes of drug-loaded microbeads were found to be in the range 596±1.1 to 860 ± 1.2 micron and %DEE in the range of 65-85%. FT-IR and DSC studies revealed the absence of drug polymer interactions. The release of aceclofenac from formulations F1 to F7 in buffer media (pH 6.8) at the end of 5h was 65.6, 60.7, 55.7, 41.2, 39.2, 27 and 25% respectively. Pulsatile system filled with eudragit coated Ca-alginate microbeads (F2) showed better drug content, particle size, surface topography, in-vitro drug release in a controlled manner. Different plugging materials like Sterculia gum, HPMC K4M and Carbopol were used in the design of pulsatile capsule. The pulsatile system remained intact in buffer pH 1.2 for 2 hours due to enteric coat of the system with HPMCP. The enteric coat dissolved when the pH of medium was changed to 7.4. The pulsatile system developed with Sterculia gum as plugging material showed satisfactory lag period when compared to HPMC and Carbopol.

Molecular Imprinted Graphene Oxide Nanocomposite for Optical Sensing of Nicotine in Human Blood Plasma

2020 ◽  
Vol 42 (6) ◽  
pp. 856-856
Author(s):  
Sehrish Qazi Sehrish Qazi ◽  
Huma Shaikh Huma Shaikh ◽  
Ayaz Ali Memon Ayaz Ali Memon ◽  
and Shahabuddin Memon and Shahabuddin Memon
Keyword(s):  
Graphene Oxide ◽  
Human Plasma ◽  
Human Blood ◽  
Optical Sensor ◽  
Single Layer ◽  
Human Blood Plasma ◽  
Buffer Concentration ◽  
Imprinted Polymer ◽  
Ft Ir

Among all psychotropic alkaloids, nicotine is more addictive, carcinogenic and capable of causing many health problems. This work is based on the development of highly robust, cheap, reliable, selective and sensitive nicotine imprinted graphene oxide nanocomposite (ImpGO nanocomposite) based optical sensor for determination of nicotine in human plasma. The ImpGO nanocomposite has been thoroughly characterized using different techniques i.e. FT-IR, SEM, TEM, Raman, etc. These characterizations revealed that ImpGO nanocomposite is comprised of single layer of graphene oxide successfully modified with imprinted polymer. The synthesized material was utilized to selectively determine nicotine using UV-vis spectrophotometer in BR buffer of 0.1 M at pH 3 and diluted human plasma. The effect of parameters such as buffer concentration, pH, amount of nanocomposite, etc on determination of nicotine using ImpGO nanocomposite were studied thoroughly. Thus, a sensitive optical method was developed for determination of nicotine in human plasma with linear range of 22-370 pM along with LOD and LOQ of 7 pM and 22 pM, respectively. The selectivity of sensor was evaluated using homologues of nicotine such as nicotine amide, caffeine and cotinine. The results obtained from biological samples showed that developed optical sensor is efficient in complex matrices of real sample.

scholarly journals Preparation, properties and applications of wheat gluten edible films

2000 ◽  
Vol 9 (1) ◽  
pp. 23-35 ◽  
Author(s):  
P. TANADA-PALMU ◽  
H. HELÉN ◽  
L. HYVÖNEN
Keyword(s):  
Weight Loss ◽  
Tensile Strength ◽  
Water Vapor ◽  
Wheat Gluten ◽  
Single Layer ◽  
Water Vapor Permeability ◽  
Edible Films ◽  
Bilayer Film ◽  
Vapor Permeability ◽  
Elongation At Break

Edible films from wheat gluten were prepared with various amounts of glycerol as a plasticizer. Water vapor permeability, oxygen permeability, tensile strength and percentage elongation at break at different water activities ( aw ) were measured. Films with low amounts of glycerol had lower water vapor and oxygen permeabilities, higher tensile strength and lower elongation at break. Wheat gluten coatings reduced weight loss during two weeks of storage for cherry tomatoes and sharon fruits compared to uncoated controls. A bilayer film of wheat gluten and beeswax significantly lowered weight loss from coated cheese cubes compared to single layer coating of wheat gluten.;

scholarly journals Comparação entre a eficiência estrutural de perfis soldados de aço e perfis de aço formados a frio

2016 ◽  
Vol 12 (3) ◽  
Author(s):  
Uiatan Aguiar Nogueira ◽  
Matilde Batista Melo ◽  
Daniel De Lima Araujo
Keyword(s):  
Bending Strength ◽  
Steel Beams ◽  
Steel Beam ◽  
Structural Elements ◽  
Structural System ◽  
Welded Steel ◽  
Bending Tests ◽  
Structural Efficiency ◽  
Cold Formed Steel

RESUMO: A Análise de elementos estruturais, realizadas durante as etapas de projeto de uma estrutura, é parte fundamental para garantia de bom desempenho e estabilidade do sistema estrutural. Na execução de algumas estruturas, como as coberturas em edificações, é usual o emprego de perfis leves de aço formados a frio devido ao seu baixo peso. Esta pesquisa tem por objetivo avaliar a eficiência estrutural desses perfis quando comparados, por exemplo, aos perfis soldados compactos. Para tanto, foram realizados ensaios de flexão em quatro vigas biapoiadas submetidas a duas forças concentradas, de forma a se obter flexão pura no meio do vão das vigas. Estas foram instrumentadas para a determinação da sua rigidez e da sua resistência à flexão. A principal contribuição deste trabalho é demonstrar a eficiência estrutural de perfis formados a frio em seção caixa submetidos à flexão em comparação com perfis de seção tipo “H” soldados. ABSTRACT: The analysis of structural elements, in a structure’s design, is an essential step to ensure good performance and stability of the structural system. In any types of structures, such as roofing in buildings, it’s usual using cold-formed steel beams due to their small weight. This research seeks to evaluate the structural efficiency of cold-formed steel beams when compared, for example, to compact welded steel beams. Thus, bending tests were performed in four simply supported beams submitted to two concentrated loads, in order to obtain pure flexure at the mid-span of the beams. These beams were instrumented for the determination of their rigidity and bending strength. The results showed that the cold-formed steel beam, box-shaped, presented structural efficiency similar to the welded steel beam “H” shaped.

Bending Strength of Al2O3 Ceramics for Textiles Machinery and Elastic Wave Characteristics by Wavelet Analysis

2007 ◽  
Vol 353-358 ◽  
pp. 345-348
Author(s):  
Ki Woo Nam ◽  
B.G. Ahn ◽  
M.K. Kim ◽  
C.S. Son ◽  
Jin Wook Kim ◽  
...  
Keyword(s):  
Elastic Wave ◽  
Bending Strength ◽  
Test Results ◽  
Composite Ceramics ◽  
Bending Tests ◽  
Three Point Bending ◽  
Wave Signal ◽  
Al2o3 Composite ◽  
Signal Characteristics ◽  
Optimized Conditions

The optimized conditions of pressureless sintering were investigated in order to obtain the bending strength and the elastic wave signal of Al2O3 composite ceramics for textiles machinery. As sintering conditions, a temperature range from 1400°C to 1700°C and time from 30 minutes to 150 minutes were applied. Three-point bending tests were conducted on the sintered materials to obtain the strength property. From the test results, the optimum sintering condition was 1600°C, 100 minutes. Al2O3 composite ceramics showed that the elastic wave signal characteristics had a regular correlativity between the optimum sintering temperature and time as well as the maximum bending strength.

Fabrication of Composite Blocks Containing Alumina Bubble Particles for Porous CBN Abrasive Wheels

2012 ◽  
Vol 499 ◽  
pp. 229-234 ◽  
Author(s):  
Q. Pan ◽  
Wen Feng Ding ◽  
Jiu Hua Xu ◽  
B. Zhang ◽  
H.H. Su ◽  
...  
Keyword(s):  
Fracture Surface ◽  
Dwell Time ◽  
Bending Strength ◽  
Ti Alloy ◽  
Abrasive Wheel ◽  
Bending Tests ◽  
Three Point Bending ◽  
Abrasive Grains ◽  
Alumina Particles ◽  
Vitrified Cbn

Alumina (Al2O3) bubble particles were added into the mixture of CBN abrasive grains, Cu-Sn-Ti alloy and graphite particles to prepare the composite blocks for porous CBN abrasive wheels. The specimens were sintered at the temperature of 920°C for the dwell time of 30 min. The bending strength of the composite blocks was measured by the three-point bending tests. The fracture surface of the blocks was characterized. The results show that, the content of alumina bubble particles does not take significant effect on the mechanical strength of the composite blocks. Even the lowest strength of the composite blocks, 98 MPa, is higher than that of the vitrified CBN abra-sive wheels. Cu-Sn-Ti alloy has bonded firmly alumina particles and CBN grains by means of the chemical reaction and corresponding products. Finally, the chip space was formed through the re-moval of the ceramic wall of the alumina bubble particles within the CBN abrasive wheel during dressing.

scholarly journals Influence of the Infill Orientation on the Properties of Zirconia Parts Produced by Fused Filament Fabrication

Materials ◽  
2020 ◽  
Vol 13 (14) ◽  
pp. 3158 ◽  
Author(s):  
Santiago Cano ◽  
Tanja Lube ◽  
Philipp Huber ◽  
Alberto Gallego ◽  
Juan Alfonso Naranjo ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Bending Strength ◽  
Complex Geometries ◽  
Fused Filament Fabrication ◽  
Moisture Evaporation ◽  
Bending Tests ◽  
Three Point Bending ◽  
Different Types ◽  
Fill Pattern ◽  
The Many

The fused filament fabrication (FFF) of ceramics enables the additive manufacturing of components with complex geometries for many applications like tooling or prototyping. Nevertheless, due to the many factors involved in the process, it is difficult to separate the effect of the different parameters on the final properties of the FFF parts, which hinders the expansion of the technology. In this paper, the effect of the fill pattern used during FFF on the defects and the mechanical properties of zirconia components is evaluated. The zirconia-filled filaments were produced from scratch, characterized by different methods and used in the FFF of bending bars with infill orientations of 0°, ±45° and 90° with respect to the longest dimension of the specimens. Three-point bending tests were conducted on the specimens with the side in contact with the build platform under tensile loads. Next, the defects were identified with cuts in different sections. During the shaping by FFF, pores appeared inside the extruded roads due to binder degradation and or moisture evaporation. The changes in the fill pattern resulted in different types of porosity and defects in the first layer, with the latter leading to earlier fracture of the components. Due to these variations, the specimens with the 0° infill orientation had the lowest porosity and the highest bending strength, followed by the specimens with ±45° infill orientation and finally by those with 90° infill orientation.

Bending strength and failure of single-layer and double-layer sandwich structure with graded truss core

2019 ◽  
Vol 226 ◽  
pp. 111204 ◽  
Author(s):  
Yang Sun ◽  
Li-cheng Guo ◽  
Tian-shu Wang ◽  
Liao-jun Yao ◽  
Xin-yang Sun
Keyword(s):  
Double Layer ◽  
Sandwich Structure ◽  
Bending Strength ◽  
Single Layer ◽  
Truss Core

Effect of Moisture Absorption on the Bending Strength of CFRP

2012 ◽  
Vol 450-451 ◽  
pp. 482-485 ◽  
Author(s):  
A Ying Zhang ◽  
Di Hong Li ◽  
Dong Xing Zhang
Keyword(s):  
Moisture Content ◽  
Composite Laminates ◽  
Immersion Time ◽  
Moisture Absorption ◽  
Bending Strength ◽  
Experimental Results ◽  
Bending Tests ◽  
Three Point Bending ◽  
Damage Propagation ◽  
Effect Of Moisture

The effects of moisture content on the bending strength of T300/914 composite laminates that immersed in water for 7 days and 14 days was discussed in this paper. The three-point bending tests were conducted on the composite laminates. Experimental results reveal that the moisture content in the laminates increased with immersion time and that moisture absorption accelerated damage propagation in the composite laminates. The bending strength of the unaged, aged specimens were characterized and analyzed. Compared to the unaged specimens, the bending strength of the composite laminates immersed for 7 and 14 days decreased by 6.62% and 16.98%, respectively. The results revealed that the bending strength of the aged specimens decreased with the increasing immersion time.

Is Synthetic Composite Bone a Substitute for Natural Bone in Screw Bending Tests?

2011 ◽  
Author(s):  
Thomas P. James ◽  
Brendan A. Andrade
Keyword(s):  
Bone Substitute ◽  
Bending Strength ◽  
Laminated Composite ◽  
Bovine Bone ◽  
Localized Deformation ◽  
Bending Tests ◽  
Natural Bone ◽  
Cortical Screw ◽  
Glass Fiber Reinforced ◽  
Composite Bone

Composite replica bones have been used extensively for biomechanical studies. These studies normally rely upon the overall tensile, compressive, and bending strength of large replica bones, such as the tibia and femur. In this study, highly localized behavior of composite bone was scrutinized by examining the material’s response to cortical screws in bending. Of interest was localized deformation of the composite material as compared to the response of natural bone under similar loading conditions. Cortical screw deflection in a laminated composite bone was compared to deflection in a bovine bone under quasi-static loading. The laminated composite bone consisted of short glass fiber reinforced epoxy as a cortical bone substitute, while polyurethane foam was used as a cancellous bone substitute. A new laser projection method was used to make comparative measurements of the slope of the screw head near to the applied load. Initial results indicate that composite bone is a reliable substitute for natural bone in quasi-static studies of cortical screw deflection.

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