scholarly journals Karakteristik Minyak Ikan Nila (Oreochromis niloticus) Hasil Pemurnian Menggunakan Arang Aktif dan Bentonit pada Hasil Samping Limbah Fillet Ikan Nila PT. Aquafarm Nusantara Semarang

Jurnal Airaha ◽  
2019 ◽  
Vol 8 (02) ◽  
pp. 096-104
Author(s):  
Sumartini ◽  
Supriyanto ◽  
Pudji Hastuti
Keyword(s):  
Fatty Acid ◽  
Melting Point ◽  
Free Fatty Acid ◽  
Moisture Content ◽  
Oreochromis Niloticus ◽  
Parameter Analysis ◽  
Peroxide Number ◽  
Active Charcoal ◽  
Experimental Laboratory ◽  
Iodin Number

PT. Aquafarm Nusantara adalah  industri pengolahan ikan modern berbasis fillet ikan Nila  yang rutin melakukan ekspor ke berbagai negara. Daging ikan Nila merupakan bagian utama yang dijadikan produk fillet ikan dan diekspor, sehingga masih banyak limbah yang dihasilkan seperti tulang, sisik, kulit, isi perut, dan kepala ikan. Penelitian ini bertujuan untuk mengetahui karakteristik dan kualitas minyak ikan dari hasil samping industri fillet ikan nila setelah mengalami pemurnian. The method used was an experimental laboratory using eight different treatments on pale dose (charcoal) 1%, 2%, 3%, bentonite 1%, 2%, 3%, active charcoal 2% : 1%, and bentonite:active charcoal 1%, 2%. Parameters used are moisture content, melting point, free fatty acid, peroxide and iodin value, brightness and clarity. The best result of parameter analysis was showed by combining betonit: actice charcoal (2%:1%), it showed the moisture content 0.05 ± 0,02%, iodin number 121,87±2,55, peroxide number 7,92±0,00%, FFA 0,23±0,05, brightness 55,67±0,09% (L*),-1,09±0,03 (a*), 23,36 ±0.03(b*), and clarity 82,79 ± 0.51%T.

scholarly journals Physiochemical analysis of oil extracted from Vitelleria paradoxa seed obtained from Wukari North Eastern Nigeria

2021 ◽  
Vol 4 (1) ◽  
pp. 059-066
Author(s):  
Azuaga TI ◽  
Azuaga IC ◽  
Okpaegbe UC ◽  
Ibrahim AI ◽  
Manasseh CK
Keyword(s):  
Fatty Acid ◽  
Melting Point ◽  
Free Fatty Acid ◽  
Specific Gravity ◽  
Moisture Content ◽  
Iodine Value ◽  
Oil Recovery ◽  
Acid Value ◽  
Ash Content ◽  
Saponification Value

Soxhlet extraction of oil from seeds of Vitelleria paradoxa was carried out using n-hexane as the solvent. Standards methods were adopted in the analysis of the physiochemical properties; moisture content, melting point, total ash content, pH, specific gravity, iodine value, saponification value, acid value, free fatty acid value and ester value were all evaluated. The oil recovery rate was good with 32.6% yield, moisture content of 3.1%, melting point of 52oC and pH 5.7. Total ash content was 50.3%, specific gravity of 0.9 g/cm3, iodine value 39 mg/L, saponification value 224.6 mgKOH/g, acid value 59.9 mgKOH/g free fatty acid (FFA) 29.9 mgKOH/L and ester value 164.7 mg/L. The results shows that oil from Vitelleria paradoxa seed holds the potentials for wider applications in foods, cosmetics, pharmaceuticals, lubricants and soap making.

scholarly journals Pengaruh Perendaman Kulit Buah Cokelat (Theobroma cacao)Terhadap Kualitas Minyak Goreng Bekas

2020 ◽  
Vol 5 (3) ◽  
Author(s):  
Mulia Aria Suzanni ◽  
Dina Akmila ◽  
Raihanaton Raihanaton ◽  
Rizki Andalia ◽  
Saudah Saudah ◽  
...  
Keyword(s):  
Fatty Acid ◽  
Free Fatty Acid ◽  
Moisture Content ◽  
Water Content ◽  
Natural Antioxidants ◽  
High Water ◽  
Acid Number ◽  
Peroxide Number ◽  
High Water Content ◽  
Waste Oil

The use of waste oil that can cause health problems. The disturbance is caused by the high peroxide number triggered by oxidation and hydrolysis of oil in the presence of free fatty acids and high water content. Reuse of waste oil can be done with several alternatives such as the addition of natural antioxidants or synthesis. This study aimed to determine the effect of soaking wet and dry chocolate fruit on the quality of waste oil. The parameters seen are water content, acid numbers, peroxide numbers and free fatty acid levels. The moisture content was determined by the oven drying method, acid numbers and free fatty acid levels by the alkalimetry titration method, and peroxide number by the iodometry method. The results showed that the waste oil soaked on the exocarp of dried cacao is more optimal in reducing the peroxide number by 38.71%, while soaking with wet exocarp is only 12.14%. Moisture content increased by 0.08% on soaking with the exocarp of dried cacao, whereas wet exsocarp is 1.63%. Acid number increased 17.42% in soaking with the exocarp of dried cacao, whereas wet exocarp is 36%. Free fatty acid levels increased 0.64% in dumping with dried exocarp, while soaking with the exocarp of wet cacao increased by 0.82%.

scholarly journals Kualitas Minyak Bunga Matahari Komersial dan Minyak Hasil Ekstraksi Biji Bunga Matahari (Helianthus annuus L.)

2012 ◽  
Vol 12 (1) ◽  
pp. 59 ◽  
Author(s):  
Dewa G Katja
Keyword(s):  
Fatty Acid ◽  
Free Fatty Acid ◽  
Moisture Content ◽  
Helianthus Annuus ◽  
Peroxide Value ◽  
Sunflower Seed ◽  
Seed Oil ◽  
Helianthus Annuus L ◽  
Sunflower Seed Oil

KUALITAS MINYAK BUNGA MATAHARI KOMERSIAL DAN MINYAK HASIL EKSTRAKSI BIJI BUNGA MATAHARI (Helianthus annuus L.) ABSTRAK Minyak komersial dan minyak hasil ekstrasi dari biji bunga matahari melalui uji kadar air, kadar asam lemak bebas, bilangan peroksida. Analisis hasil ekstrak biji bunga matahari diperoleh kadar air 0,43%, kadar asam lemak bebas 0,47% dan bilangan persoksida 5,22 mek/kg. analisis minyak komersial diperoleh kadar air 0,21%, kadar asam lemak bebas 0,28% dan bilangan peroksida 4,18 mek/kg. Hasil analisis dengan kromatografi gas kedua sampel menunjukkan kadar asam lemak bebas berbeda.       Berdasarkan uji kualitas yang dilakukan terhadap kedua sampel yang dianalisis terdapat hasil yang diperoleh tidak memenuhi syarat yang ditentukan yakni kadar asam lemak bebas 0,08% dan bilangan peroksida 2 mek/kg. Kata kunci: Asam lemak bebas, bilangan proksida, minyak biji bunga matahari  QUALITY OF COMMERCIAL SUNFLOWER OIL AND OIL EXTRACTION SEEDS SUNFLOWER (Helianthus annuus L.) ABSTRACT Experimental study of analyzing the extract oil from sunflower seed compare with the commercial sunflower seed oil according to the company standard which includes determining of moisture content, free fatty acid content, peroxide value and the fatty acids compositions is reported in this paper. The result show that the moisture content of the extract oil is 0,43%, free fatly acid content is 0,47%, and the peroxide value is 5,22% mek/Kg. For the commercial sunflower seed oil company product that is 0,21% for the moisture, free fatty acid is 0,28% and the peroxide value is 4,89 mek/Kg. The gas chromatography analysis indicated that the most fatty acid from both samples is linoleic acid. The quality of the extract sunflower seed oil has not been improved to conform with the commercial quality according to the company standard, that is 0,08% for the free fatty acid and 2 mek/Kg for the peroxide value. Keywords: Free fatty acid, peroxide value, sunflower seeds oil

scholarly journals Perubahan Mutu Minyak Kelapa dan Minyak Sawit Selama Penggorengan

Buletin Palma ◽  
2016 ◽  
Vol 16 (1) ◽  
pp. 1
Author(s):  
STEIVIE KAROUW ◽  
CHANDRA INDRAWANTO
Keyword(s):  
Fatty Acid ◽  
Free Fatty Acid ◽  
Moisture Content ◽  
Palm Oil ◽  
Oil Quality ◽  
Coconut Oil ◽  
Thermal Reactions ◽  
Frying Process ◽  
Fatty Acid Peroxide

<p>Abstrak</p><p>Proses penggorengan akan menyebabkan perubahan mutu minyak akibat reaksi hidrolisis, oksidasi dan proses termal. Penelitian ini bertujuan untuk mengetahui perubahan mutu  minyak kelapa dan minyak sawit selama penggorengan. Minyak kelapa dan minyak sawit masing-masing digunakan untuk menggoreng kentang pada suhu 170°C selama 15 menit. Minyak tersebut digunakan untuk 3 kali penggorengan. Pada akhir penggorengan dilakukan pengambilan sampel minyak untuk dievaluasi kadar air, kadar asam lemak bebas, bilangan peroksida dan bilangan TBA (Tiobarbituric acid). Hasil penelitian menunjukkan bahwa sebelum penggorengan minyak kelapa dan minyak sawit memiliki kadar air yang hampir sama, tetapi kadar asam lemak bebas, angka peroksida dan TBA minyak kelapa lebih rendah dibanding minyak sawit. Selama penggorengan minyak kelapa dan minyak sawit menunjukkan pola perubahan kadar air yang hampir sama. Pada 1 kali dan 2 kali penggorengan kadar asam lemak bebas, angka peroksida dan angka TBA minyak kelapa dan minyak sawit cenderung berfluktuasi. Pada 3 kali penggorengan minyak kelapa memiliki kadar asam lemak bebas,  angka  peroksida  dan  angka  TBA  yang  lebih  rendah  dibandingkan  minyak  sawit.  Hasil  yang  diperoleh menunjukkan   bahwa   minyak   kelapa  lebih   stabil   terhadap   reaksi   oksidasi   dibanding   minyak   sawit   selama penggorengan.</p><p> </p><p>Pattern of Coconut Oil and Palm Oil Quality During Frying</p><p>ABSTRACT</p><p> </p><p>Frying was a process which affected the quality of oil due to hydrolysis, oxidation and thermal reactions. The aim of the research was to study the quality pattern of coconut oil and palm oil quality during frying. The oils were utilized to fry french fries at 170°C for 15 minutes and then used in frying process for 3 times. Samples of oil were taken at the end of each frying period and analyzed for its moisture, free fatty acid, peroxide and TBA (tiobarbituric acid) values. The results showed that, coconut oil and palm oil having similary moisture content before and during frying. Otherwise free fatty acid, peroxide and TBA values at coconut oil lower then palm oil. During 1 and 2 times of frying period these two oils showed fluctuation in free fatty acid, peroxide and TBA values. During 3 times of frying, coconut oil contained free fatty acid, peroxide and TBA value lower than palm oi. Thus, we consider that coconut oil was more stable to oxidation compared to palm oil during frying</p>

CHARACTERISTICS OF CANADIAN LARD

1947 ◽  
Vol 25f (1) ◽  
pp. 63-75 ◽  
Author(s):  
H. J. Lips ◽  
G. A. Grant
Keyword(s):  
Fatty Acid ◽  
Melting Point ◽  
Free Fatty Acid ◽  
Iodine Number ◽  
Fatty Acid Content ◽  
Correlation Coefficients ◽  
Smoke Point ◽  
Storage Life ◽  
Mean Values ◽  
Swift Stability

Mean values for measured properties of 33 samples of lard obtained from 26 packing plants across Canada were: iodine number, 58.7; saponification number, 193.9; melting point, 43.5 °C.; smoke point, 382° F.; colour, 8.8Y, 1.6R; unsaponifiable matter, 0.43%; fatty acid composition: saturated, 45.6%, oleic, 44.7%, linoleic, 8.7%, linolenic, 0.6%, arachidonic, 0.4%; storage life at 26.7 °C., 9.2 weeks; Swift stability, 3.5 hr.; iodimetric peroxide, 1.6 ml. of 0.002 N thiosulphate per gm.; ferrometric peroxide, 9.7 m.e. per kgm.; Kreis test, 9.9; Stamm test, 2.3; alpha-dicarbonyl test, 3.4; free fatty acid, 0.4%; fluorescence, 79.2. The distribution of values is shown by histograms.Simple correlation coefficients computed between measured properties showed the following to be associated: melting point with iodine number; free fatty acid content with melting point, smoke point, and red colour; storage life at 26.7 °C. with log of Swift stability and initial ferrometric peroxide, Kreis, and alpha-dicarbonyl values.

scholarly journals Comparative Analysis of Physico-Chemical Properties of Oil Extract From Two Varieties of Fluted Pumpkin Seeds Using Different Extraction Methods

2018 ◽  
Vol 13 (2) ◽  
pp. 48-60
Author(s):  
M. O. Sunmonu ◽  
E. O. Ajala ◽  
M. M. Odewole ◽  
S. Morrison ◽  
A. M. Alabi
Keyword(s):  
Refractive Index ◽  
Fatty Acid ◽  
Free Fatty Acid ◽  
Moisture Content ◽  
Crude Protein ◽  
Chemical Properties ◽  
Acid Value ◽  
Ash Content ◽  
Crude Fibre ◽  
Mean Values

This study investigates physical and chemical properties two seeds namely Ugba (Telfairia pedata) and Ugwu (Telfairia occidentalis) using soaking soxhlet methods of extraction. The physical properties examined are moisture content, ash content, crude protein, fat and oil, crude fibre and carbohydrates. The chemical properties examined are Acid value (mgKOH/g), saponification value, iodine value, free fatty acid, peroxide and refractive index. Higher mean values of moisture content, ash content, crude fibre and carbohydrates were noticed in Ugwu than in Ugba under soaking method. However, the trend was reversed for crude protein and free fatty acid, in whose case they appear to be higher in Ugba than in Ugwu. For soxhlet method, moisture content, ash content, crude fibre and carbohydrates seems to have higher mean values in Ugwu seed compared to when Ugba seed was used. However, crude protein and fat and oil content were higher using Ugba seed than Ugwu seed oil. For soaking method, Ugba seed seem to produce higher mean values of sap value, iodine value, and refractive index when compared with Ugwu seed. On the other Ugwu, seems to produce acid value, free fatty acid and peroxide value when compared with ugba for soaking method. Using soxhlet apparatus however, Ugba seed produces higher mean values for acid value, sap value, iodine value, and free fatty acid compared to Ugwu. The reverse was the case with peroxide and refractive index, still with soxhlet apparatus.Kathmandu University Journal of Science, Engineering and TechnologyVol. 13, No. 2, 2017, page: 48-60

scholarly journals Penurunan Bilangan Peroksida Dan Asam Lemak Bebas Pada Minyak Jelantah Menggunakan Serbuk Mahkota Dewa

2020 ◽  
Vol 2 (2) ◽  
pp. 83-87
Author(s):  
Mutiara Putri Utami Susanto ◽  
Kenny Kencanawati ◽  
Dwi Tia Septiani ◽  
Sani Nurahayu
Keyword(s):  
Fatty Acids ◽  
Fatty Acid ◽  
Free Fatty Acid ◽  
Free Fatty Acids ◽  
Fatty Acid Analysis ◽  
Peroxide Number ◽  
Cooking Oil ◽  
Used Cooking Oil ◽  
Stirring Time

The study used mahkota dewa as adsorben to decrease of the peroxide number and free fatty acids on the used cooking oil with immersion variations for 2 days dan 3 days and also concentration variations of mahkota dewa 5 % w/v, 10 % w/v, and 20 % w/v. The results of the peroxide analysis test still exceed the required number of SNI namely 10 meq O2/kg and the results of the free fatty acid analysis test in the sample with immersion and stirring time for 2 days and 3 days the concentration of  mahkota dewa 20 % w/v has met the SNI, which is 1.04 % and 0.91%.

scholarly journals Extraction and Comparative Characterization of Oils from Edible Seeds of Glycine max and Sesamum indicum

2021 ◽  
pp. 1-9
Author(s):  
Victor Henry Azubuike Enemor ◽  
Ejike Celestine Orji ◽  
Uchechukwu Chibuzo Ogbodo ◽  
Ogechukwu Frances Nworji ◽  
Chinaza Lucy Ibeneme
Keyword(s):  
Glycine Max ◽  
Fatty Acid ◽  
Melting Point ◽  
Free Fatty Acid ◽  
Specific Gravity ◽  
Seed Oil ◽  
Soybean Seed ◽  
Sesame Seed ◽  
Sesamum Indicum ◽  
Sesame Seed Oil

Aim: The incidence of heart-related disease conditions due to consumption of cholesterol containing oils and the increasing global demand for oil for domestic and industrial purposes have necessitated the need for scientific evaluation of other neglected indigenous plants for potential quality oil yield. This study thus aimed at extracting and comparing physicochemical and nutritional properties of seed oils from Glycine max and Sesamum indicum with a view to diversifying alternative sources of oil to meet teeming industrial and health needs and for food security. Methodology: Solvent extraction method was employed to extract oil from seed samples which were further subjected to estimation of physicochemical indices such as free fatty acid, saponification value, iodine value, peroxide value, specific gravity, refractive index, density, pH, melting temperature and viscosity according to methods described by using titration method. Results: Findings indicated higher saponification (412.33 mgKOH/mg), acid (2.99 mgKOH/g), free fatty acid (1.49 mgKOH/g), viscosity (0.13 Pas) and melting point (5.66 oC) values for sesame seed oil than for soybean seed oil. However, soybean seed oil showed higher density (0.837 g/ml), specific gravity (0.842 Kg/m3), pH (6.21), iodine (47.25 wij’s or g/iodine/g) and peroxide (40.80 mEq/Kg) indices than that obtained for sesame seed oil though mean values were not significantly different. Conclusion: From observed measured parameters, sesame seed may be suitable for industrial purposes such as the production of soap and paint owing to its high saponification, free fatty acid, viscosity and melting point values while soybean seed oil may be excellent source for domestic and nutritional consumption in addition to industrial use.

Influence of Drying Methods on Primary Processing Techniques of Cocoa Beans Based on Free Fatty Acid Content

2019 ◽  
Vol 56 (3) ◽  
pp. 249
Author(s):  
E. Shahanas ◽  
Seeja Thomachan Panjikkaran ◽  
C. L. Sharon ◽  
E. R. Aneena ◽  
B. Suma ◽  
...  
Keyword(s):  
Fatty Acid ◽  
Free Fatty Acid ◽  
Moisture Content ◽  
Free Fatty Acid Content ◽  
Acid Content ◽  
Fatty Acid Content ◽  
Drying Methods ◽  
The Sun ◽  
Cocoa Beans ◽  
Processing Techniques

<p>A systematic study was conducted to standardize the fermentation periods, methods and the performance of drying methods (natural sun drying and artificial oven drying) in the development of free fatty acid content in cocoa beans. Cocoa beans were subjected to different days of fermentation, starting with one day up to seven days and various fermentation methods (basket, heap and sack method). Heap method at seventh day of fermentation attained the best results with maximum per cent of fully fermented beans and lowest free fatty acid content (&lt;1.75%). After fermentation, the cocoa beans were sun-dried and oven dried. The pH of sun dried beans ranged from 4.71 to 5.91, while that of oven dried beans was between 4.53 and 5.89. The sun dried beans contained higher moisture content than artificially oven dried beans and the bean recovery was also more in sun dried beans. The lipase activity prone to free fatty acid formation was higher in oven dried cocoa beans than sun dried beans. However the free fatty acid content was increased in both sun dried and oven dried cocoa beans (1.26 and 1.47%) compared to fermented cocoa beans, but it remains below the permissible limit of 1.75%.</p>

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