scholarly journals Influence of testing environment on static fatigue behavior of a glass and a polycrystalline ceramic

2021 ◽  
Vol 32 (3) ◽  
pp. 56-64
Author(s):  
Sara Fraga ◽  
Gabriel Kalil Rocha Pereira ◽  
Luís Felipe Guilardi ◽  
Liliana Gressler May ◽  
Luiz Felipe Valandro ◽  
...  

Abstract It aims on evaluate the effect of the test environment on static fatigue behavior of lithium disilicate-based (LD), and yttrium oxide-stabilized zirconia (YSZ) ceramics. Specimens of LD (IPS e.max CAD, Ivoclar Vivadent) and YSZ (IPS e.max ZirCAD MO, 3 mol% Y2O3, Ivoclar Vivadent) were randomly allocated into three groups: tested in air, inert (paraffin oil, Sigma Aldrich) or distilled water. The static fatigue test (n=15) was performed using a piston-on-three ball assembly, adapted from ISO 6872, as follows: starting load 100 N for LD and 300 N for YSZ; loading application time set to 1 hour for each loading step; step size of 50 N for LD and 100 N for YSZ, applied successively until fracture. Data from static fatigue strength (MPa) and time to fracture (hours) were recorded. Fractographic analysis was executed. Survival analysis corroborates absence of influence of environment on static fatigue outcomes (fatigue strength, time to fracture and survival rates) for YSZ. For LD, specimens tested in air presented statistically superior survival rate and static fatigue strength (p= 0.025). In regards of time to fracture, LD tested in air were superior than when tested in distilled water (p=0.019) or inert (p=0.017) environments. No statistical differences for Weibull modulus were observed. Failures started on the tensile stress surface. Thus, the test environment did not affect slow crack growth (SCG) mechanisms during static fatigue test of YSZ ceramics, but it plays a significant role for the static fatigue behavior of lithium disilicate-based glass ceramics, indicating a high susceptibility to SCG.

1992 ◽  
Vol 287 ◽  
Author(s):  
W. Braue ◽  
G. D. Quinn

ABSTRACTThe static fatigue behavior of sintered Y2O3/A12O3-fluxed Si3N4 in air is controlled by slow crack growth or creep fracture. Partial devitrification of the amorphous grain boundary phase at 1000°C and 1100°C improves the static fatigue resistance with specimens surviving up to 1500 hrs. during stress rupture experiments. In this study the early stages of partial devitrification during static fatigue testing at 1000°C are investigated by conventional and analytical transmission electron microscopy with emphasis on nucleation and growth of δ-Y2Si2O7 and X1-Y2SiO5 and possible constraints from different stress states. The results show that the stress state does not affect the nature of the secondary phase assemblage. However, the amount of crystallization is higher within the tensile region of the flexural specimens than in areas which experienced compressive stresses.


Ceramics ◽  
2019 ◽  
Vol 2 (3) ◽  
pp. 426-440 ◽  
Author(s):  
Jacques Lamon

SiC-based fibers are sensitive to delayed failure under constant load at high temperatures in air. Static fatigue at intermediate temperatures < 800 °C was attributed to slow crack growth from flaws located at the surface of fibers, driven by the oxidation of free carbon at grain boundaries. The present paper examines the static fatigue behavior of SiC-based Hi-Nicalon fibers at high temperatures up to 1200 °C and Hi Nicalon S fibers at intermediate temperatures (500–800 °C). The degradation of stress- rupture time relation of multifilament tows with increasing temperature was investigated. Predictions of tow lifetime based on critical filament-based model of tow failure were compared to experimental stress-rupture time diagrams. Critical filaments are characterized by strength–probability relation. The critical filament-based model was found to describe satisfactorily the static fatigue behavior of fiber tows at these temperatures. The influence of various factors on lifetime as well as the origins of variability is analyzed.


2010 ◽  
Vol 24 (15n16) ◽  
pp. 2502-2505 ◽  
Author(s):  
MD. SHAMIMUR RAHMAN ◽  
TAKESHI KATSUMA ◽  
DAISUKE YONEKURA ◽  
RI-ICHI MURAKAMI

Titanium alloy has an attractive strength-to-weight ratio and good fatigue properties. However, the titanium alloy has very poor wear resistance, therefore, surface treatments must be considered in order to make the contact parts. Hard thin film deposited by PVD technique is well-known to improve the wear resistance. In this study, chromium nitride ( CrN ) film was applied to titanium alloy and its effect on the fatigue behavior was investigated. Ti -6 Al -4 V alloy was used as a substrate material. The CrN film was deposited by arc ion plating (AIP) method at two different negative bias voltages because the film hardness, crystal orientation and surface morphology were strongly depended on the bias voltage during the deposition. Tension-tension fatigue test and tensile test were carried out to investigate the fatigue properties. As the result, the fatigue strength was influenced by the deposition of the CrN film, especially, the fatigue strength was remarkable decreased by the deposition of the CrN film at high negative bias voltage compared to the uncoated specimen and the deposition of the CrN at low negative bias voltage. The difference of the fatigue strength was also investigated on the basis of crack initiating behavior during fatigue test and tensile test.


2014 ◽  
Vol 627 ◽  
pp. 417-420 ◽  
Author(s):  
Yukio Miyashita ◽  
Hugo Inzunza ◽  
Adrian Elizondo ◽  
Yoshiyuki Murayama ◽  
Yuichi Otsuka ◽  
...  

Fatigue behavior of Mg-Al-Ca-Mn alloy with T6 treatment was studied at room temperature and 150°C by conduction rotating bending fatigue test. Fatigue strength at high temperature was lower than that at room temperature in the alloys with and without heat treatment. However, degradation of fatigue strength at high temperature in the T6 treated alloy was not significant compared to the as-extruded alloy. Fatigue crack initiation and propagation behavior was observed with replication technique by conducting interrupted fatigue test at room temperature and 150°C. Multiple cracking was significantly observed at 150°C in both as-received and T6 treated alloys. Change in grain size and randomization of crystal orientation due to the heat treatment could affect the fatigue property.


1982 ◽  
Vol 22 (03) ◽  
pp. 420-428 ◽  
Author(s):  
M. Hanzawa ◽  
H. Yokota ◽  
Y. Toda ◽  
K. Yokoyama

Abstract Factors influencing tensile fatigue strength of 50-mm wire ropes were investigated with a wire-breakage detecting system. The fatigue strength increased with an increase in wire strength and diameter and a decrease in self-rotativity of ropes. The epoxy resin was satisfactory as a socketing material. Introduction More and more offshore oil wells are being drilled in deeper waters. For the purpose of economy, offshore structures for deepsea use, such as the tension leg platform (TLP) and guyed tower, are moored by wire ropes. The wire ropes used in such applications directly receive the loads repeatedly applied by waves and tides. Therefore, the fatigue behavior of wire rope is an important factor in the design of such offshore structures. Wire ropes are used also for long-span suspension bridges such as those being constructed to connect Honshu and Shikoku in Japan. In such bridges, the fatigue strength does not cause problems for main cables receiving little live load, but it is important for hanger ropes on which bridge traffic imposes much live load. Thus, there is a strong demand to determine fatigue characteristics and clarify fatigue behavior in relation to tensile breaking load of such large-diameter wire ropes-i.e., size range of 85, 130, and 180 mm.Most conventional wire rope fatigue data have been obtained by bending tests. Few tensile fatigue test data are available, and those are mainly for small-diameter wireropes (6.4 and 12.7 mm).Few reports have been made for larger-diameter wire ropes and the fatigue tests conducted have given no specific definition of fatigue life. The best attempt has been visual examination of broken wire in the outermost layer of the wire rope. In the fatigue test of large-diameter wire ropes comprising a large number of wires, however, wire breakage does not always occur in the outermost layer, but can take place in the inner layers and even in sockets under certain conditions. To determine the fatigue strength of large-diameter wire ropes exactly, therefore, it is necessary to detect wire breakage during the fatigue test and thereby determine fatigue life.It was against such a background that a device for detecting wire breakage in wire rope being fatigue tested was developed by making use of acoustic emission (AE) and an accelerometer. With this device, tensile fatigue tests have been conducted on various kinds of 50-mm-diameter wire ropes that were similar to practical wire rope in construction and strength. A study comparing test results was conducted on factors affecting the fatigue strength of large-diameter wire ropes, along with an investigation on socketing materials having high fatigue performance. Experimental Procedure Commercial large-diameter wire ropes are manufactured with many diameters - e.g., hanger ropes for long-span suspension bridges are 85 mm, those for guyed towers are 130 mm, and those for TLP's are 180 mm. To test full-size wire ropes, a fatigue-testing machine should have a capacity of more than 4 MN.Only a 2-MN fatigue-testing machine was available, so the maximum testable nominal diameter was 50 mm. Therefore, wire ropes having a 50-mm nominal diameter were prepared with wires having the same strengths and similar constructions as those of full-size commercial wire ropes. Table 1 lists the specifications of the fatigue-tested wire ropes. Ropes 9S6, 9SL6, 6S7, and 6S8 are of the center-fit-rope-core (CFRC) type for hanger-rope use. SPEJ p. 420


2021 ◽  
Vol 5 (3) ◽  
pp. 67
Author(s):  
Jacques Lamon ◽  
Adrien Laforêt

The present paper investigates the static fatigue behavior of Hi-Nicalon fiber-reinforced SiC–SiC minicomposites at high temperatures in the 900–1200 °C range, and under tensile stresses above the proportional limit. The stress–rupture time relation was analyzed with respect to subcritical crack growth in filaments and fiber tow fracture. Slow crack growth from flaws located at the surface of filaments is driven by the oxidation of free carbon at the grain boundaries. Lifetime of the reinforcing tows depends on the statistical distribution of filament strength and on structural factors, which are enhanced by temperature increase. The rupture time data were plotted in terms of initial stresses on reinforcing filaments. The effect of temperature and load on the stress–rupture time relation for minicomposites was investigated using results of fractography and predictions of minicomposite lifetime using a model of subcritical growth for critical filaments. The critical filament is the one whose failure by slow crack-growth triggers unstable fracture of the minicomposite. This is identified by the strength–probability relation provided by the cumulative distribution function for filament strength at room temperature. The results were compared to the fatigue behavior of dry tows. The influence of various factors related to oxidation, including multiple failures, load sharing, and variability, was analyzed.


1992 ◽  
Vol 287 ◽  
Author(s):  
Chih-Kuang Jack Lin ◽  
Michael G. Jenkins ◽  
Matitison K. Ferber

ABSTRACTTensile fatigue behavior of a hot-isostatically-pressed (HIPed) silicon nitride was investigated over ranges of constant stresses, constant stress rates, and cyclic loading at 1150-1370°C. At 1150°C, static and dynamic fatigue failures were governed by a slow crack growth mechanism. Creep rupture was the dominant failure mechanism in static fatigue at 1260 and 1370°C. A transition of failure mechanism from slow crack growth to creep rupture appeared at stress rates ≤10−2 MPa/s for dynamic fatigue at 1260 and 1370°C. At 1 150-1370°C, cyclic loading appeared to be less damaging than static loading as cyclic fatigue specimens displayed greater failure times than static fatigue specimens under the same maximum stresses.


Author(s):  
Burçin Arıcan ◽  
Ayfer Atav Ateş

The aim of this study was to compare the cyclic fatigue resistance (CFR) of PathFile (Dentsply Sirona, Ballaigues, Switzerland) and ScoutRace (FKG Dentaire, La Chaux-de-Fonds, Switzerland) glide path files which were either new or previously used. Forty PathFile (PF) 19/.02 and 40 ScoutRace (SR) 20/.02 instruments were used for this study. Half of the files in each group were used (PF-U and SR-U) in the 3D demo tooth models (FKG Dentaire, La Chaux-de-Fonds, Switzerland) for creating glide paths, while the other half was new (PF-N and SR-N) and directly subjected to the cyclic fatigue test. The new and used files (n=80) were rotated in the cyclic fatigue test device with an artificial stainless-steel canal (60° curvature, 5 mm radius 1.5 mm width and 3.0 mm depth) under the continuous irrigation with distilled water at 37°C until fracture occurred. Time to fracture was recorded and the Weibull reliability analysis was performed. Data were statistically analysed. Conformity to normal distribution was examined using the Shapiro-Wilk test. A paired two-sample t-test was used to compare the TTF values according to the time within the groups. The new instruments (PF-N and SR-N) showed better CFR than the used groups (PF-U and SR-U) (P<0.05). The TTF values of PF were statistically higher than SR in both new and used groups (P<0.05). The predicted time for %99 survival for the files was PF-N> SR-N>PF-U >SR-U. Reuse of both glide path instruments reduced the time to fracture and the cyclic fatigue resistance of the files.


2013 ◽  
Vol 27 (19) ◽  
pp. 1341027
Author(s):  
YU-HENG LU ◽  
XUAN YE ◽  
LEI HU ◽  
FEI LUO ◽  
ZHI-YU XIAO

Fe -2 Cu -2 Ni -1 Mo -1 C powder metallurgy material was fabricated by die-wall lubricated warm compaction and ultrasonic fatigue test was carried out for as-sintered and heat treatment samples. Material fatigue strength reaches 249 MPa under axial fatigue testing. The sintered material consists of acicular martensite, pearlite, bainite and retained austenite. Tempered martensite is the major phases after heat-treatment. Cleavage plane and dimples is mixed fracture for sample after axial fatigue test. Mechanical properties of after heat treatment materials are improved and fatigue strength reaches 382 MPa under 107 cycles in bending ultrasonic fatigue test. The fatigue strength increases significantly in high cycles range.


1993 ◽  
Vol 333 ◽  
Author(s):  
Masamichi Obata ◽  
Akira Honda ◽  
Hirohisa Ishikawa ◽  
Tadashi Mano

ABSTRACTStatic fatigue behavior is one of the important factors for life prediciton of ceramic materials. In this study, SCG (slow crack growth) parameters were measured under atmosphere conditions, and the static fatigue behavior of alumina, PSZ (partially stabilized zirconia), and titanium oxide was examined.According to the results of the evaluatin of the static fatigue behavior, the destruction probability after 1,000 years would be less than 1/40,000 when tensile stresses occurring in the material were less than 79.4, 241.3, 8.0 MPa for alumina, PSZ, and titanium oxide, respectively. However titanium oxide could not be used because of the wall thickness that would be needed to accomplish this stress. The life prediction method includes only tht effect of preexisting flaws so the method to estimate the effect of localized corrosion is required for the future examination of the application of ceramic materials.


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