scholarly journals  Evaluation of caraway essential oil from different production areas of Serbia

2014 ◽  
Vol 41 (No. 3) ◽  
pp. 122-130 ◽  
Author(s):  
M.G. Aćimović ◽  
S.I. Oljača ◽  
V.V. Tešević ◽  
M.M. Todosijević ◽  
J.N. Djisalov

Caraway fruits contain essential oils that give caraway its characteristic aroma. This paper evaluates quantity and composition of the essential oil from the annual caraway grown in different production areas of Serbia. Experiments were conducted in three production areas: Banat, Bačka and Srem, during two years. The fruits contained 3.95% of oil on average. The highest content of essential oil was obtained in the production area of Banat, a part of Serbia where environmental conditions are very favourable for cultivation of medicinal plants. Weather conditions have not a significant influence on the content of essential oil in caraway fruits. However, weather conditions as well as production region had a great influence on seed yield and essential oil yield. There were 22 compounds determined in caraway essential oil by GC/MS. The main components were carvone and limonene, whose mixture constituted from 97.69 to 98.62% of total oil composition. Carvone/limonene ratio was 0.58% on average, therefore, it can be concluded that this annual caraway belongs to limonene chemotype.  

2016 ◽  
Vol 11 (10) ◽  
pp. 1934578X1601101
Author(s):  
Kaan Polatoğlua ◽  
Betül Demirci ◽  
İhsan Çalιş ◽  
Kemal Hüsnü Can Başer

The essential oil of aerial parts of Helichrysum conglobatum (Viv.) Steudel. (Asteraceae) from Cyprus was analyzed by GC and GC-MS. The essential oil yield was 0.01, v/w. Forty five compounds were identified in the oil comprising 96.1% of the total. The essential oil was mainly composed of sesquiterpene type compounds and oxygenated sesquiterpene derivatives. The main components of the oil were β-caryophyllene (14.6%), γ-curcumene (14.1%), hexadecanoic acid (13.5%), tetradecanoic acid (7.5%), rosifoliol (5.4%) and δ-cadinene (5.3%). This is the first report on the essential oil composition of H. conglobatum from Cyprus.


2012 ◽  
Vol 7 (9) ◽  
pp. 1934578X1200700 ◽  
Author(s):  
Megil J. McNeil ◽  
Roy B. R. Porter ◽  
Lawrence A. D. Williams

The chemical composition of the essential oil obtained from the aerial parts of Cleome serrata by hydrodistillation was analyzed by employing GC-FID, GC-MS and RI. Fourteen compounds comprising 90.4% of the total oil composition were characterized. The main components identified were ( Z)-phytol (53.0%) and di(2-ethylhexyl)-phthalate (DEHP) (14.7%). The oil was evaluated for its in vitro antimicrobial activities against nine pathogenic microorganisms using the filter paper disc diffusion method. Moderate antimicrobial activity was observed against five of the pathogens assayed. In addition, the essential oil was tested against the sweet potato weevil, Cylas formicarius elegantulus. Strong knockdown insecticidal activity was observed.


HortScience ◽  
2013 ◽  
Vol 48 (11) ◽  
pp. 1393-1396 ◽  
Author(s):  
Valtcho D. Zheljazkov ◽  
Tess Astatkie ◽  
Barry O'Brocki ◽  
Ekaterina Jeliazkova

Anise (Pimpinella anisum L.) is a spice, an essential oil crop, and a medicinal plant with a long history of use. Anise seed oil is extracted from anise seed through steam distillation. There is no experimentally established optimal time for distillation of anise seed. We hypothesized that the distillation time (DT) can be customized for optimum yield and composition of anise essential oil. In this study, we determined the effect of nine steam DTs (5, 15, 30, 60, 120, 180, 240, 360, and 480 minutes) on essential oil yield and essential oil composition of anise seed. We developed regression models to predict essential oil yield, the concentration of individual constituents, and the yield of these constituents as a function of DT. Highest essential oil yield (2.0 g/100 g seed, 2%) was obtained at 360-minute DT. The concentration of transanethole, the major anise oil constituent, varied from 93.5% to 96.2% (as a percent of the total oil) and generally was high at 15- to 60-minute DT and low at 240- to 480-minute DT. However, the yield of transanethole (calculated from the essential oil yield and the concentration of transanethole in the oil) increased with increasing DT to reach maximum at 360-minute DT. The concentration of the other oil constituents varied significantly depending on the DT, and some of them were higher at the shorter DT than at the longer DT. However, the yields of these constituents were highest at longer DT (either 360 or 480 minutes). DT can be used to obtain anise essential oil with different composition that would benefit the essential oil industry. This study demonstrated the need for providing DT in reports where anise seed essential oil yield and composition are discussed. This article can also be used as a reference point for comparing studies in which different DTs were used to extract essential oil from anise seed.


Author(s):  
Erman Duman ◽  
Mehmet Musa Özcan ◽  
Zrira Saadiab ◽  
Mustafa Mete Özcan

The chemical composition of essential oil, which is isolated by hydrodistillation of aerial parts of Thymus zygioides growing wild in Turkey, have been determined by GC and GC/MS. Essential oil yield on a dry weight basis of aerial parts from T. zygioides was 0.45%. A total of twenty two constituents were identified by GC-MS analyses, the main components representing 92.3% the oil was identified as limonene (24.11%), cis-linalool oxide (22.91%), eucalyptol (8.65%). 3-octonol (7.04%), nerol (4.47%) geranyl acetate (3.19%), carvacrol (2.74%), linalyl propanoate (2.95%) and sabinene (2.23%). The essential oil of T. zygioides was characterized by its high content of limonene (24.11%).


2012 ◽  
Vol 57 ◽  
pp. 71-76 ◽  
Author(s):  
Gjoshe Stefkov ◽  
Ivana Cvetkovikj ◽  
Marija Karapandzova ◽  
Svetlana Kulevanova

The main objective of this study was to analyze and identify the essential oil composition of S. officinalis populations growing in Republic of Macedonia and to evaluate these data according to different standards’ requirements for, commercially most utilized, Dalmatian sage. The essential oil yield, obtained after hydrodestilation from leaves, of three different populations of Salvia officinalis L. from Republic of Macedonia was determined, varying from 1.40 to 3.46%. The GC/FID/MS analysis of the composition of the essential oils revealed 63, 57 and 51 components in Galicica Mtn., Jablanica Mtn. and Karaorman Mtn. sage populations, respectively. The main components of the oil, in all three samples, were the terpene hydrocarbons, encompassing the monoterpenes: camphor (13.15 - 25.91%), α-thujone (19.25 - 26.33%), β-thujone (2.03 - 5.28%), 1,8-cineole (6.51 – 13.60%), α-pinene (0.93 – 1.47%), borneol (1.07 – 4.67%), then sesquiterpenes: trans (E)-caryophyllene (1.72 – 5.33%), α-humulene (2.89 – 7.99%), viridiflorol (4.27 – 7.99%), and the diterpene manool (2.13 - 3.79%). Thus, our results for the essential oil composition of sage complied with the reference values specified in the DAC 86 monograph for Salvia essential oil.


2015 ◽  
Vol 43 (2) ◽  
pp. 432-438 ◽  
Author(s):  
Aneta WESOŁOWSKA ◽  
Monika GRZESZCZUK ◽  
Dorota JADCZAK ◽  
Paweł NAWROTEK ◽  
Magdalena STRUK

The chemical composition of the essential oils obtained by hydrodistillation from the aerial parts of Thymus serpyllum and Thymus serpyllum‘Aureus’ has been investigated by gas chromatography-mass spectrometry (GC-MS). Forty-seven compounds (99.67% of the total oil) wereidentified in the essential oil of T. serpyllum. The main components found in the oil were carvacrol (37.49%), -terpinene (10.79%), -caryophyllene (6.51%), p-cymene (6.06%), (E)--ocimene (4.63%) and -bisabolene (4.51%). Similarly, carvacrol (44.93%), -terpinene(10.08%), p-cymene (7.39%) and -caryophyllene (6.77%) dominated in the oil of T. serpyllum ‘Aureus’. A total of forty three compounds wereidentified in this oil, representing 99.49% of the total oil content. On the basis of the obtained data it was proved that the content of 1-octen-3-ol,eucalyptol, (Z)--ocimene, (E)--ocimene, -terpinene, carvacrol methyl ether, germacrene D and -bisabolene was significantly higher for T.serpyllum while T. serpyllum ‘Aureus’ was characterized by a significantly higher content of 3-octanone, 3-octanol, p-cymene, borneol andcarvacrol. The isolated essential oils were evaluated for their antimicrobial activity against nine reference strains (Escherichia coli, Staphylococcusaureus, Staphylococcus epidermidis, Streptococcus agalactiae, Enterococcus faecalis, Bacillus cereus, Micrococcus luteus, Proteus vulgaris and Candidaalbicans) by the microdilution technique. Based on this test, the minimum inhibitory concentrations (MIC) of essential oil were calculated. Thevolatile oil obtained from T. serpyllum showed the highest antimicrobial activity relative to the strain of E. coli (MIC=0.025 μL/mL) and to theyeast C. albicans (MIC=0.05 μL/mL). Similarly, a significant antimicrobial activity exhibited T. serpyllum ‘Aureus’ essential oil, although the MICvalues obtained in that case for E. coli and C. albicans strains were twice as high and were respectively 0.05 μL/mL and 0.1 μL/mL.


2011 ◽  
Vol 6 (2) ◽  
pp. 1934578X1100600
Author(s):  
Milica Pavlović ◽  
Silvana Petrović ◽  
Marina Milenković ◽  
Maria Couladis ◽  
Olga Tzakou ◽  
...  

The essential oil obtained by hydrodistillation from the roots of Anthriscus nemorosa (Bieb.) Sprengel (Umbelliferae) was analyzed by GC and GC-MS. Among sixty-two compounds identified (representing 89.0% of the total oil), the main components were: n-nonane (12.1%), n-hexadecanol (6.9%), δ-cadinene (6.4%), β-pinene (6.0%) and germacrene D (5.4%). Furthermore, the antimicrobial activity of the oil was evaluated against the Gram-positive bacteria Staphylococcus epidermidis (ATCC 12228) and Bacillus subtilis (ATCC 6633), the Gramnegative bacterium Escherichia coli (ATCC 25922), and a yeast Candida albicans (ATCC 10259 and ATCC 24433) using the broth microdilution method.


2010 ◽  
Vol 5 (1) ◽  
pp. 1934578X1000500 ◽  
Author(s):  
Anne Orav ◽  
Janne Sepp ◽  
Tiiu Kailas ◽  
Mati Müürisepp ◽  
Elmar Arak ◽  
...  

Variations in the essential oil composition of aerial parts of pineapple weed (Chamomilla suaveolens (Pursh) Rydb.) growing wild in Estonia, were determined using GC/FID and GC/MS. Forty-four components were identified, representing over 90% of the total oil. Nine compounds have not been mentioned in the literature before. The principal biologically active compounds in C. suaveolens oils were (Z)-en-yne-dicycloether (17.0 – 40.7%), (E)-β-farnesene (19.5– 32.2%), geranyl isovaleriate (8.4 –18.4%), palmitic acid (0.3 – 9.4%) and myrcene (1.1 – 7.9%). The investigation seems to approve the benefit of using aerial parts of pineapple weed as the substitute for flowers.


2011 ◽  
Vol 76 (4) ◽  
pp. 523-528 ◽  
Author(s):  
Ram Verma ◽  
Rajendra Padalia ◽  
Chandan Chanotiya ◽  
Amit Chauhan ◽  
Anju Yadav

Hydrodistilled essential oil of the aerial parts of Laggera crispata (Vahl) Hepper & Wood, collected from the Kumaon region of the western Himalayas was analysed by gas chromatography and gas chromatography-Mass Spectrometry. Eighty constituents, accounting for 83.9 % of the total oil composition, were identified. The oil was mainly dominated by sesquiterpenoids (45.3 %) and benzenoid compounds (33.9 %). Among them, 2,5-dimethoxy-p-cymene (32.2 %), 10-epi-?-eudesmol (14.7 %), ?-caryophyllene (6.9 %), and caryophyllene oxide (5.4 %) were major components of the oil.


2007 ◽  
Vol 2 (1) ◽  
pp. 1934578X0700200 ◽  
Author(s):  
Hossein Nazemiyeh ◽  
Seied M. Razavi ◽  
Abbas Delazar ◽  
Rogaieh Hajiboland ◽  
Valiollah Mozaffarian ◽  
...  

The composition of the essential oils of the umbels and fruit of Prangos uloptera, an indigenous Iranian medicinal plant, was determined by GC-MS analyses. A total of 10 and 18 compounds were identified, respectively, from the essential oils of the umbels and the fruit. The identified compounds represented, respectively, 93.2% and 83.0% of the total essential oils. While the main components of the umbels oil were α-pinene (31.78%), β-bourbonene (15.9%), α-curcumene (10.65%), spathulenol (9%) and m-cymene (5.51%), those of the fruit oil were α-pinene (14.98%), β-bourbonene (7.81%), α-humulene (7.74%), germacrene B (7.23%) and n-tetracosane (6.65%).


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