Evaluation of Mechanical and Wear Properties of Ceramic and Inorganic compounds based Composite via PM route and Optimization through Robust design technique
Abstract The present research study investigates the Mechanical, Physical, and Tribological properties of powder metallurgy (PM) produced AA6063 alloy reinforced with silicon nitride (Si3N4) and copper nitrate (CuN2O6). Incorporation of Si3N4 & CuN2O6 reinforcement in matrix material ranged from 6 to 12 % Si3N4 in a 6-step interval and 2 to 6 %CuN2O6 in a two-step interval. The characterizations were made on the PM-produced specimens using OM, EDS, XRD, and Hardness. The reinforcement particles were uniformly distributed, which was attributed to a homogeneous mixer of matrix and reinforcements. The test findings show that as the reinforcing percentage of the ceramic and inorganic compound increases, properties such as hardness and density rise considerably and monolithically. The existence of phases such as Si3N4 and CuN2O6 reinforcement in the AA6063 matrix was ensured by X-ray diffraction. The hardness of AA6063/12%Si3N4/6%CuN2O6 increased by 88% over the base alloy due to a mismatch in thermal expansion between the Al matrix and reinforcement, which causes massive internal stress, causing the aluminium matrix to plastically deform to accommodate the reduced volume expansion of Si3N4 and CuN2O6 particles. The dry sliding wear test was determined using the Pin-on-Disc method, and the results show that the composite is more wear-resistant. An orthogonal array and analysis of variance were utilized to evaluate the solution, including parameters using the Taguchi robust design technique. The weight percentage of the Si3N4/CuN2O6 compound and the relationship between weight % of reinforcement and applied load had the most significant impact on composite wear resistance. The produced composite's wear morphology was studied using images from a scanning electron microscope and energy dispersive spectroscopy.