scholarly journals Physicochemical Characterization of Cattle Dung Fibre Under the Hydrothermal Process

2021 ◽  
Author(s):  
Vinayak Fasake ◽  
Perminder Jit Kaur ◽  
Kavya Dashora
Keyword(s):  
Hydrothermal Treatment ◽  
Incubation Time ◽  
Hydrothermal Process ◽  
Physicochemical Characterization ◽  
Physicochemical Analysis ◽  
Added Value ◽  
Cattle Dung ◽  
Cow Dung ◽  
X Ray Crystallography ◽  
Different Temperatures

Abstract Cattle dung fibre is a lignocellulosic material abundant and sustainable non-wood source of polymeric components, which can be converted into high added-value products. Hydrothermal treatment of the fibre obtained from cow dung was explored using four different temperatures (120, 140, 160 and 180 ◦C) and incubation times (0 and 120 minutes) at a fixed material to water ratio (1:10). The present study resulted in the highest yield of 94% (w/w) that gradually decreased with temperature and incubation time. The physicochemical analysis revealed that hydrothermal treatment resulted in high cellulose, low lignin, and ash content (51.6%, 30.93%, and 6.3%, respectively) at 160◦C for 2 hr incubation time and was appropriate for pulp and paper production. The SEM and X-ray crystallography indicates the treatment resulted in separated fibrils and a porous structure. Both FTIR studies and chemical characterisation techniques were used to optimize the temperature and duration of hydrothermal treatment. Overall, the study presents the first report on the extraction of fibres from cow dung and their hydrothermal treatment. In perspective, it is possible to achieve the properties required for its industrial-scale conversion to eco-friendly papers by heating the fibre under controlled conditions.

scholarly journals Alkali-Hydrothermal Treatment of K-Rich Igneous Rocks for Their Direct Use as Potassic Fertilizers

Minerals ◽  
2021 ◽  
Vol 11 (2) ◽  
pp. 140
Author(s):  
Aaron Mbissik ◽  
Abdellatif Elghali ◽  
Muhammad Ouabid ◽  
Otmane Raji ◽  
Jean-Louis Bodinier ◽  
...  
Keyword(s):  
Hydrothermal Treatment ◽  
Inductively Coupled Plasma ◽  
Structural Changes ◽  
Raw Materials ◽  
Hydrothermal Process ◽  
Atomic Emission ◽  
Igneous Rocks ◽  
Gravimetric Analysis ◽  
African Countries ◽  
Naoh Solution

Due to the increasing demand for conventional sources of potassium (K) and their inaccessibility by African countries, K-rich igneous rocks are increasingly studied as potential alternative sources. In this study, six potassic igneous rocks (syenites and trachytes) from the Tamazeght, Jbel Boho, Ait Saoun, and El Glo’a regions (Morocco) were sampled and characterized. Then they were hydrothermally treated to enhance their K release for potential use as potassic fertilizers. The raw materials are mainly formed by microcline (up to 74%), orthoclase (20–68%), albite (36–57%), biotite-muscovite (15–23%), and titanite, calcite, hematite, and apatite as accessory minerals. These samples were crushed and milled to reach a particle size <150 µm and mixed with 4 N NaOH solution in an autoclave. The liquid/solid (L/S) ratio was about 44 mL/50 g. The powders were allowed to react with the solution at 170 °C for 7 h. For all tests, NaOH reacted completely with the powders and no liquid was observed after the treatment. X-ray diffraction (XRD), thermal gravimetric analysis (TGA), infrared spectroscopy (IRTF), and scanning electron microscopy (SEM-EDS) were carried out on treated samples to characterize the mineralogical and structural changes due to the alkali-hydrothermal treatment. Indeed, the treated samples revealed the presence of sodic neoformed phases such as thermonatrite, sodalite, analcime, and cancrinite. The treated material was leached for a week using deionized water and the elements released were measured using inductively coupled plasma–atomic emission spectroscopy (ICP-AES). The hydrothermal process showed a strong effect on structure breakdown as well as on the release of K and other nutrients such as P, Fe, Si, Mg, and Ca. Therefore, the alkali-hydrothermal treatment allowed the release of 50.5 wt% K. Moreover, the release of Mg, Ca, Fe, P, K, and Si were significantly increased. Mg, Ca, Fe, P, K, and Si release within raw materials was about (0.5–3.6), (3.5–31.4), (0.01–0.4), (0.01–0.3), (20–55), and (4.6–8) mg/kg, respectively, whereas treated samples showed a higher release of these elements. Quantitatively, Mg, Ca, Fe, P, K, and Si releases were about (10–11.8), (60–70), (7–20), (1.2–15), (218–1278), and (1119–2759) mg/kg, respectively. Consequently, the treated igneous rocks (syenite and trachyte) could be directly used as potassic fertilizers that would also be a source of other nutrients.

Ability of Inactivated Yeast Powder To Adsorb Patulin from Apple Juice

2012 ◽  
Vol 75 (3) ◽  
pp. 585-590 ◽  
Author(s):  
CAIXIA GUO ◽  
TIANLI YUE ◽  
SHAIMAA HATAB ◽  
YAHONG YUAN
Keyword(s):  
Incubation Time ◽  
Apple Juice ◽  
Incubation Temperature ◽  
Absolute Ethyl Alcohol ◽  
Initial Concentration ◽  
Different Temperatures ◽  
Yeast Powder ◽  
Commercial Yeast ◽  
The Stability ◽  
Phosphate Buffered Saline

This study aimed to investigate the adsorption of patulin from apple juice, using two types of inactivated yeast powder: laboratory-prepared yeast powder (LYP) and commercial yeast powder (CYP). The effects of incubation time, pH, incubation temperature, adsorbent amount, and initial concentration of patulin and the stability of the yeast-mycotoxin complex were assessed. The results showed that the efficiencies of the two yeast types in adsorbing patulin were similar. The ability of the powders to remove patulin increased with longer incubation times, and patulin concentration was below detectable levels with LYP and CYP at approximately 36 and 30 h, respectively. The highest removal of patulin was achieved at pH 5.0 for both powder types, and there were no significant differences in patulin decrease at different temperatures (4, 29, and 37°C). Additionally, the adsorption percentage of patulin increased significantly with the increase of absorbent amount and decrease of initial concentration of patulin. Stability of the yeast-patulin complex was assessed, and patulin was more stable when washed in phosphate-buffered saline (pH 4.0) than in absolute ethyl alcohol. These results suggest that inactivated yeast powder has potential as a novel and promising adsorbent to bind patulin effectively.

scholarly journals Heat Exchanger for Bio-Digester under Thermophilic Range

2019 ◽  
Vol 5 ◽  
pp. 79-88
Author(s):  
Prajwal Sapkota ◽  
Laxman Poudel
Keyword(s):  
Heat Exchanger ◽  
Anaerobic Digestion ◽  
Heat Exchangers ◽  
Heating System ◽  
Gas Production ◽  
Cow Dung ◽  
Digestion Rate ◽  
Digestion Process ◽  
Different Temperatures ◽  
Long Time

Bio-gas has been one of the sources of renewable energy and has been used from long time. It is produced by the anaerobic digestion or decomposition of organic compounds and has different process. The digestion process is carried out by bacteria present in the waste and it is highly dependent on the bacteria which work differently on different temperatures. The rate of anaerobic digestion is highest at hemophilic temperature (55°C). Similarly, it is moderate at mesophilic temperature (35°C) and is lowest at psychrophilic (below 20°C). Thus, to attain the highest digestion rate a thermophilic heating system has beend eveloped. The heating system uses five heat exchangers to heat the influent at digester which is of 35m3 volume, to maintain temperature at 56°C. The volume of bio-gas production from this system which uses cow dung as digestingmaterial is about 28 m3 per day.

scholarly journals Sensory and Physicochemical Characterization of Sourdough Bread Prepared with a Coconut Water Kefir Starter

Foods ◽  
2020 ◽  
Vol 9 (9) ◽  
pp. 1165 ◽  
Author(s):  
Mansi Limbad ◽  
Noemi Gutierrez Maddox ◽  
Nazimah Hamid ◽  
Kevin Kantono
Keyword(s):  
Lactic Acid ◽  
Shelf Life ◽  
Starter Culture ◽  
Physicochemical Characterization ◽  
Physicochemical Analysis ◽  
Starter Cultures ◽  
Coconut Water ◽  
Sensory Profile ◽  
Sourdough Bread ◽  
Water Kefir

There is a recognized need for formulating functional food products using selected lactic acid bacteria (LAB) starter cultures from various sources such as kefir, yoghurt or kombucha that have health benefits. The principle objective of this study was to investigate the use of a coconut water kefir-based fermentation starter culture using Lactobacillus fermentum and Lactobacillus plantarum to develop a sourdough bread. Check-all-that-apply (CATA) sensory profiling was used in this study to evaluate the sensory profile of sourdough breads that varied with culture type, culture concentrations, with and without added yeast, and with fermentation for 18 and 24 h. Based on correspondence analysis (CA) of the CATA results, bread samples with positive sensory attributes were chosen for further physicochemical analysis. Physicochemical analyses (texture, proximate composition, shelf life, carboxylic acid analysis and amino acid analysis) were carried out on breads formulated with starter culture concentrations of 8.30 log CFU/mL of L. fermentum, 4.90 log CFU/mL of L. fermentum and 9.60 log CFU/mL of L. plantarum, each fermented for 24 h without baker’s yeast. The bread sample that was formulated with a coconut water kefir (CWK) starter culture containing 9.60 log CFU/mL of L. plantarum, without dry yeast and fermented for 24 h, had significantly higher values for almost all amino acids and a lower protein content compared to samples formulated using CWK cultures containing 8.30 log CFU/mL of L. fermentum and 4.90 log CFU/mL of L. fermentum, both without dry yeast and fermented for 24 h. The bread sample formulated with CWK starter culture containing 9.60 log CFU/mL of L. plantarum, without dry yeast and fermented for 24 h, also produced significant quantities of organic acids (pyruvic acid, acetic acid, lactic acid and succinic acid). These changes in the physicochemical properties can improve overall bread quality in terms of flavor, shelf life, texture and nutritional value.

scholarly journals Influence of Pyrolysis Temperature on Product Distribution and Characteristics of Anaerobic Sludge

Energies ◽  
2019 ◽  
Vol 13 (1) ◽  
pp. 79
Author(s):  
Muhammad Usman Hanif ◽  
Mohammed Zwawi ◽  
Sergio C. Capareda ◽  
Hamid Iqbal ◽  
Mohammed Algarni ◽  
...  
Keyword(s):  
Pyrolysis Temperature ◽  
Product Distribution ◽  
Biofuel Production ◽  
Thermochemical Conversion ◽  
Anaerobic Sludge ◽  
Cow Dung ◽  
High Heating Value ◽  
Bio Oil ◽  
Different Temperatures ◽  
Combustible Gases

Pyrolysis of anaerobically digested sludge can serve as an efficient biomass for biofuel production. Pyrolysis produces products like char, bio-oil, and combustible gases by thermochemical conversion process. It can be used for sludge treatment that decreases sludge disposal problems. Sludge produced from anaerobic co-digestion (microalgae, cow dung, and paper) waste has high carbon and hydrogen content. We investigated the candidacy of the anaerobic sludge having high heating value (HHV) of 20.53 MJ/kg as a reliable biomass for biofuels production. The process of pyrolysis was optimized with different temperatures (400, 500, and 600 °C) to produce high quantity and improved quality of the products, mainly bio-oil, char, and gas. The results revealed that with the increase in pyrolysis temperature the quantity of char decreased (81% to 55%), bio-oil increased (3% to 7%), and gas increased (2% to 5%). The HHV of char (19.2 MJ/kg), bio-oil (28.1 MJ/kg), and gas (18.1 MJ/kg) were predominantly affected by the amount of fixed carbon, hydrocarbons, and volatile substance, respectively. The study confirmed that the anaerobic sludge is a promising biomass for biofuel production and pyrolysis is an efficient method for its safe disposal.

scholarly journals Effects of organic amendment on some soil physicochemical characteristics and vegetative properties of Zea mays in wetland soils of the Niger Delta impacted with crude oil

2019 ◽  
Vol 8 (S1) ◽  
pp. 423-435
Author(s):  
Francis E. Egobueze ◽  
Josiah M. Ayotamuno ◽  
Chukwujindu M. A. Iwegbue ◽  
Chibogwu Eze ◽  
Reuben N. Okparanma
Keyword(s):  
Zea Mays ◽  
Crude Oil ◽  
Incubation Time ◽  
Contaminated Soils ◽  
Niger Delta ◽  
Organic Amendments ◽  
Plant Performance ◽  
Wetland Soils ◽  
Cow Dung ◽  
Total Period

Abstract Purpose This study sought to investigate the effects of organic amendments on the degradation of hydrocarbons and vegetative properties of Zea mays grown in crude oil-contaminated wetland soils of the Niger Delta, Nigeria. Methods Two soil types were investigated, namely, fadama soil (oxisol) and swamp forest soil (utisol). For each soil type, 48 treatment cells and 1 control containing 1 kg of soil each were spiked with crude oil at concentrations ranging from 50 to 200 g kg−1, representing 5–20% (m/m) contamination levels, respectively. Then, 5 days after the contamination, the soils were amended with cow dung (CD), poultry waste (PW), and palm oil waste (POW). The ratios of soil to organic amendments used were 1:1 and 2:1. The soils were tilled and irrigated regularly, and monitored for a total period of 112 days. The same conditions were used to investigate the vegetative properties of Z. mays in these oil-contaminated soils with organic amendments. Results The total organic carbon (TOC) and pH increased significantly within the first 2 weeks after crude oil contamination; thereafter, the pH of the soil decreased significantly over incubation time, while there was steady increase in TOC with incubation time. The percentage nitrogen and total petroleum hydrocarbons (TPH) decreased significantly. The utisol soil showed better plant performance, despite the lower hydrocarbon degradation rate. Conclusion The organic amendments showed a TPH degradation trend that followed the order: PW > CD > POW. They also improved the seed emergence of Zea mays.

scholarly journals Qualidade físico-química e toxicológica de farinha obtida do eixo central de jaca

2016 ◽  
Vol 11 (4) ◽  
pp. 91
Author(s):  
Hyago Costa Sousa ◽  
Nathan José Pereira da Silva ◽  
Emmanuel Moreira Pereira ◽  
Carlos Roberto Marinho da Silva Filho ◽  
Agda Letícia Barbosa de Macêdo
Keyword(s):  
Physicochemical Characterization ◽  
Artemia Salina ◽  
Viable Alternative ◽  
Central Axis ◽  
Different Temperatures

A produção de farinha do eixo central de jaca se apresenta como uma alternativa viável para o aproveitamento dessa parte do fruto e sua utilização na indústria. O projeto foi desenvolvido no Centro de Ciências Humanas, Sociais e Agrárias, Bananeiras-PB pertencente a Universidade Federal da Paraíba. Os frutos foram adquiridos no pomar do CCHSA. As farinhas foram obtidas a partir da secagem do eixo central em quatro diferentes temperaturas 50, 60, 70 e 80 °C. Foi determinada a potencialidade toxicológica frente Artemia Salina do eixo central e de suas respectivas farinhas bem como sua caracterização físico-química. O eixo central de jaca não apresentou toxicidade assim como as farinhas obtidas a 50, 60 e 70 °C. A farinha do eixo central obtida a temperatura de 50 °C apresentou os melhores resultados nas análises físico-químicas.Physicochemical and toxicological quality of flour obtained from the central axis of jackfruitAbstract The production of flour from the central axis of jackfruit is presented as a viable alternative to the use of this part of the fruit and its use in industry. The project was developed in the Humanities Center, Social and Agricultural, Bananeiras-PB belonging to the Federal University of Paraíba. The fruits were purchased in CCHSA orchard. The flour were obtained by drying the central axis at four different temperatures 50, 60, 70 and 80 ° C. It was determined the toxicological potential front Artemia Salina central axis and their respective flours and their physicochemical characterization. The central axis of jackfruit showed no toxicity as well as the flour obtained at 50, 60 and 70 ° C. The flour the central axis obtained at 50 ° C showed the best results in physicochemical analyzes.

scholarly journals ASSESSMENT OF PHYSICOCHEMICAL QUALITY OF THE POLLUTING LOAD OF LEACHATES FROM THE WILD DUMP OF EL HAJEB CITY (MOROCCO)

2017 ◽  
Vol 5 (6) ◽  
pp. 63-71 ◽  
Author(s):  
Abderrahmane Gamar ◽  
Zakaria Khiya ◽  
Touria Zair ◽  
Mohammed El Kabriti ◽  
Abdelaziz Bouhlal ◽  
...  
Keyword(s):  
Water Table ◽  
Physicochemical Characterization ◽  
Specific Treatment ◽  
Physicochemical Analysis ◽  
International Standards ◽  
Mineral Salts ◽  
Inorganic Matter ◽  
The One ◽  
Permeable Soil

The dump in the town of El Hajeb (Morocco) is devoid of a collection and treatment system of the generated brownish effluents known as leachates. In a permeable soil and of a water table circulating in shallow depth, these percolate, after their generation, accumulate at the bottom of the waste and can infiltrate through the ground to reach the underlying water table, thus causing its contamination. Leachate would require, therefore, a specific treatment before their rejection in the receiving environment. This study aims to make a physicochemical characterization of these leachates. To do this, we conducted a series of sampling, from May 2015 to January 2017. During this period, the physicochemical analysis revealed, on the one hand, that it is discharge juice in the acidogenesis phase, conveying a significant  pollutant load rich in organic and inorganic matter (COD = 23597.5 ± 595.61 mgO2 L-1), in mineral salts (EC = 17.55 ± 0.72 mS cm-1) and in nutrient salts (TKN = 888.54 ± 13.53 mg-N L-1 and TP = 139.65 ± 48.89 mg-P L-1), concentrations exceed the values allowed by Moroccan and international standards, what makes these effluents toxic to the surrounding environment. By the present study, we incite decision-makers to manage well effectively the discharges taking into account the risks of the leachates generated.

scholarly journals Synthesis and Catalase Mimic Activity of MnO2 Nano Powder Prepared by Hydrothermal Process

2019 ◽  
Vol 27 (2) ◽  
pp. 228-237 ◽  
Author(s):  
Rashed T. Rasheed ◽  
Sariya D. Al-Algawi ◽  
Rosul M. N.
Keyword(s):  
Crystal Structure ◽  
Electron Microscopy ◽  
Annealing Temperature ◽  
Hydrothermal Process ◽  
X Ray Diffraction ◽  
X Ray ◽  
Nano Powder ◽  
Atomic Force ◽  
Different Temperatures ◽  
Scanning Electron

Manganese dioxide (MnO2) nanopowder has been synthesized by hydrothermal method. MnO2 was annealed at different temperatures (250, 400, 550, 700˚C). The crystal structure and surface morphology of these nanostructures were characterized by X-ray diffraction (XRD), Atomic Force Microscope (AFM) and Scanning Electron Microscopy (SEM). The catalase mimic activity (catalytic activity) of MnO2 against hydrogen peroxide (H2O2) was studied by using the new method and found that 400˚C is the best annealing temperature.

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