Evaluation of resistance to corrosion cracking of irradiated austenitic chromium-nickel steels by impact bending tests on miniature specimens

Author(s):  
B. Z. Margolin ◽  
N. E. Pirogova ◽  
A. A. Sorokin ◽  
A. M. Morozov

In this work, we present results of a bending test of miniature specimens made of chromium-nickel stainless austenitic steels of grades 321 (08Kh18N10T), 316 (06Kh16N11M3) and 304 (02Kh18N9) irradiated to various damage doses from 4 to 125 dpa in different energy neutron spectra. Effects of the damage dose and the neutron energy spectrum on the intergranular fracture energy, which determines the strength of grain boundaries, are studied. Two neutron spectra are considered: one characteristic of the active zone of PWR and WWER reactors, and the other is typical for the active zone of fast core reactors. The relationship between the resistance to corrosion cracking of irradiated chromium-nickel steels 321, 316 and 304 and the strength of grain boundaries is considered.

Author(s):  
B. Z. Margolin ◽  
A. M. Morozov ◽  
N. E. Pirogova ◽  
M. N. Grigoriev

The paper proposes methods for assessing the strength of grain boundaries according to the results of testing miniature specimens by impact bending. Results of bending at low temperature are given to assess the strength of grain boundaries in austenitic chromium-nickel steels. The test temperature was determined when the proportion of brittle intergranular fracture of embrittled chromium-nickel steel 10Kh18N9 is at least 90%. Three types of miniature specimens of different geometric shapes have been developed, providing approximately the same absorbed energy when tested for impact bending. It is shown when it is necessary to use such miniature specimens.


Author(s):  
B. Z. Margolin ◽  
N. E. Pirogova ◽  
A. A. Sorokin ◽  
V. I. Kokhonov

This paper presents results of a corrosion cracking test of specimens of irradiated austenitic chromium- nickel steels of grades 321 (Kh18N10T), 316 (06Kh16N11M3) and 304 (02Kh18N9). Specimens were irradiated to different damage dose from 4.5 to 150 dpa. The tests were carried out in autoclaves in the water environment simulating a coolant of the first circuit of WWER reactors at temperatures of 290–315°С. The influence of the damage dose and the neutron energy spectrum on the tendency of steels to stress corrosion cracking (SCC) is analyzed. The dominant SCC mechanisms for various austenitic steels are determined. Loading modes effects on the SCC resistance of specimens irradiated to the same damage dose are compared.


Author(s):  
Ho-Sang Shin ◽  
Jin-Ki Hong ◽  
Koo-Kab Chung ◽  
Hae-Dong Chung ◽  
Gwang-Yil Kim ◽  
...  

As the design life of new nuclear power plant increases, the austenitic stainless cladding integrity of reactor vessel becomes one of the new concerns. Since 1970’s, there have been some specific recommendations on delta ferrite content of austenitic cladding of reactor vessels and welds. It has been known that the delta ferrite is beneficial for reducing micro-fissure in welds, though the high delta ferrite content increases the probability of embrittlment of welds. In this study, the mechanical and microstructural properties of austenitic weld metals with the limit values of the recommended range (5 ∼ 18 FN) of the delta ferrite control on low alloy steels were characterized by using bending test and scanning electron microscopy. The base metal was ASME Code Sec. II specification SA 508 Gr. 3 Cl. 1 plate and weld materials were EQ308L and EQ309L strips. Four kinds of cladding were deposited with submerged arc welding process on SA508 cl.3 plates. The bending tests were performed through ASME code Sec. IX and the microstructure of fractured surfaces was analyzed by scanning electron microscopy (SEM). In bending tests, there were no fractures except the highest delta ferrite content specimens (28FN). From the SEM observation of fractured surfaces, cracks initiated from the interface between austenite and ferrites phases in the cladding layer and propagated through the continuous interfaces between two phases. For specimens without continuous interfaces of two phases, though the cracks were observed in the interface of phases, the propagation of cracks was not observed. From the test results, continuous interfaces between austenite matrix and ferrite phase provide the path for crack propagation. And the delta ferrite content affects the integrity of cladding of reactor vessel.


Author(s):  
Hisakazu Tajika ◽  
Takahiro Sakimoto ◽  
Tsunehisa Handa ◽  
Rinsei Ikeda ◽  
Joe Kondo

Recently high grade pipeline project have been planned in hostile environment like landslide in mountain area, liquefaction in reclaimed land or the frost heave in Polar Regions. Geohazards bring large scale ground deformation and effect on the varied pipeline to cause large deformation. Therefore, strain capacity is important for the pipeline and strain based design is also needed to keep gas transportation project in safe. High grade steel pipe for linepipe tends to have higher yield to tensile (Y/T) ratio and it has been investigated that the lower Y/T ratio of the material improves strain capacity in buckling and tensile limit state. In onshore pipeline project, pipe usually transported in 12 or 18m each and jointed in the field. Girth weld (GW) is indispensable so strength matching of girth weld towards pipe body is important. In this study strain capacity of Grade X70 high strain pipes with size of 36″ OD and 23mm WT was investigated with two types of experiments, which are full scale pipe bending tests and curved wide plate tests. The length of the specimen of full scale bending tests were approximately 8m and girth weld was made in the middle of joint length. A fixed internal pressure was applied during the bending test. Actual pipe situation in work was simulated and both circumferential and longitudinal stress occurred in this test. Test pipes were cut and welded, GTAW in first two layer and then finished by GMAW. In one pipe, YS-TS over-matching girth weld (OVM) joint was prepared considering the pipe body grade. For the other pipe, intentionally under-matching girth weld (UDM) joint was prepared. After the girth welding, elliptical EDM notch were installed in the GW HAZ as simulated weld defect. In both pipe bending tests, the buckling occurred in the pipe body at approximately 300mm apart from the GW and after that, deformation concentrated to buckling wrinkle. Test pipe breaking locations were different in the two tests. In OVM, tensile rupture occurred in pipe body on the backside of buckling wrinkle. In UDM, tensile rupture occurred from notch in the HAZ. In CWP test, breaking location was the HAZ notch. There were significant differences in CTOD growth in HAZ notch in these tests.


Author(s):  
Shinobu Kawaguchi ◽  
Naoto Hagiwara ◽  
Mitsuru Ohata ◽  
Masao Toyoda

A method of predicting the leak/rupture criteria for API 5L X80 and X100 linepipes was evaluated, based on the results of hydrostatic full-scale tests for X60, X65, X80 and X100 linepipes with an axially through-wall (TW) notch. The TW notch test results clarified the leak/rupture criteria, that is, the relationship between the initial notch lengths and the maximum hoop stresses during the TW notch tests. The obtained leak/rupture criteria were then compared to the prediction of the Charpy V-notch (CVN) absorbed energy-based equation, which has been proposed by Kiefner et al. The comparison revealed that the CVN-based equation was not applicable to the pipes having a CVN energy (Cv) greater than 130 J and flow stress greater than X65. In order to predict the leak/rupture criteria for these linepipes, the static absorbed energy for ductile cracking, (Cvs)i, was introduced as representing the fracture toughness of a pipe material. The (Cvs)i value was determined from the microscopic observation of the cut and buffed Charpy V-notch specimens after static 3-point bending tests. The CVN energy in the original CVN-based equation was replaced by an equivalent CVN energy, (Cv)eq’ which was defined as follows: (Cv)eq = 4.5 (Cvs)i. The leak/rupture criteria for the X80 and X100 linepipes with higher CVN energies were reasonably predicted by the modified equation using the (Cvs)i value.


Author(s):  
Pornvitoo Rittinon ◽  
Ken Suzuki ◽  
Hideo Miura

Copper thin films are indispensable for the interconnections in the advanced electronic products, such as TSV (Trough Silicon Via), fine bumps, and thin-film interconnections in various devices and interposers. However, it has been reported that both electrical and mechanical properties of the films vary drastically comparing with those of conventional bulk copper. The main reason for the variation can be attributed to the fluctuation of the crystallinity of grain boundaries in the films. Porous or sparse grain boundaries show very high resistivity and brittle fracture characteristic in the films. Thus, the thermal conductivity of the electroplated copper thin films should be varied drastically depending on their micro texture based on the Wiedemann-Franz’s law. Since the copper interconnections are used not only for the electrical conduction but also for the thermal conduction, it is very important to quantitatively evaluate the crystallinity of the polycrystalline thin-film materials and clarify the relationship between the crystallinity and thermal properties of the films. The crystallinity of the interconnections were quantitatively evaluated using an electron back-scatter diffraction method. It was found that the porous grain boundaries which contain a significant amount of vacancies increase the local electrical resistance in the interconnections, and thus, cause the local high Joule heating. Such porous grain boundaries can be eliminated by control the crystallinity of the seed layer material on which the electroplated copper thin film is electroplated.


2006 ◽  
Vol 309-311 ◽  
pp. 1191-1194
Author(s):  
Shuichi Wakayama ◽  
Teppei Kawakami ◽  
Junji Ikeda

Microfracture process during bending tests of alumina ceramics used for artificial joints was evaluated by acoustic emission (AE) technique. Four-point bending tests were carried out in air, refined water, physiological saline and simulated body fluid. AE behavior during bending test inhibited the rapid increasing point of AE events and energy prior to the final unstable fracture. It was understood that the bending stress at the increasing point corresponds to the critical stress for maincrack formation. The critical stress was affected by water in environments more strongly than fracture strength. Consequently, it was suggested that the characterization of maincrack formation is essential for the long-term reliability assessment of load-bearing bioceramics.


Author(s):  
Tomáš Binar ◽  
Jiří Švarc ◽  
Petr Dostál ◽  
Michal Šustr ◽  
Jan Tippner

This article deals with the spread of corrosion in material at different exposure times, and its effect on the measured brittle fracture and notch impact strength under different temperature conditions. To assess the degradational effect of corrosion on the material characteristics represented by the measured impact strength, we conducted a fractographic analysis of fracture surfaces, the aim of which was to evaluate the spread of corrosion in the material. In the first part of the experiment, two corrosion tests are simulated with a duration time of 432 and 648 hours, to compare the degradation effect of corrosion on the notch impact strength, depending on the duration of the corrosion tests. The following part shows the results of the impact bending test, where the experiment was conducted in an area of reduced and increased temperatures. The final part summarizes the results of the fractographic analysis of sample fracture surfaces from the impact bending tests. Based on the measured the length of the corrosion cracks, we analyzed the sample at the notch and from the material surface after the impact bending test.


Author(s):  
Mohammed Abdulhussein Al-Shuwaili ◽  
Alessandro Palmeri ◽  
Maria Teresa Lombardo

Push-out tests (POTs) have been widely exploited as an alternative to the more expensive full-scale bending tests to characterize the behaviour of shear connections in steel-concrete composite beams. In these tests, two concrete slabs are typically attached to a steel section with the connectors under investigation, which are then subjected to direct shear. The results allow quantifying the relationship between applied load and displacements at the steel-concrete interface. Since this relationship is highly influenced by the boundary conditions of POT samples, different experimental setups have been used, where the slabs are either restricted or free to slide horizontally, as researchers have tried to reduce any discrepancy between POT and full-scale composite beam testing. Based on a critical review of various POT configurations presented in the dedicated literature, this paper presents an efficient one-sided POT (OSPOT) method. While OSPOT and POT specimens are similar, in the proposed OPSPOT setup only one of the two slabs is directly loaded in each test, and the slab is free to move vertically. Thus, two results can be obtained from one specimen, i.e. one from each slab. A series of POTs and OSPOTs have been conducted to investigate the behaviour and the shear resistance of headed stud connectors through the two methods of testing. The results of this study than were compared with those of different POTs setups conducted by other researchers. The new OSPOT results show in general an excellent agreement with the analytical predictions offered by both British and European standards, as well as the estimated shear resistance proposed other researchers in the literature. These findings suggest that the proposed one-sided setup could be used as an efficient and economical option for conducting the POT, as it has the potential not only to double the number of results, but also to simplify the fabrication of the samples, which is important in any large experimental campaign, and to allow testing with limited capacity of the actuator. 


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