Effects of Delta - Ferrite Content on the Integrity of Reactor Vessel Cladding

Author(s):  
Ho-Sang Shin ◽  
Jin-Ki Hong ◽  
Koo-Kab Chung ◽  
Hae-Dong Chung ◽  
Gwang-Yil Kim ◽  
...  

As the design life of new nuclear power plant increases, the austenitic stainless cladding integrity of reactor vessel becomes one of the new concerns. Since 1970’s, there have been some specific recommendations on delta ferrite content of austenitic cladding of reactor vessels and welds. It has been known that the delta ferrite is beneficial for reducing micro-fissure in welds, though the high delta ferrite content increases the probability of embrittlment of welds. In this study, the mechanical and microstructural properties of austenitic weld metals with the limit values of the recommended range (5 ∼ 18 FN) of the delta ferrite control on low alloy steels were characterized by using bending test and scanning electron microscopy. The base metal was ASME Code Sec. II specification SA 508 Gr. 3 Cl. 1 plate and weld materials were EQ308L and EQ309L strips. Four kinds of cladding were deposited with submerged arc welding process on SA508 cl.3 plates. The bending tests were performed through ASME code Sec. IX and the microstructure of fractured surfaces was analyzed by scanning electron microscopy (SEM). In bending tests, there were no fractures except the highest delta ferrite content specimens (28FN). From the SEM observation of fractured surfaces, cracks initiated from the interface between austenite and ferrites phases in the cladding layer and propagated through the continuous interfaces between two phases. For specimens without continuous interfaces of two phases, though the cracks were observed in the interface of phases, the propagation of cracks was not observed. From the test results, continuous interfaces between austenite matrix and ferrite phase provide the path for crack propagation. And the delta ferrite content affects the integrity of cladding of reactor vessel.

1989 ◽  
Vol 153 ◽  
Author(s):  
D. Feldman ◽  
M.A. Lacasse

AbstractThe morphology of blended polyurethane (PU) sealants was studied by scanning electron microscopy (SEM) and differential scanning calorimetry (DSC). The PU was modifided by mechanical mixing with various amounts of Lignin (L) to achieve a homogeneous blend. Specimens were subjected to control (C), accelerated weathering (AW), and natural weathering (NW) conditions. Results obtained from SEM analysis reveal an even distribution of L particles in the PU matrix. Furthermore, the SEM photomicrographs clearly emphasize the differing morphologies of the constituent phases. They also depict the differences in surface texture between control and aged specimens. The DSC analysis shows that the two phases are immiscible which is in agreement with observations by microscopy.


2003 ◽  
Vol 11 (4) ◽  
pp. 354-360 ◽  
Author(s):  
Wilson José Garbelini ◽  
Guilherme Elias Pessanha Henriques ◽  
Manoel Troia Junior ◽  
Marcelo Ferraz Mesquita ◽  
Cássia Cilene Dezan

The bond strength by three point bending strength of two metal substrates (commercially pure titanium or grade II, and Ti-6Al-4V alloy or grade V) combined to three distinct low-fusing ceramic systems (LFC) and the nature of porcelain-metal fracture by scanning electron microscopy (SEM) were evaluated. The results were compared to a combination of palladium-silver (Pd-Ag) alloy and conventional porcelain (Duceram VMK68). Sixty metal strips measuring 25x3x0.5mm were made - 30 of titanium grade II and 30 of titanium grade V, with application of the following types of porcelain: Vita Titankeramik, Triceram or Duceratin (10 specimens for each porcelain). The porcelains were bonded to the strips with dimensions limited to 8x3x1mm. The control group consisted of ten specimens Pd-Ag alloy/Duceram VMK68 porcelain. Statistical analyses were made by one-way analysis of variance (ANOVA) and Tukey test at 5% significance level. Results showed that the bond strength in control group (48.0MPa ± 4.0) was significantly higher than the Ti grade II (26.7MPa ± 4.1) and Ti grade V (25.2MPa ± 2.2) combinations. When Duceratin porcelain was applied in both substrates, Ti grade II and Ti grade V, the results were significantly lower than in Ti grade II/Vitatitankeramik. SEM analysis indicated a predominance of adhesive fractures for the groups Ti grade II and Ti grade V, and cohesive fracture for control group Pd-Ag/Duceram. Control group showed the best bond strength compared to the groups that employed LFC. Among LFC, the worst results were obtained when Duceratin porcelain was used in both substrates. SEM confirmed the results of three point bending strength.


1989 ◽  
Vol 154 ◽  
Author(s):  
D. FeldMan ◽  
N. A. Lacasse

AbstractThe morphology of blended polyurethane (PU) sealants was studied by scanning electron microscopy (SEM) and differential scanning calorimetry (DSC). The PU was modifided by mechanical mixing with various amounts of Lignin (L) to achieve a homogeneous blend. Specimens were subjected to control (C), accelerated weathering (AW), and natural weathering (NW) conditions. Results obtained from SEM analysis reveal an even distribution of L particles in the PU matrix. Furthermore, the SEM photomicrographs clearly emphasize the differing morphologies of the constituent phases. They also depict the differences in surface texture between control and aged specimens. The DSC analysis shows that the two phases are immiscible which is in agreement with observations by microscopy.


2018 ◽  
Vol 29 (2) ◽  
pp. 175
Author(s):  
Wisam J. Aziz ◽  
Raad S. Sabri ◽  
Abbas K. Jarallah

Abstract Titanium dioxide was prepared using pulsed laser ablation (PLA) and hydrothermal method. Scanning electron microscopy images showed that the product from hydrothermal method had a nanotube shape, whereas those from PLA in liquid were nanoparticles. The optical properties in the absorption curve of product from the hydrothermal method were slightly greater than those from the PLA method, and the energy gaps were 3.39 and 3.26 eV for the hydrothermal method and PLA, respectively. XRD results showed that the TiO2 prepared through PLA showed one phase (rutile), whereas those prepared through hydrothermal method showed two phases (anatase and rutile). Moreover, the product from hydrothermal method had smaller particle size smaller than that from PLA. Furthermore, the product yield and the required reaction time of the hydrothermal method were higher than those of PLA.


World Science ◽  
2019 ◽  
Vol 1 (11(51)) ◽  
pp. 25-30
Author(s):  
Подрезов Ю. М. ◽  
Ремез М. В. ◽  
Холявко В. В. ◽  
Прокопчук М. Д.

The temperature and velocity sensitivity of the mechanical properties of TiAl-based alloys were investigated. The structure was determined by scanning electron microscopy in SEI mode. Mechanical properties were determined by the results of tensile and bending tests. It was found that the temperature and velocity dependence of the mechanical properties in alloys with 47% Al is practically absent. This makes them promising for use as structural materials, due to the stability of their properties.


2018 ◽  
Vol 910 ◽  
pp. 52-57
Author(s):  
Yuan Yuan ◽  
Peng Wan Chen ◽  
Er Feng An ◽  
Jian Rui Feng

In this investigation, thin Aluminum alloys 2A12 and Copper T2 composite plates which are both 1mm thick were obtained successfully by the method of explosive welding. The effect of annealing on the interface microstructures of the composite plates was investigated under different temperatures. Optical microscopy, scanning electron microscopy, micro-hardness test and bending test were performed. The results demonstrated that the Al/Cu composite plates were bonded well. The bonding interface of the Al/Cu composite plates had a wavy form. Micro-hardness measurements showed that the hardness of the composite plates near the interface was higher than other parts and the hardness of the whole composite plates was lower after annealing. The bending test showed the composite plates can be deformed or shaped.


2012 ◽  
Vol 186 ◽  
pp. 130-134
Author(s):  
Maria W. Richert ◽  
Jan Richert ◽  
Marzanna Książek ◽  
Agnieszka Hotloś ◽  
Paweł Pałka ◽  
...  

Powder metallurgy is widely used to the production of AgNi and AgSnBi powders employed for electrical contacts. In the work AgNi and AgSnBi powders were consolidated by the cyclic extrusion compression (CEC) method enabling cyclic unlimited deformation. In the initial stage the AgNi powder contained the two phases Ag and Ni, recognized by the EDX technique using scanning electron microscopy (SEM). The investigations shown that the Ni phase is distributed in the form of small granules around larger Ag granules. In the AgSnBi powder phases Ag + Bi + Ag3Sn (ξ) were distributed uniformly. It was found that after the CEC consolidation phases were excellently joined without cavities and cracks. Detailed observations of microstructure have been performed by the transmission electron microscopy (TEM) and revealed inside the consolidated granules nanometric grains with the nanometric twins inside.


2015 ◽  
Vol 1767 ◽  
pp. 107-111
Author(s):  
Lioudmila Fomina ◽  
Jorge Godínez Sánchez ◽  
José A. Olivares ◽  
Fabio L. Cuppo Sant´Anna ◽  
Luis E. Sansores ◽  
...  

ABSTRACTHyperbranched structures containing pyrrole units were obtained from ortho-, meta- and para-diaminodiphenyldiacetylenes as AB2 type monomers by one-step polymerization.The para-hyperbranched compound was observed by optical microscopy and scanning electron microscopy.Microscopy studies identify two phases. The first is the insoluble one which gives origin to flake type structures. The second is acetone soluble phase, which generated crystalline structure manifesting in optic anisotropy and rhomboids and triangles dendrimeric structures.


Author(s):  
P.S. Porter ◽  
T. Aoyagi ◽  
R. Matta

Using standard techniques of scanning electron microscopy (SEM), over 1000 human hair defects have been studied. In several of the defects, the pathogenesis of the abnormality has been clarified using these techniques. It is the purpose of this paper to present several distinct morphologic abnormalities of hair and to discuss their pathogenesis as elucidated through techniques of scanning electron microscopy.


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