scholarly journals Calibration of spectrometric detectors for air kerma rates in environmental monitoring

2020 ◽  
Vol 35 (4) ◽  
pp. 323-330
Author(s):  
Marcel Ohera ◽  
Daniel Sas ◽  
Petr Sladek

The spectrometric systems, especially based on NaI(Tl) and HPGe detectors, are used for nuclide identification and calculation of their activities from the ground measurements and air-borne monitoring. The determination of the air kerma (dose) rates is also very important for environmental measurements. In such cases, the detectors should be calibrated for air kerma (dose) rates in nGyh?1 or ?Gyh?1. A simple calibration of NaI(Tl), HPGe as well as plastic detectors for the low-level air kerma rates is presented in this contribution. This calibration is based on comparing the relative absorbed energy rate in detectors (MeVs?1) calculated from spectra with the air kerma rates calculated by the Monte Carlo simulation and supplementary to the data from the RSS Reuter&Stokes high pressure ion chamber. This method also eliminates the conversion from the non-air kerma rates in crystals to the air kerma rates. Three different types of small cylindrical detectors were calibrated for the air kerma rates from the background of 26 nGyh?1 to some tens of ?Gyh?1 in the energy range to the maximum of 3 MeV. The results of calibrations of the 3" x 3" NaI(Tl), HPGe detector and a small plastic detector (made of polystyrene) including soxme examples of environmental measurements are presented.

2019 ◽  
Vol 323 (1) ◽  
pp. 399-413 ◽  
Author(s):  
Anumaija Leskinen ◽  
Susanna Salminen-Paatero ◽  
Antti Räty ◽  
Merja Tanhua-Tyrkkö ◽  
Taneli Iso-Markku ◽  
...  

AbstractDetermination of 14C, 55Fe, 63Ni and gamma emitters in two different types of activated reactor pressure vessel (RPV) steel samples were carried out. The gamma emitters were analysed using HPGe detectors with ISOCS and standard geometry calibrations. Two radioanalytical procedures for the 14C, 55Fe, 63Ni analysis were developed using inactive samples and activated samples were analysed using modified procedures. A Monte Carlo code was used for the modelling of the activation results. The obtained measured and calculated results were comparable.


Author(s):  
D. R. Liu ◽  
S. S. Shinozaki ◽  
R. J. Baird

The epitaxially grown (GaAs)Ge thin film has been arousing much interest because it is one of metastable alloys of III-V compound semiconductors with germanium and a possible candidate in optoelectronic applications. It is important to be able to accurately determine the composition of the film, particularly whether or not the GaAs component is in stoichiometry, but x-ray energy dispersive analysis (EDS) cannot meet this need. The thickness of the film is usually about 0.5-1.5 μm. If Kα peaks are used for quantification, the accelerating voltage must be more than 10 kV in order for these peaks to be excited. Under this voltage, the generation depth of x-ray photons approaches 1 μm, as evidenced by a Monte Carlo simulation and actual x-ray intensity measurement as discussed below. If a lower voltage is used to reduce the generation depth, their L peaks have to be used. But these L peaks actually are merged as one big hump simply because the atomic numbers of these three elements are relatively small and close together, and the EDS energy resolution is limited.


2020 ◽  
Vol 70 (12) ◽  
pp. 4594-4600

The purpose of this study was to characterize some types of biomass wastes resulted from different activities such as: agriculture, forestry and food industry using thermogravimetric and ICP-MS analyses. Also, it was optimized an ICP-MS method for the determination of As, Cd and Pb from biomass ash samples. The ICP-MS analysis revealed that the highest concentration of metals (As, Cd, Pb) was recorded in the wood waste ash sample, also the thermogravimetric analysis indicated that the highest amount of ash was obtained for the same sample (26.82%). The biomass wastes mentioned in this study are alternative recyclable materials, reusable as pellets and briquettes. Keywords: ash, biomass, ICP-MS, minor elements, TG


2018 ◽  
Vol 69 (5) ◽  
pp. 1139-1144
Author(s):  
Iosif Lingvay ◽  
Adriana Mariana Bors ◽  
Livia Carmen Ungureanu ◽  
Valerica Stanoi ◽  
Traian Rus

For the purpose of using three different types of painting materials for the inner protection of the transformer vats, their behavior was studied under actual conditions of operation in the transformer (thermal stress in electro-insulating fluid based on the natural ester in contact with copper for electro-technical use and electro-insulating paper). By comparing determination of the content in furans products (HPLC technique) and gases formed (by gas-chromatography) in the electro-insulating fluid (natural ester with high oleic content) thermally aged at 130 �C to 1000 hours in closed glass vessels, it have been found that the presence the investigated painting materials lead to a change in the mechanism and kinetics of the thermo-oxidation processes. These changes are supported by oxygen dissolved in oil, what leads to decrease both to gases formation CO2, CO, H2, CH4, C2H4 and C2H6) and furans products (5-HMF, 2-FOL, 2 -FAL and 2-ACF). The painting materials investigated during the heat treatment applied did not suffer any remarkable structural changes affecting their functionality in the electro-insulating fluid based on vegetable esters.


Medicina ◽  
2021 ◽  
Vol 57 (7) ◽  
pp. 679
Author(s):  
Monica Iuliana Ungureanu ◽  
Liliana Sachelarie ◽  
Radu Ciorap ◽  
Bogdan Aurelian Stana ◽  
Irina Croitoru ◽  
...  

Background and Objectives: Different types of food introduced gradually in the diet will expose children to different food allergens, increasing the chance of developing allergic diseases. The aim of our study was to determine if allergen-specific IgE values can influence, depending on the diet, the prediction of remission of urticaria in children. Materials and Methods: This prospective study was conducted in 132 patients diagnosed over two years with urticaria, admitted to “Sf. Maria” Clinical Pediatric Hospital Iaşi. Total IgE assay was performed by ELISA, and determination of specific serum IgE by the CLA System Quanti Scan method (Innogenetics, Heiden, Germany). Data were gathered and statistical analysis was performed using statistical software SPSS, using descriptive and inferential statistics. Results: The determination of specific IgE to food allergens was performed on a total of 132 cases. The values of specific IgE were positive for one or more food allergens in 84 patients (63.64%). The most common allergens involved were: cow’s milk in 33.3% cases, egg white in 22.6% cases, and hazelnuts in 11.9% cases. The specific IgE values for the different types of food included in our study had a predictive value for disease remission. Conclusions: The determination of specific IgE confirms the presence of a particular food allergen and may have predictive value for the future development of an allergic manifestation.


2020 ◽  
Vol 1679 ◽  
pp. 022045
Author(s):  
S B Rybalka ◽  
E A Kulchenkov ◽  
A A Demidov ◽  
N A Zhemoedov ◽  
A Yu Drakin ◽  
...  

Author(s):  
Seung Wan Hong ◽  
Tae Won Kim ◽  
Jae Hun Kim

Abstract Physicians and nurses stand with their back towards the C-arm fluoroscope when using the computer, taking things out of closets and preparing drugs for injection or instruments for intervention. This study was conducted to investigate the relationship between the type of lead apron and radiation exposure to the backs of physicians and nurses while using C-arm fluoroscopy. We compared radiation exposure to the back in the three groups: no lead apron (group C), front coverage type (group F) and wrap-around type (group W). The other wrap-around type apron was put on the bed instead of on a patient. We ran C-arm fluoroscopy 40 times for each measurement. We collected the air kerma (AK), exposure time (ET) and effective dose (ED) of the bedside table, upper part and lower part of apron. We measured these variables 30 times for each location. In group F, ED of the upper part was the highest (p < 0.001). ED of the lower part in group C and F was higher than that in group W (p = 0.012). The radiation exposure with a front coverage type apron is higher than that of the wrap-around type and even no apron at the neck or thyroid. For reducing radiation exposure to the back of physician or nurse, the wrap-around type apron is recommended. This type of apron can reduce radiation to the back when the physician turns away from the patient or C-arm fluoroscopy.


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